OPSIS LiquidLINE

SoxROC Extraction Unit

Automatic, Flexible and Safe
For solvent extractions

LP 1006 www.liquidline.se
 The SoxROC Extraction Unit
OPSIS LiquidLINE brings, once again, innovation to the wet chemistry market.
—— Innovative batch handling reduces operator time
—— Unique sealing system improves recovery of solvents
—— Unique control of solvent removal adds flexibility

By tradition Soxhlet is associated with solvent extraction. However, during all the
years since the Soxhlet method was described several improvements have been
made. Maybe the most important was when hot extraction was launched. This
drastically reduced the extraction time needed. The OPSIS LiquidLINE SoxROC
Extraction Unit is based on Randall and Twisselmann techniques, using hot solvent
and a closed system for optimal analytical conditions, still giving the same results
as the classical and well accepted Soxhlet.

The SoxROC is designed to be flexible and is therefore also capable of extractions

using other solvents and samples.

Stage 1 - Boiling
Boiling solvent is cover-
ing the sample so that
extractable material can Stage 2 - Rinsing
be liberated. The material is extracted
by the refluxed, con-
densed, solvent. Stage 3 - Drying
The cups are automati-
cally separated from the
hotplate and the cooling
phase beings.

www.liquidline.se
Reducing Time and Errors
—— With SoxROC, you can extract as many as 42 samples per
day with no loss in precision or accuracy.
—— Automation of all extraction steps and an innovative batch
handling reduces risk for errors.
—— Typically up to five times faster than the classical Soxhlet
technique.

Reducing Costs and Use of Solvents

—— Unique sealing system with more than 90% recovery reduces
cost for solvents and low water consumption saves water.
—— A large selection of seals, cups and standard thimbles
reduces costs when changing between applications and
solvents.
—— One single compact system without wires or computers
reduces costs for installation and operation.

Adding Flexibility and Safety

—— Unique control of solvent reduction adds flexibility for different
applications.
—— Security with high standard against dust, liquids and
explosives. All valves close to solvents are ATEX classified.
—— Operator safety is important and the SoxROC is equipped
with protection shield, closed addition of solvents, and easy
removal of recovered solvents.

The SoxROC follows officially approved methods for fat extraction.

 Benefits
After more than 25 years of experience within analysis, and with the introduction of the
world’s first wireless Kjeldahl system, we are now reinventing solvent extraction.
The SoxROC can be used for all common applications on the market, and meets the
requirements for an automatic system including boiling, rinsing and drying.
The SoxROC is also prepared for the future with several unique benefits.

Higher levels of Efficiency and Automation

The SoxROC is designed to allow fully automatic extraction
of up to 6 samples simultaneously.
The SoxROC will perform the complete process of boiling,
rinsing and recovery after inserting the samples. The pivoting
hotplate will ensure rapid cooling afterwards.

—— Innovative batch handling saves time and reduces

risk for errors. Easy to insert and manage 6 samples
simultaneously. A practical tray carrier makes it easy
to inspect samples before and after extraction. Same
sample tray can be used both in the balance room and
when inserting cups into the SoxROC.

—— A high throughput of 42 samples per day can

be achieved. Up to 6 samples can be extracted
simultaneously.

—— Fully automatic system with boiling, rinsing, and

recovery. The pivoting hotplate separates from the
cups for rapid cooling.

—— Several times faster than the classical

Soxhlet method with no loss
of accuracy or precision.

www.liquidline.se
Saving Costs
OPSIS LiquidLINE engineers have spent considerable
time to create a closed system which gives high efficiency
on heating and high recovery of solvents. This makes the
SoxROC a very cost efficient solution.
—— More than 90% recovery of solvents reduces costs.

—— Efficient cooling saves water costs.

—— OPSIS LiquidLINE designed sealing rings.

—— Unique two-fold sealing system with firstly manual

closing and secondly pivoting hotplate. Flexible sealing
with adaptive springs on all 6 positions.

—— All material in contact with solvents are in PTFE.

Added Flexibility and Solvent Control

The SoxROC can store up to six different extraction
applications which at any time easily can be reprogrammed.
To ensure flexibility, a solvent control and a large selection of
accessories are available.
—— Unique control of solvent removal makes it possible to
adjust solvent volumes at the different extraction steps.
It also makes it easy to achieve a consistent solvent
level at rinsing and drying. Possible to program the
valves with the amount of opening times, intervall and
opening time.

—— A large selection of cups makes it easy to adjust the

SoxROC to your applications. Glass and aluminium
cups in two different sizes. Smaller cups for more
efficient solvent use and aluminium cups for more
efficient boiling.

—— Different seals and thimble holders for different

applications.

—— Different lengths of standard cellulose thimbles, based

on 25 and 33 mm diameter, can be used.
 Operator Safety
Every care has been taken to ensure that the SoxROC is
safe and can be used in a safe way by the operator. To
avoid contact with solvents it is possible to add solvents
inside the instrument. It is also easy to remove solvents with
the flexible recovery tank.
—— Protection shield to cover cups during extraction
makes it safe for the operator. Automatic sensors will
stop extraction in case the protection shield is opened.

—— Closed addition of solvents by opening the top cover

of the instrument. Possible to add solvent before and
during extraction. Separate recovery tank with easy
access on the front panel.

—— Samples and cups are removed in one step so there

is no risk that solvent will drip from thimbles onto
the hotplate. It also saves time when operating the
instrument.

—— Main electronics are mounted in a pressurised box,

ensuring that no solvent can enter and cause electric
sparks. All valves close to solvents are ATEX classified.
The SoxROC follows IP55 for protection against dust
and liquids.

—— Overheat temperature level is automatically adjusted to

selected program temperature. Monitoring is done via
two separate safety systems.

One Integrated System

The SoxROC is easy to install in your lab. The system is
small and compact with no need for additional computers,
wires, or compressors.
—— One instrument with no additional requirement for
computers, compressors or complex wires to be
installed.

—— Recovery solvent tank inside the instrument, easy to

remove when emptying solvents.

www.liquidline.se
Customise
The SoxROC is built with the laboratory in mind, which means that it can be customised
towards your specific applications. The OPSIS LiquidLINE range is already prepared for a
variety of methods, solvents, filters and samples.
The following accessories might be added to your SoxROC system.

Cups
The better thermal conductivity in aluminium makes
it ideal for applications or scenarios when it is
desirable to run the extraction at low temperatures.
Aluminium cups are more durable than glass. Glass
cups in Borosilicate makes visual inspection easy
during the extraction.
The SoxROC has two sizes of cups, 160 ml and
200 ml in both aluminium and glass. The 200 ml is
ideal for Large Sample Volumes (LSV) and the small
cups improve the usage of solvents - saving costs.

Thimbles
You can use the most common thimbles on the
market with the SoxROC. Cellulose thimbles
33x80 mm, 33x94 mm as well as 25x80 mm,
26x60 mm and 25x75 mm will all work well with
the instrument.

Demanding Solvents
The SoxROC instrument is built to withstand most solvents.
However, seals and cup holders might require specific
configuration for certain solvents.
Viton seals are standard but specific PTFE coated seals are
recommended for certain solvents such as Acetone, Ethyl
Acetate and Acetonitrile. The SoxROC filter holder is made
of stainless steel which works well in most applications.
However, for the above solvents, it is instead recommended
to use SoxROC PTFE holders.
Please consult OPSIS LiquidLINE to confirm the best
configuration for your specific applications.
SoxROC Extraction Unit, SX-320-A/SX-360-A
Ordering Information
SX-320-A SoxROC Extraction Unit 2 position including:
2 Viton seals, 2 Filter Holders Ø33 mm, 1 Sample tray, 1 box of Boiling stones, 1
box of Thimbles 33x80 mm, 1 Recovery flask, User guide and aluminium cups
SX-360-A SoxROC Extraction Unit 6 position including:
6 Viton seals, 6 Filter Holders Ø33 mm, 1 Sample tray, 1 box of Boiling stones,
1 box of Thimbles 33x80 mm or 25x80 mm, 1 Recovery flask, Cup stand, User
guide and selection of cups
Cups Ø48 160 ml Aluminium and Borosilicate cups
Ø54 200 ml Aluminium and Borosilicate cups
Thimbles Recommended 25x80 mm and 33x80 mm. Compatible with standard filters and
any length, up to 100 mm, of Ø25/Ø33 mm thimbles
Holders and Seals Viton and PTFE coated seals, Stainless Steel Filter Holders and PTFE Holders
Features and Performance
Sample Positions 6 (SX-360-A), 2 (SX-320-A)
Capacity Samples per day 42 (SX-360-A)
Measuring Range Method 0.1-100% Fat (actual measurement on balance)
Accuracy According to official approvals
Solvent Recovery >90%
Typical Extraction Time Typically 40 to 70 minutes, depending on application
Batch Handling Yes. OPSIS LiquidLINE Innovative Batch System
Fully Automated Yes. Automated Hot Solvent Extraction
Programmable Yes. 6 fully customised programs
Temperature Control Yes. 30-300˚C
Manage Removal of Solvent Yes. Adjustable emptying solvent levels, including leaving solvent at
end of extraction
Adding Solvent during Extraction Yes. Closed solvent addition also during extraction
Removable Recovery Tank Yes. Easy to remove recovery flask located at front of the instrument.
Extraction and Rinsing Time 0-999 minutes, programmable for both steps
Safety Systems
User Protection Protection door monitoring. Automatic door lock and sealing during extraction.
Temperature Protection Two separate safety systems with independent CPU´s, sensors, and heating
control. Automatic setting of over-temperature.
EX Protection ATEX components for internal exposed valves, IP65 for other internal electronics,
Pressurized electronics cabinet. IP55 for liquid and dust protection
Technical Data
Operating Temperature For indoor use only, 5˚C - 40˚C, max 80 % relative humidity
Power Supply 190-240 VAC, 50-60 Hz, 10A
Power Consumption max 600W (SX-320-A), max 1300W (SX-360-A)
Water Consumption 1 l/min at 20˚C
Dimensions (WxHxD) 630 x 520 x 540 mm (SX-360-A), 440 x 520 x 540 mm (SX-320-A)
Weight 63 kg (SX-360-A), 57 kg (SX-320-A)
Specifications subject to change without notice
Opsis AB, Box 244
SE-244 02 Furulund Sweden
Telephone +46 46 72 25 00
Telefax +46 46 72 25 01
E-mail info@opsis.se
www.liquidline.se
LP 1006
2018 02

OPSIS AB • +46 46 72 25 00 • info@opsis.se • www.liquidline.se