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Experiment 7 Data Sheet PDF

This document describes an experiment involving organic derivatives of water, including alcohols (1-butanol, 2-butanol, tert-butyl alcohol) and others (phenol, diisopropyl ether). Various tests were performed to analyze solubility, oxidation, and functional group reactions. Solubility depended on molecular branching and proportions of hydrophilic/hydrophobic bonds. Potassium permanganate and Tollen's tests categorized compounds by oxidation ability. Lucas test differentiated primary, secondary, and tertiary alcohols. Ferric chloride and iodoform tests identified specific functional groups that undergo characteristic reactions. The experiment analyzed physical and chemical properties of organic water derivatives to classify compound structure and re

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Christian Batayen
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346 views5 pages

Experiment 7 Data Sheet PDF

This document describes an experiment involving organic derivatives of water, including alcohols (1-butanol, 2-butanol, tert-butyl alcohol) and others (phenol, diisopropyl ether). Various tests were performed to analyze solubility, oxidation, and functional group reactions. Solubility depended on molecular branching and proportions of hydrophilic/hydrophobic bonds. Potassium permanganate and Tollen's tests categorized compounds by oxidation ability. Lucas test differentiated primary, secondary, and tertiary alcohols. Ferric chloride and iodoform tests identified specific functional groups that undergo characteristic reactions. The experiment analyzed physical and chemical properties of organic water derivatives to classify compound structure and re

Uploaded by

Christian Batayen
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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EXPERIMENT 7

ORGANIC DERIVAT IVES OF WAT ER

Name: ____________________________________ Date: ______________

Group number: _______ Section: ___________

Table 1. Sample Description

DESCRIPTION
SAMPLE
(color, clarity, physical state)

1-butanol

2-butanol

tert-butyl alcohol

phenol

diisopropyl ether

Table 2. Solubility tests

OBSERVATION
SAMPLE
Water +/- NaOH +/- H2SO4 +/-

1-butanol

2-butanol

tert-butyl
alcohol

phenol

diisopropyl
ether

Page 1 of 5 ORGANIC DERIVATIVES OF WATER | Chem 31.1 Department. of Chemistry UP Visayas\


1. For the representative alcohols, explain the solubility behavior in water as a function of branching in
the molecule.

________________________________________________________________________________

________________________________________________________________________________

2. For phenol and ether, explain the solubility behavior in water as a function of the relative proportions
of hydrophilic bonds and hydrophobic bonds in the molecule.

________________________________________________________________________________

________________________________________________________________________________

3. Which among the representative compounds is/are soluble in NaOH? Write the acid-base reactions
involve.

________________________________________________________________________________

Acid-base reaction

4. Enumerate the classes of organic derivatives of water that are soluble in concentrated H2SO4. What
generalization can be made for a substance to be soluble in concentrated H2SO4?

________________________________________________________________________________

________________________________________________________________________________

Table 3. Potassium permanganate test

Description of reagent (hot, acidic KMnO4): ________________________________________________

SAMPLE RESULTS

Before heating After heating +/-

1-butanol

2-butanol

tert-butyl alcohol

phenol

diisopropyl ether

Page 2 of 5 ORGANIC DERIVATIVES OF WATER | Chem 31.1 Department. of Chemistry UP Visayas\


Table 4. Tollen’s test

Description of reagent (ammoniacal AgNO3): ________________________________________________

SAMPLE RESULTS +/-

1-butanol

2-butanol

tert-butyl alcohol

phenol

diisopropyl ether

5. Based on the result of KMnO4 and Tollen’s test, categorize the classes of organic derivatives of
water as to:

Easily oxidizable: _________________________________________________________________

Oxidizable: _______________________________________________________________________

Resistant to oxidation: _____________________________________________________________

Table 5. Lucas test

Description of reagent (HCl-ZnCl2): ________________________________________________

SAMPLE RESULTS +/-

1-butanol

2-butanol

Tert-butanol

phenol

diisopropyl ether

Page 3 of 5 ORGANIC DERIVATIVES OF WATER | Chem 31.1 Department. of Chemistry UP Visayas\


6. Based on the result of KMnO4 and Lucas test on the representative alcohols, give a generalization
on how each class of alcohols can be differentiated:

Primary alcohol: _________________________________________________________________

Secondary alcohol: ________________________________________________________________

Tertiary alcohol: _________________________________________________________________

Table 6. Ferric chloride test

Description of reagent (FeCl3): ________________________________________________

SAMPLE RESULTS +/-

1-butanol

2-butanol

tert-butyl alcohol

phenol

diisopropyl ether

7. What class of organic compound reacts with FeCl 3 solution?

_________________________________________________________________________________

Table 7. Iodoform test

Description of reagent (I2/KI): ________________________________________________

SAMPLE RESULTS +/-

1-butanol

2-butanol

tert-butyl alcohol

Page 4 of 5 ORGANIC DERIVATIVES OF WATER | Chem 31.1 Department. of Chemistry UP Visayas\


phenol

diisopropyl ether

8. What are the structural requirements for an alcohol to react with the iodoform reagent?

_________________________________________________________________________________

Page 5 of 5 ORGANIC DERIVATIVES OF WATER | Chem 31.1 Department. of Chemistry UP Visayas\

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