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Esprecto BLFO PDF

The document contains analysis results from 10 spectra of a sample. Each spectrum provides elemental analysis results showing concentrations of O, Fe, La and Bi. The concentrations vary slightly between spectra but Bi is consistently the dominant element at around 60% by weight.

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johan
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20 views14 pages

Esprecto BLFO PDF

The document contains analysis results from 10 spectra of a sample. Each spectrum provides elemental analysis results showing concentrations of O, Fe, La and Bi. The concentrations vary slightly between spectra but Bi is consistently the dominant element at around 60% by weight.

Uploaded by

johan
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
You are on page 1/ 14

7/26/2016 11:20:01 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 1


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 241979
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
57.89

Area
216147

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
6.98
12.24
1.16
37.13

Intensity
Corrn.
0.7718
1.0304
0.9040
0.9072

Weight%
14.34
18.82
2.03
64.82
100.00

Weight%
Sigma
0.38
0.31
0.29
0.48

Atomic%
57.53
21.63
0.94
19.91

7/26/2016 11:20:25 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 2


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 217308
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.02

Area
217956

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
7.67
10.21
0.97
33.39

Intensity
Corrn.
0.7824
1.0216
0.8982
0.9044

Weight%
16.97
17.29
1.87
63.88
100.00

Weight%
Sigma
0.42
0.32
0.31
0.51

Atomic%
62.78
18.33
0.80
18.10

7/26/2016 11:24:12 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 3


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 203610
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
57.97

Area
219014

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
7.35
8.95
0.81
31.77

Intensity
Corrn.
0.7781
1.0215
0.8962
0.9064

Weight%
17.45
16.18
1.67
64.70
100.00

Weight%
Sigma
0.44
0.32
0.32
0.53

Atomic%
64.07
17.03
0.71
18.19

7/26/2016 11:34:14 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 4


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 228974
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.00

Area
217447

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
7.52
12.11
2.23
33.18

Intensity
Corrn.
0.7987
1.0214
0.9062
0.8966

Weight%
15.50
19.52
4.05
60.92
100.00

Weight%
Sigma
0.40
0.32
0.31
0.50

Atomic%
59.11
21.33
1.78
17.78

7/26/2016 11:38:22 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 5


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 217609
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.27

Area
218109

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
7.20
11.00
2.25
32.74

Intensity
Corrn.
0.7917
1.0229
0.9055
0.8991

Weight%
15.48
18.31
4.24
61.98
100.00

Weight%
Sigma
0.41
0.32
0.32
0.51

Atomic%
59.64
20.20
1.88
18.28

7/26/2016 11:42:04 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 6


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 210007
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
57.94

Area
218712

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
6.96
10.93
2.12
32.16

Intensity
Corrn.
0.7906
1.0236
0.9057
0.8995

Weight%
15.29
18.54
4.06
62.10
100.00

Weight%
Sigma
0.41
0.32
0.32
0.51

Atomic%
59.21
20.57
1.81
18.41

7/26/2016 11:50:21 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 7


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 265946
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.21

Area
215041

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
7.63
15.31
3.80
37.24

Intensity
Corrn.
0.8052
1.0247
0.9141
0.8924

Weight%
13.49
21.25
5.91
59.35
100.00

Weight%
Sigma
0.34
0.31
0.30
0.46

Atomic%
54.38
24.55
2.75
18.32

7/26/2016 11:54:53 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 8


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 255120
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.08

Area
215660

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
7.09
14.58
3.72
36.15

Intensity
Corrn.
0.8009
1.0265
0.9147
0.8937

Weight%
13.10
21.02
6.01
59.86
100.00

Weight%
Sigma
0.36
0.31
0.31
0.47

Atomic%
53.69
24.69
2.84
18.79

7/26/2016 11:59:40 AM

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 10


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 243517
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.12

Area
215998

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
6.44
13.71
3.71
33.45

Intensity
Corrn.
0.8023
1.0269
0.9162
0.8928

Weight%
12.78
21.23
6.43
59.56
100.00

Weight%
Sigma
0.36
0.33
0.32
0.49

Atomic%
52.89
25.17
3.07
18.88

7/26/2016 12:13:01 P M

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 12


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 215370
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
57.99

Area
218084

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 4
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
21.04
7.59
3.22
19.61

Intensity
Corrn.
1.0087
0.9426
0.8768
0.8496

Weight%
37.47
14.46
6.59
41.47
100.00

Weight%
Sigma
0.50
0.31
0.35
0.55

Atomic%
82.27
9.10
1.67
6.97

7/26/2016 12:15:01 P M

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 13


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 234347
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.25

Area
217248

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
15.14
10.95
4.37
30.73

Intensity
Corrn.
0.8865
0.9832
0.8944
0.8718

Weight%
25.00
16.30
7.15
51.56
100.00

Weight%
Sigma
0.42
0.29
0.31
0.49

Atomic%
72.59
13.56
2.39
11.46

7/26/2016 12:19:04 P M

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 14


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 198440
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.06

Area
219290

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 4
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
20.25
6.41
2.83
19.35

Intensity
Corrn.
0.9973
0.9422
0.8730
0.8526

Weight%
38.28
12.83
6.11
42.78
100.00

Weight%
Sigma
0.52
0.31
0.36
0.56

Atomic%
83.33
8.00
1.53
7.13

7/26/2016 12:21:29 P M

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 15


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 217080
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
57.92

Area
218260

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
No peaks omitted
Processing option : All elements analyzed (Normalised)
Number of iterations = 4
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
27.31
4.83
2.23
12.53

Intensity
Corrn.
1.1609
0.9069
0.8599
0.8329

Weight%
50.61
11.45
5.58
32.36
100.00

Weight%
Sigma
0.58
0.32
0.39
0.59

Atomic%
88.77
5.76
1.13
4.34

7/26/2016 12:23:47 P M

Project 1
Project: Project 1
Owner: INCA
Site: Site of Interest 1

Sample: Sample 1
Type: Default
ID:

Spectrum Label: Spectrum 16


Livetime 60.0 s
Acquisition geometry ( degrees ):
Tilt = 0.0
Azimuth = 0.0
Elevation = 40.0
Accelerating voltage = 20.00 kV
Total spectrum counts = 221027
Sample data :
Strobe :

Energy (eV)
7.5

Resn. (eV)
58.01

Area
218027

Energy (eV)
-.1
6925.8

Resn. (eV)
59.50
145.48

Area
216288
93139

Optimization data : Cobalt K series


Strobe :
Optimization element :

Sample is unpolished X-ray corrections may be approximate.


Sample is uncoated
Detector efficiency : Calculation

Spectrum processing :
Peak possibly omitted : 3.682 keV
Processing option : All elements analyzed (Normalised)
Number of iterations = 3
Standard :
O SiO2 1-Jun-1999 12:00 AM
Fe Fe 1-Jun-1999 12:00 AM
La LaB6 1-Jun-1999 12:00 AM
Bi Bi 1-Jun-1999 12:00 AM
Element
OK
Fe K
La L
Bi M
Totals

App
Conc.
12.19
10.92
4.37
26.70

Intensity
Corrn.
0.8872
0.9879
0.9012
0.8700

Weight%
22.79
18.32
8.04
50.85
100.00

Weight%
Sigma
0.42
0.32
0.34
0.51

Atomic%
69.36
15.97
2.82
11.85

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