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Requisition Form For Xps Measurements Central Research Facility, IIT Kharagpur-721302

1. This document is a requisition form for XPS measurements at the Central Research Facility of IIT Kharagpur. 2. It requires users to provide details about their sample, including its composition and preparation method. A reference mentioning similar XPS results must also be provided. 3. Users must submit the form and pay applicable charges depending on their affiliation before being allotted a time slot for XPS analysis.

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138 views3 pages

Requisition Form For Xps Measurements Central Research Facility, IIT Kharagpur-721302

1. This document is a requisition form for XPS measurements at the Central Research Facility of IIT Kharagpur. 2. It requires users to provide details about their sample, including its composition and preparation method. A reference mentioning similar XPS results must also be provided. 3. Users must submit the form and pay applicable charges depending on their affiliation before being allotted a time slot for XPS analysis.

Uploaded by

deepakmitr
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as PDF, TXT or read online on Scribd
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REQUISITION FORM FOR XPS MEASUREMENTS

Central Research Facility, IIT Kharagpur-721302


No.: Date of submission:
IMPORTANT NOTES:
i. The form must be filled in completely and properly. Otherwise, it will be cancelled.
ii. Samples which can degas in ultra-high vacuum will strictly not be allowed. Sample(s) should not contain
radioactive isotopes.
iii. The sample composition and how it is prepared must positively be mentioned in section 2.
iv. A peer-reviewed reference mentioning XPS result(s) on similar sample(s) must also be provided for
guidance.
v. Any false justification about sample history will disqualify the person for the next 2 months.
vi. Samples need to be submitted two days before the XPS slot date.

1. User’s Profile
Name: _Designation: _ Tel. / Mob. No.: _
Roll No. / EC: Department / Centre:

Name of the Institute / College / Industry:-_ _

2. Sample Details
Metal/Alloy Oxide and its Compound Polymer and Rubber$ Ceramic and Advanced Materials
$
Please be informed that polymer and rubber samples will be measured at low
temperatures (120 K) necessarily in order to avoid any chemical breakdown of the sample
and any slow physical damage to the instrument.
Sample Composition/Formula/Structure:
_________________ Solid (bulk) Pellet Thin Film Powder*
Form (please tick):
*Convert powders into hard pellets and evacuate it in a desiccator for the XPS measurements. Otherwise,
the decision for XPS on the powder itself will be taken by the authorities.
Number of samples (2 samples per slot for XPS spectra): Page

Method of Preparation in detail (submit on a separate sheet): Attached? YES NO


Reference (hard copy attached): Journal _ Volume

Any other detail:

3. Desired Options (please tick)


a. Surface cleaning by sputtering: YES NO
b. Mode: Surface Survey

c. Element-specific Scan:
YES Elements: NO

d. Any specific feature expected? Please write.

ǂ
Signature of the user e-mail (write clearly):
Date:

Signature of the Supervisor (for Students/RS/Project Staff)


Name of the supervisor (in CAPITAL LETTERS)
N.B.:
1. Users from IITKGP: Submit a hard copy of the form, along with the literature reference, in the XPS lab (CRF
Old Building, Ground Floor, Room No. 6).
Outsiders: Send the completed form and the literature reference in a zipped format to xpscrfiitkgp@gmail.com.
2. The sample(s) must be handed over to the lab two days before the measurement schedule. Otherwise, the form will
be cancelled.
3. Please ensure that the samples are ultra-high vacuum compatible. Otherwise, the measurements will be
abandoned.
4. Please collect the sample and data (bring a new CD) on the next working day after the measurement. USB drive
are not allowed.
ǂ
5. The user will be informed about the date and time of experiment via e-mail. Please state whether you would
like to be present in the lab during the measurement.
*
Next requisition will be accepted only after the current measurement is done.

Amount(s) to be paid:

CHARGES DURATION AMOUNT IN INR (Survey Scan)


Internal (institute) 1 slot (1 hour) 500/-
Internal (project) 1 slot (1 hour) 2500/-
External users (academic/R & D) 1 slot (1 hour) 2500/-
Industry 1 slot (hour) 5000/-
Samples from abroad 1 slot (hour) 100 USD
Declaration
INTERNAL

Please transfer an amount of ₹ _ from the Operating Grant of the Department / Centre, account no. ----
--------------------------- in SRIC Account No. 95562010000805. Slots will be provided once the proof of fund transfer is
provided.

Dy. Registrar (F&A) HoD / HoC


(with date and seal)

PROJECT
Please transfer an amount of ₹ _ from the sponsored / consultancy project code to the SEMC
account in SRIC. Slots will be provided once the proof of fund transfer is provided.

Principal Investigator
Asst. Registrar (SRIC) (with date and seal)

EXTERNAL
I agree to transfer the required amount to Account No. 95562010000805, IFSC Code: CNRB0019556.
Name of account holders :- SRIC,IIT KHARAGPUR OR
*
I agree to pay the required amount to The Dean, SRIC, IIT Kharagpur for the above work through the demand
draft/cheque number dated .
Signature of the user (outsider)
Declaration by the user

The results recorded will acknowledge “the XPS facility at the Central Research Facility, IIT Kharagpur”, if
communicated for publication. A copy of the publication will be submitted to the XPS Lab through e-mail to
xpscrfiitkgp@gmail.com.
Any special recognition (award, journal cover-page, special citation) of the results will be reported and a copy
of the reprint/photograph/award will be submitted to the XPS Lab for internal documentation

Slot allotted date:-


Signature of the user
To be filled up at the XPS Laboratory

Please allot time and complete the work.


In-Charge XPS Laboratory

Name of the Operator:

Designation

Vacuum check status:

Date of Measurement:

Signature of the Operator

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