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IR Mass NMR Exercises

The document provides instructions to analyze IR, mass, and 1H-NMR spectroscopy data to identify bonds, molecular fragments, and hydrogen environments for 10 compounds. For each compound, the type of bonds from the IR spectrum, molecular mass from mass fragments, and details of hydrogen peaks from 1H-NMR spectroscopy must be identified. A key lists the 10 compounds as: 1-bromopropane, propanone, propanoic acid, methyl ethanoate, 2-propanol, ethanal, 1-propanamine, propanamide, pentane, and 2-chloropropane.

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380 views12 pages

IR Mass NMR Exercises

The document provides instructions to analyze IR, mass, and 1H-NMR spectroscopy data to identify bonds, molecular fragments, and hydrogen environments for 10 compounds. For each compound, the type of bonds from the IR spectrum, molecular mass from mass fragments, and details of hydrogen peaks from 1H-NMR spectroscopy must be identified. A key lists the 10 compounds as: 1-bromopropane, propanone, propanoic acid, methyl ethanoate, 2-propanol, ethanal, 1-propanamine, propanamide, pentane, and 2-chloropropane.

Uploaded by

anthor
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as DOCX, PDF, TXT or read online on Scribd
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IR, Mass and 1H-NMR spectroscopy exercises

From
1

the 3 spectra given for each compound Identify:


the type of bonds from IR spectrum
the molecular mass of the compound and/or molecular fragments from the mass spectrum
the number of different hydrogen environments and the relative numbers of H atoms in
each environment from the 1H-NMR spectrum
Spectra
Analysis
Bonds

Mr of fragments

No. of peaks/ Area under


each peak/ Chemical shift
/Splitting pattern

Bonds

Mr of fragments

No. of peaks/ Area under


each peak/ Chemical shift
/Splitting pattern

Bonds

Mr of fragments

No. of peaks/ Area under


each peak/ Chemical shift
/Splitting pattern

Bonds

Mr of fragments

No. of peaks/ Area under


each peak/ Chemical shift
/Splitting pattern

Bonds

Mr of fragments

No. of peaks/ Area under


each peak/ Chemical shift
/Splitting pattern

Bons

Mr of fragments

No. of peaks/ Area under


each peak/ Chemical shift
/Splitting pattern

Bonds

Mr of fragments

No. of peaks/ Area under


each peak/ Chemical shift
/Splitting pattern

In CDCl3

Bonds

Mr of fragments

No. of peaks/ Area under


each peak/ Chemical shift
/Splitting pattern

Bonds

Mr of fragments

No. of peaks/ Area under


each peak/ Chemical shift
/Splitting pattern

1
0

Bonds

Mr of fragments

No. of peaks/ Area under


each peak/ Chemical shift
/Splitting pattern

Key:
1.
2.

1-bromopropane
Propanone/acetone

3.
4.

Propanoic acid
Methyl ethanoate

5.
6.

2-propanol
Ethanal

7.
8.

1-propanamine
Propanamide

9.

Pentane

10.

2-chloropropane

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