Stone Testing: An Excerpt From The Dimension Stone Design Manual, Version VIII (May 2016)
Stone Testing: An Excerpt From The Dimension Stone Design Manual, Version VIII (May 2016)
© 2016
All rights reserved. No part of this document may be reproduced or transmitted in any form or by means
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system, without written permission from the Natural Stone Institute.
Stone Testing slicing the stone thin with an ultraprecision,
thin-blade diamond saw. The stone slice on a
slide is then precision-ground to a precise
1.0 INTRODUCTION thickness of about 20 to 30 microns. At that
thickness most minerals, regardless of color,
1.1 General. Testing evaluates the are translucent and can be studied under a
suitability of a specific stone for a particular microscope. In this way minerals can be
application. The strength of the stone is tested identified, the crystal or fragment boundaries
to determine its resistance to crushing and can be evaluated, and incipient microfractures
bending. The density, or specific gravity, is can be seen, as can any chemical degradation
tested to design a support system capable of that may weaken stone, permit water entry, or
carrying the weight of the stone. The amount allow unanticipated breakup.
of water the stone will absorb (absorption rate)
will help determine the resistance of the stone 1.3.2 Exact identification of the minerals by
to staining and freezing. The stone’s wear thin section is a subjective, experience-based
resistance and slip resistance are crucial in skill and is largely being replaced by exact
flooring applications. methods of chemical analysis. Having both the
thin section and chemical analysis is the
1.2 ASTM tests, many of which are preferred procedure, as the physical features
conducted within engineering parameters, do can be seen documented on known mineral
not include petrographic and other geologic crystals or grains.
tests useful to evaluating stone behavior
through time in adverse environmental 1.4 X-ray diffraction (XRD) analysis is
settings. If and when a failure occurs, questions one of the tried-and-true analytical techniques
about what went wrong and why are asked; used for decades in petrology and remains the
however, test data reviewed frequently may preferred technique in certain situations.
not reveal information useful to answer these However, more modern analytical techniques
questions. Stone behavior is directly related to have evolved that are far more precise, analyze
the behavior of the mineral or minerals that
far more compounds and elements, and are
make up the stone. Knowing something about rapidly replacing XRD for most routine
physical and chemical characteristics of the purposes.
common minerals found in stone can be very
useful in understanding its behavior. 1.5 Lithogeochemistry, the chemical
analysis of stone, relies on many new
1.3 Petrography is the science of procedures too numerous to attempt
description and classification of rocks. A explanation here. The following are just a few
petrograpic analysis can be arranged through notable lithogeochemical analysis procedures:
most construction material laboratories. A
comprehensive petrographic analysis will often 1.5.1 Instrumental Neutron Activation
suffice to answer many behavioral questions. Analysis (INAA)
Other, more sophisticated analyses performed
in well-equipped chemical laboratories to 1.5.2 Atomic Absorption Spectroscopy (AA)
determine exact chemical and trace element
content can also be useful. 1.5.3 Inductively Coupled Plasma Emission
Spectroscopy (ICP-OES)
1.3.1 Perhaps the most common and time-
tested petrologic studies use thin sections of 1.5.4 X-ray Fluorescence Spectroscopy (XFS)
stone. These are prepared by polishing small
samples very flat, gluing them to glass
microscope slides (1" x 3" to 2" x 3"), and
2.0 ASTM STANDARD TEST 2.3.1 These specifications are the standard
METHODS AND methods for determining the characteristics of
building stone needed for proper design for a
SPECIFICATIONS
particular application. They should be
performed with care and the results used with
2.1 ASTM International, formerly
an understanding of their intent and
known as the American Society for Testing and
limitations. An independent testing laboratory
Materials, has developed several standard test
properly equipped and capable of performing
methods to evaluate stone characteristics so
the tests should perform all tests. Stone
that stones can be compared on a uniform basis.
Producers or Distributors, Associations, and
The Marble Institute of America recommends
other Promotional Organizations may publish
ASTM methods and standards for dimension
typical test values. While these values can serve
stone as guidelines for specification and
as a guide, current tests should be conducted
installation. ASTM International is the world’s
on the actual stone to be used for a particular
largest voluntary standards development
project.
organization. Note that stone testing according
to European methods and conditions may use
2.4 Review for Suitability. ASTM test
different procedures that give different results
results for various stones are guidelines and
than do ASTM methods for the same stone.
information on the stone characteristics. In
This is particularly true of tests for abrasion
many cases, an Engineer should be employed
(wear). The ASTM Standard Test Methods are
to review the results of the test data and
listed in Chapter 2.
compare with actual installation methods to
determine if the stone is suitable for the
2.2 Current Standards. ASTM standards
application in the specified thickness suggested,
are revised from time to time. A revised
and if not, what changes should be employed to
version is indicated with a hyphen followed by
make the stone work as intended for the job in
a two-digit number after the basic designation
question. Evaluation and/or testing of
of the standard, e.g., ASTM C119-11, showing
compatibility of grouts, sealers, setting
that it was revised in 2011. An additional
methods, and anchoring must be performed
number in parentheses, e.g., ASTM C97-
along with the stone.
92(1994), indicates that the 1992 edition was
5.9.3 The stones are abraded using a machine 5.10.2 The second concern is the abrasive.
developed by Kessler. The machine includes a ASTM C97 specifies a particular abrasive that
horizontal, round, cast iron “lap” about 9" in is no longer being produced. The ASTM
diameter, which rotates at a speed of 45 committee is currently conducting round-
revolutions per minute (rpm). The specimens robin tests among different laboratories to
are mounted in a holder that rotates in the same determine a possible correction factor or a
direction as the lap, but at a different speed. different test method which will produce
While the lap and the specimen rotate, an abrasion index numbers that are the same as
abrasive flows onto the lap to abrade the from the methods of ASTM C241, so that new
bottom of the specimens. Each specimen test results can be compared with earlier
supports a load of 2,000 grams, which includes results. In the meantime, test laboratories have
the weight of the specimen holder, but not the had to develop a correction factor by
specimen itself. comparing the results for stones having
different abrasion resistances, e.g., soft and
5.9.4 For the test, the stones are dried for medium marble and granite, using the old and
48 hours and weighed. The specimens are then currently available abrasives.
abraded in the Kessler machine for 5 minutes
(225 revolutions at 45 rpm), dusted off, and