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Chemical Analysis in The Electron Microscope

The chapter describes principles of the chemical analysis in the SEM and TEM. From "Electron Microscopy and Analysis" textbook by Peter J. Goodhew, John Humphreys and Richard Beanland. Courtesy of Taylor and Francis Books UK.

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722 views62 pages

Chemical Analysis in The Electron Microscope

The chapter describes principles of the chemical analysis in the SEM and TEM. From "Electron Microscopy and Analysis" textbook by Peter J. Goodhew, John Humphreys and Richard Beanland. Courtesy of Taylor and Francis Books UK.

Uploaded by

CORE Materials
Copyright
© Attribution ShareAlike (BY-SA)
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as PDF, TXT or read online on Scribd
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Contents

(Note: Page numbers are as in the whole book so that the index remains valid)

Acronyms …………………………………………………….……………………… iii


Preface ………………………………………………………………………………. iv

6 Chemical analysis in the electron microscope

6.1 The generation of X-rays within a specimen ……………... 170


6.2 Detection and counting of X-rays ………………………… 174
6.3 X-ray analysis of bulk specimens …………………………. 184
6.4 X-ray analysis of thin specimens in the TEM ……………... 193
6.5 Quantitative analysis in an electron microscope …………... 196
6.6 Electron energy loss spectroscopy (EELS) ………………... 205
6.7 A brief comparison of techniques …………………………. 212
6.8 Questions …………………………………………………... 213

Further reading ……………………………………………………………..…………... 236


Answers …………………………………………………………………………………... 238
Index …………………………………………………………………………..…………... 243
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).
__________________________________________________________
Electron Microscopy and Analysis,
Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.
Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).

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