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Answer The Following Questions

This document is the question paper for an 8th semester pharmacy examination on Advanced Pharmaceutical Analysis. It contains 8 questions testing students' knowledge of various analytical techniques and procedures. The questions cover topics like Bragg's equation, paramagnetic substances, X-ray diffraction, partition coefficients, size exclusion chromatography, X-ray fluorescence spectroscopy, differential thermal analysis, condensation reactions, and procedures for qualitative and quantitative analysis of drugs like atenolol, propranolol, ampicillin, and rifampicin. Students are required to answer 1 compulsory question with 10 short questions and any 5 questions out of the remaining 7.

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Ankita Upadhyay
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432 views2 pages

Answer The Following Questions

This document is the question paper for an 8th semester pharmacy examination on Advanced Pharmaceutical Analysis. It contains 8 questions testing students' knowledge of various analytical techniques and procedures. The questions cover topics like Bragg's equation, paramagnetic substances, X-ray diffraction, partition coefficients, size exclusion chromatography, X-ray fluorescence spectroscopy, differential thermal analysis, condensation reactions, and procedures for qualitative and quantitative analysis of drugs like atenolol, propranolol, ampicillin, and rifampicin. Students are required to answer 1 compulsory question with 10 short questions and any 5 questions out of the remaining 7.

Uploaded by

Ankita Upadhyay
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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Registration no:

Total Number of Pages: 02 B.Pharm


PH.E.9(PH.8.6)

8th Semester Regular / Back Examination 2015-16


ADVANCED PHARMACEUTICAL ANALYSIS
BRANCH: Pharmacy
Time: 3 Hours
Max Marks: 70
Q.CODE: W352
Answer Question No.1 which is compulsory and any five from the rest.
The figures in the right hand margin indicate marks.

Q1 Answer the following questions: (2 x 10)


a) What is Bragg’s equation.
b) What is Lande’s splitting factor.
c) What do you mean by stable and unstable paramagnetic substances.
d) What do you mean by K lines and L lines?
e) Write the analytical methods for paracetamol.
f) Write the procedure involved in riboflavin tablet.
g) What is meant by condensation reaction?
h) Write notes on Folin’s reagent.
i) Write analytical procedure of chloropheneramine maleate.
j) What is partition or distribution co-efficient?

Q2 a) What are X-ray diffraction methods are used for investigation of the (5)
internal structure.
b) Write the procedure and principle using PDAC as analytical reagent for (5)
the estimation of drugs.

Q3 a) Write briefly on scintillation counter. (5)


b) Explain diazotization followed by coupling. (5)

Q4 Describe size exclusion chromatography. (10)

Q5 a) Mention the principle and methods of X-ray fluorescence spectroscopy. (5)


b) Write the instrumentation and application of DSC. (5)

Q6 a) Draw a schematic diagram of a typical DTA apparatus mention the (5)


factors that affecting DTA curve.
b) By using Gibb’s reagent write the procedure and principle for the (5)
estimation of drugs.
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Q7 a) Write the principle and procedure of condensation reaction using the (5)
reagent PDAB.
b) Describe in detail about SCFC. (5)

Q8 Write the procedure involved in the qualitative and quantitative analysis (5 x 2)


of following drugs ( attempt any two)
a) Atenolol and propranolol hydrochloride.
b) Ampicillin and rifampicin
c) Folic acid and nicotinamide
d) Sulphacetamide and sulphamethoxazole

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