QUANTACHROME

NOVAe SERIES
®

HIGH-SPEED SURFACE AREA & PORE SIZE ANALYZERS

© 2008 Quantachrome Corporation .&

 The Gas Sorption Process
Industries Served Before performing gas sorption
experiments, solid surfaces must
Particle characterization be freed from contaminants such
technology serves a wide as water and oils. Surface cleaning
(degassing) is most often carried out
variety of industries, by placing a sample of‑the solid in a
including: glass cell and heating it under
vacuum or flowing gas. Figure 1
Aerospace illustrates how a solid particle 1 A section of one greatly
Agriculture containing cracks and orifices (pores) enlarged particle of a
of different sizes and shapes may look solid.
Automotive
after its pretreatment.
Aviation
Batteries Once clean, the sample is brought to
a constant temperature by means of
Building Materials
an external bath. Then, small amounts
Ceramics of a gas (the adsorbate) are admitted
Chemicals in steps into the evacuated sample 2
For laboratory research and development. Communications chamber. Gas molecules that stick to
the surface of the solid (adsorbent) The monolayer
Equipment are said to be adsorbed and tend to of adsorbed
Construction molecules; approxi-
form a thin layer that covers the entire
mately 20% saturation.
Consumer Goods adsorbent surface. Based on the well-
known Brunauer, Emmett and Teller
Cosmetics
(B.E.T.) theory, one can estimate the
Electrical &  number of molecules required to
Electronics cover the adsorbent surface with a
Environmental monolayer of adsorbed molecules, Nm 3
(see Figure 2). Multiplying Nm by the
Services The multilayer/
cross-sectional area of an adsorbate
Foods molecule yields the sample’s ­surface capillary
condensation
Food Processing area.
stage
For industrial QA/QC and analytical services.
Fuel Cells Continued addition of gas molecules approximately
Manufacturing 70% ­saturation.
beyond monolayer formation leads to
Marine the gradual stacking of multiple layers
(or multilayers). The formation occurs
Medical Devices
in parallel to capillary condensation
Metals (see Figure 3). The latter process is
Mining & Minerals appoximated by the Kelvin equation,
Munitions which quantifies the proportionality
between residual (or equilibrium) gas
Oil Exploration
pressure and the size of capillaries
Optics capable of condensing gas within 4
Paints & Coatings them. Total pore volume
Paper & Packaging filling; approximately
Methods such as the classical one by
100% ­saturation.
Petrochemicals Barrett, Joyner and Halenda (B.J.H.) or
Pharmaceuticals the more accurate Density Functional
Theory (DFT) models, allow the
Plastics
computation of pore sizes from
Rubber equilibrium gas pressures. Knowing the density of the adsorbate, one
Textiles Experimental isotherms of adsorbed can calculate the volume it occupies and,
gas volumes relative ­versus pressures consequently, the total pore volume of
Water Treatment
(at equilibrium), are converted to the sample. If at this stage the adsorption
cumulative or differential pore size process is reversed by withdrawing known
­distributions. amounts of gas from the system in steps,
one generates desorption isotherms.
As the equilibrium adsorbate The resulting ­hysteresis leads to isotherm
pressures approach saturation, the shapes that can be ­related to those
pores become completely filled with expected from particular pore‑shapes.
adsorbate (see Figure 4).
NOVA e Series Overview
®

Quantachrome’s patented NOVA e Applications for Quality Control

series offers a full line of high-quality, NOVA 1200e—the “Any Gas” surface and Research
high-performance Surface Area and area and micropore size analyzer.
Pore Size Analyzers, with eight fully • Enhanced single-sample analyzer
automatic models to meet the needs
suitable for a variety of applications.
of any research or quality assurance
laboratory. Carbon for rubber,
• Useable with most non-corrosive
adsorbate gases such as argon, CO2 adsorbents (gas separation
The NOVAe Series—designed for and light hydrocarbons over a wide and water purification), gas
today’s laboratory. range of temperatures. masks, inks, laser printers
• Affordably-priced—perfect for any and copiers.
• Plus all the features of the NOVA
laboratory.
1000e.
• Space saving—each unit takes up Catalysts for the
NOVA 2000e—measures two
less bench space than an open samples simultaneously. automotive, fertilizer, fuel
3-ring binder. • Get all the capabilities of the NOVA cell and petrochemical
• Versatile—a wide range of character‑ 1000e in a two-station instrument. industries.
ization techniques for powdered and • Provides higher laboratory efficiency
porous materials. and productivity. Organic materials for
• Upgradeable—can adapt to meet adhesives, chromatography, Coal ash
• Flexible operation—analysis type
your expanding or changing independent for each station (BET cosmetics, foodstuffs,
laboratory needs. and/or pore size measurement). detergents, explosives,
• PC option—use Windows-based ion exchange resins,
NOVA 2200e—features “Any Gas”
software or run stand-alone. capability for dual-sample analysis. pharma­ceuticals and
NOVA 1000e—rapid single-sample • Combines the qualities of the NOVA ­plastics.
surface area and pore size 1200e and the NOVA 2000e.
analyzer. • Meets the special needs of the busy Minerals such as alumina,
• Perform fully automated multi-point research laboratory. clays, hydroxyapatite,
B.E.T. analysis in as little as eight pigments, phosphates,
NOVA 3000e—measures up to three
minutes. samples simultaneously. silicas, zirconia, etc., used
• Eliminate the need for helium with • Analyze up to three samples at one for abrasives, adsorbents,
patented NO Void Analysis™ (NOVA) time or two plus continuous Po biomaterials, ceramics, Natural zeolite
technology. measurement. cements, desiccants, fillers,
• Analyze up to 200 data points (100 • Save space with four on-board papers and paints.
adsorption points and 100 sample preparation ports.
desorption points). • Plus all the capabilities of the NOVA Powdered metals and
• Prepare two samples by vacuum or 1000e and NOVA 2000e. ferrites for batteries,
flow methods simultaneously with pressure formed/ sintered
NOVA 3200e—features “Any Gas”
sample analysis—at different capability for analysis of up to products, electronics,
temperatures if required. three samples. magnets and magnetic
• Access degasser during analysis to • Combines the qualities of the NOVA tape.
start/stop flow or vacuum degassing 1200e and the NOVA 3000e.
with Analysis Interrupt. NOVA 4000e—maximum through- Other applications related
Carbon black
• Get data "on the fly" by uploading out with four sample stations to bone, composite
data to a PC from current analysis. • Four samples at one time, or three materials, fibers, rigid
plus continuous Po measurement. foams, soil, sludge, slurries,
• Eliminate cell calibration with classi‑
cal helium-void-volume mode. • Four degas ports. suspensions and well cores.

• Transfer data via RS232 or printer • See Nova 1000/2000e for other
port. capabilities.

• Enhance performance with NOVA 4200e—features "Any Gas"

Windows®-compatible software. capability for analysis of up to four
samples.
• Verify performance with rapid • Everything the Nova 4000e can do
calibration check. plus expanded capabilities of using a
wide range of analysis gases.
The NOVA Series produces the results
NOVA e Series
®

you need...
• Single and multi-point B.E.T. surface area with QUALITY CONTROL • RESEARCH
y-intercept, “C” constant, slope and correlation System Status
coefficient. Display
Vacuum or flow
• Up to 100 adsorption and 100 desorption degassing Coolant
isotherm points. Level
Heating Sensor
• B.J.H. pore size distribution calculated from mantles
the adsorption or desorption isotherm.

• Total pore volume.

• Average pore radius.

...and with optional NovaWin software 1, 2, 3 or 4

samples
• Dubinin-Radushkevich micropore area, average
micropore width and adsorption energy.

• Langmuir surface area with slope, intercept,

constant and correlation coefficient.

• Plot of single-point B.E.T. surface area as a

function of relative pressure. RS232 port
for optional
• t-method for micropore area and volume Degas PC control
(Halsey, deBoer and carbon black methods). temperature via NOVAWin
controls software
• Density Functional Theory calculations for unified
micropore and mesopore size distributions.
Status and
Critical components of highest quality data display
to ensure reliable results
• High-sensitivity pressure transducer with Automated
excellent stability. Analysis selection dewar elevator
keypad
• High-resolution 16-bit A/D converter.

• Robust dewar elevator for years of Feature highlights of the NOVAe Series
trouble-free operation.
NOVA NOVA NOVA NOVA NOVA NOVA NOVA NOVA
• Filter gaskets to prevent vacuum system Functional Capability by Model
1000e 1200e 2000e 2200e 3000e 3200e 4000e 4200e
contamination by powdered samples.
Surface area analysis        
• Reliable solenoid valves and leak-free        
(10-9 cc/sec) dosing manifold. Mesopore size distribution  
 
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

Standard micropore methods 
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 
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
• Sensitive RTD coolant level sensor
Analysis stations 1 1 2 2 3 3 4 4
Accurate results require
proper sample preparation “Any Gas” capability —  —  —  — 

• Each station provides sample

preparation under vacuum or flow conditions.

• Backfill after vacuum degas with helium or

adsorptive.

• Temperature range from ambient to 450ºC*

ACCESSORIES
with independent selection.
Gas Regulator Assembly
• Flow rate selection for each station.
Proper Nova functioning is assured when high-quality gas regulators are used.
• Optional, multi-station degassing units for Quantachrome supplies complete assemblies which include two-stage regulators with
busy laboratories: MasterPrep, FloVac dual gauges, cylinder connector, isolation valve and 1/8" gas line connector. The regulators
and Flow Degassers. feature stainless steel, non-venting diaphragms and the appropriate CGA fitting for specific
gases. Different assemblies are available for nitrogen (and other inerts including helium),
hydrogen, carbon monoxide, oxidizing gases etc.
* 350ºC standard with mantles supplied;
450ºC with optional quartz heating mantles Rotary Micro Riffler
Like most powder and porous materials characterization, surface area and pore size studies
generally require sub-samples much smaller than the original samples. The Rotary Micro
Riffler uses the most accurate way of splitting a powder sample into smaller fractions- spin
riffling. The vibrating hopper features adjustable feed rate and the variable-speed collector
uses standard or micro test tubes.
NOVA e Series Benefits
®
NOVAWin™ - Windows® Based Software
Operational conveniences Revolutionary ease-of-use, for Operation from PC
speed, and accuracy NOVAWin™ is a PC based • PC based initialization and
• Simultaneous analysis of up
to four samples with NOVA program for operation of the control of NOVA analysis.
• Patented NO Void Analysis™ NOVA series of instruments
4000/4200e for dramatic • View isotherms in “real-time”
(NOVA) technology eliminates utilizing the familiar features
increase in productivity.
helium, reducing analysis costs. during analysis.
of the Microsoft® Windows®
• Degas up to four samples
• Alternatively, use classical helium- operating system. NOVA • Store analysis configurations
while analysis is in progress
void-volume mode to match your operators will find this to be for fast recall.
for maximum throughput.
existing SOPs. a user-friendly, graphical
• Automatic analysis, compu- environment to work in. • Compatible with virtually any
• RTD coolant level sensor for printer via Windows® operating
tation, display and printing
constant void volume and high
of results. NOVAWin™ incorporates system.
accuracy as coolant evaporates.
• Keyboard selection from Quantachrome Instruments’ • Zoom into any part of a graph
• MaxiDose™ algorithm
unlimited number of analysis many years of experience in and perform a linear best fit for
reduces analysis time without
types offers fast run initialization. particle analysis through the any set of data points.
compromising accuracy.
• Wide variety of sample cells to
inclusion of our extensive
• Low surface area capabilities with methods of data reduction
accommodate any sample.
compensation for adsorption on and report generation in this
• Compact, benchtop design to cell walls. versatile software package.
conserve valuable lab space.
• Access degasser during an analy‑
• Protective doors for safety. sis to start/stop flow or vacuum 21 CFR Part 11 compliant version available.
degassing with Analysis Interrupt.
Meets technical demands
• Get data "on the fly" by upload‑
• Full equilibration technology ing data to a PC from the current
with choice of pressure analysis with Nova Software.
tolerance, equilibration time and
relative pressure (P/Po) points. Output capabilities
• Multiple Po options for speed and • Front panel display of results
accuracy: user entered, calculated upon completion of analysis.
from ambient, measured once, or
continuously updated throughout • Automatic report generation on
analysis (NOVA 2000e through optional printer.
Nova 4200e). • Communication with PC for analy‑
• Upgrades easily as your needs sis set up, data acquisition and
expand; analysis stations can be reporting.
added up to a maximum of 4.
Analysis Presets
• Built-in microprocessor guided
calibration for optimum • Allows the user to establish
performance consistent with predefined analysis protocols.
ISO-9000 requirements. Choose from many methods of data reduction.
• Speed up operation by reducing
• Manual mode diagnostics for entries needed to start each run.
performance verification and
maintenance. System Manager • Adsorption and desorption • Mesopore size distribution by
isotherms (linear and logarith‑ BJH method
• Real-time display of analysis • Exclusive control of key settings
mic scales)
status for instant user update such as RS232 settings, critical • Mesopore size distribution by
of analysis progress. operation parameters, isotherm • BET surface area DH method
measurement, or operation
• Calibration verification is fast. restrictions. • Langmuir surface area • Micropore size distribution by
Calibration performed in just a MP method
few minutes. • Micropore volume and surface
area by t-plot method (Halsey, • Density functional theory for
deBoer or carbon STSA unified micropore and meso‑
equations) pore size distribution includ‑
ing library of adsorbates and
• Dubinin Radushkevich micro‑
adsorbent pairs, eg. argon on
pore surface area
zeolite, nitrogen on silica, CO2
• Dubinin Astakhov micropore on carbon, etc.
area and size distribution
• Fractal dimension by NK and
FHH methods.
SPECIFICATIONS NOVA
1000e
NOVA
1200e
NOVA
2000e
NOVA
2200e
NOVA
3000e
NOVA
3200e
NOVA
4000e
NOVA
4200e
Performance
Analysis stations 1 2 3 4
Measurement types: B.E.T., STSA, adsorption isotherm, desorption isotherm
Surface area range: 0.01m2/g to no known upper limit
Pore size range: 0.35 to >400nm (3.5 to >4000 Å)
Minimum pore volume: (liquid) 2.2 x 10-6 ml/g
Minimum pore volume: (STP) 0.0001 cc/g

Adsorbates
Nitrogen P P P P P P P P
Other non-corrosive gases (Ar, CO2, H2, C4H10, etc.) __ P __ P __ P __ P
Degassing
Preparation Ports 2 4
Methods Vacuum and Flow
Temperature range: ambient - 450ºC*, 1ºC intervals
Accuracy ±5ºC

Pressure Transducers
Accuracy (% of span) ±0.1
Minimum pressure (mm Hg) resolution 0.016
Minimum relative pressure P/Po (N2) resolution
2 x 10-5
Physical
Dimensions (WxDxH) 51 cm x 51 cm x 79 cm
Weight 36.29 kg (80 lbs.)
Electrical 100-240 V, 50/60 Hz *450ºC with optional quartz heating mantles.

Additional Degassing Options

Sample Preparation control valves to allow the addi‑ insertion into any sample cell.
tion or removal of individual Cooling stations are provided to
Consistent and reliable surface sample cells without interrupt‑ hold sample cells after sample
area results depend upon proper ing the other samples in process. preparation.
sample preparation procedures. A built-in heater provides user-
selectable degas temperature to These degassers provide a virtual‑
In terms of B.E.T. analysis, the 400ºC, in steps of 1ºC, monitored ly continuous supply of properly
limiting step in rate of through‑ continuously on the digital display. prepared samples for the NOVAe
put is often sample preparation. series of surface area and pore
The complete degassing of The MasterPrep features size analyzers.
samples can often require several individual temperature program‑
hours, while surface measure‑ ing for each of the six sample
ments may require as little as 8 stations, from the build-in key‑
minutes. pad or by PC software (PC not
included). In vacuum mode, the
The NOVAe Series features MasterPrep's and FloVac’s select‑
built-in vacuum or flow sample The MasterPrep Degasser set up
for vacuum degassing
able evacuation rates and back-fill
preparation ports that permit gases add convenience and
the simultaneous degassing of versatility. A selection of fittings
samples while measurements augment the NOVA’s sample
are provided to accommodate
are in progress. preparation facilities: the
short and tall glassware as well as
MasterPrep and the FloVac
three different diameter stems.
Degasser for combined flow
The Masterprep, FloVac & and vacuum degassing, and the
In flow mode, all units’ needle
Flow Degasser offering the flow
Flow Degassers method only.
valves allow careful control of
flow rate to avoid elutriation
For additional flow and vacuum (blowing out) of fine powders.
degassing, Quantachrome offers Each device features six sample
The metal flow tubes for each The Flow Degasser for flow
three valuable complements to stations, each with individual degassing of up to six samples
station provide variable depth
Services
Application Laboratory
Fee-basis analytical service for a wide range of physical properties: surface area,
micropore and mesopores characterization by gas sorption, meso and macropore
measurements by mercury intrusion porosimetry, density by gas pycnometry,
bulk and tapped powder density, water sorption isotherms, catalyst characterization
using reactive gas sorption, TPR/TPD/TPO etc. Staffed by experts; data interpretation
by top scientists in their fields, often at no additional charge.

Operator Training Courses

Many users benefit from detailed training classes focusing on instrument operation,
report generation and interpretation of results. Get the most out of your investment/
equipment budget. Learn about latest advancements in measurement techniques.
Try out the latest software versions, taught by our specialists. Classes are held at
Quantachrome's headquarters in Boynton Beach, Florida throughout the year. Fully
customized classes are available at client's home facility.

Knowledge Transfer Program

Two-day classroom style educational courses. You do not have to be a Quantachrome
customer to benefit. Covers theory, application, and results interpretation for the field
of porous materials characterization. Courses are customized and presented at your
own facility to an unlimited number of attendees.

Service Plans
Every Quantachrome instrument comes with at least a full 12-month warranty. Larger
instruments are installed by an expert technician - at no extra charge. To ensure
trouble free operation in the years to come, our Service Department offers a variety of
maintenance and service contract options. Our service technicians are factory trained
and teach instrument operation plus routine maintenance skills to operators. Refers to
USA only. Outside USA, contact your local Quantachrome representative for their offerings.
Factory warranty valid worldwide.

Technical Support
• Application Notes: Any or all of our comprehensive listing of notes is available
on request. Notes library is continually expanded to feature breakthrough
developments in porous materials characterization. Our science staff will assist
users with applications for which a note does not already exist.

• Newsletter: Quantachrome publishes “Porous Materials Highlights”, available

electronically. Features application articles, news, events, people and more.

Contributions from users are always welcome.

• Website www.quantachrome.com: Provides detailed instrument specifications

and brochures, events calendar, course schedules and special announcements.
Ask questions to our experts through our feedback form.
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Quantachrome is also recognized as JAPAN

an excellent resource for authoritative Quantachrome Instruments Japan G.K.
analysis of your samples in our fully
equipped, state-of-the-art powder KSP W311 Sakado 3-2-1, Takatsu-ku
characterization laboratory. Kawasaki-shi, Kanagawa 213-0012 Serving Porous
Japan Materials and Powder
Phone: +81 44 829 1525 Characterization
Fax: + 81 44 829 1527 Needs Since 1968
www.quantachrome.co.jp
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Quantachrome Instruments Application Laboratory. in accordance with ISO9001:2008.

Our policy of continuous development may cause the information and specifications contained herein to change without notice or liability. © 2012-2013 Quantachrome Corporation 0313