International University, Vietnam National University - HCMC 1

CHEMISTRY LABORATORY

REPORT
EXPERIMENT 1: CHEMICAL REACTIONS

Group: ______________ Section: _____1_________ Date: ____________

Group members:

Seq. Full name Student ID % contribution Signature Score

(total = 100%)
1

Total score: _______/15__

Present well: 1 point

Clear picture: 1 point

Total = 15 points

The report must be typed and handed in together with the signed data sheet by the deadline
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I. Introduction (1pt)
(Introduce what experiments you do in this report)

II. Experimental (1pt)

(Describe what experiments you did in this report, write down each step of your
experiments)

III. Results and discussion

1. Reactions of Cu2+

Reaction Observation Chemical Equation

0.5M CuSO4 (0.25 pts)

+ 2M NaOH

0.5M CuSO4 (0.25 pts)

+ 2M NH4OH

Comments: (0.25 pts)

2. Reactions of silver halides

Reaction Observation Chemical Equation

0.5M KCl (0.5 pts)

+ 0.1M AgNO3

0.5M KCl (0.5 pts)

+ 0.1M AgNO3

+ 2M NH4OH

0.5M KBr (0.5 pts)

+ 0.1M AgNO3

0.5M KBr (0.5 pts)

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+ 0.1M AgNO3

+ 2M NH4OH

Comments: (0.25 pts)

3. Reactions of H2O2

Reaction Observation Chemical Equation

0.1M KMnO4 (0.25 pts)

+ 2M H2SO4

+ H2O2

0.1M KI (0.25 pts)

+ 2M H2SO4

+ H2O2

H2O2 (0.25 pts)

+ MnO2

Comments: (0.25 pts)

4. Reactions of KMnO4

Reaction Observation Chemical Equation

0.5M Na2SO3 (0.5 pts)

+ 2M H2SO4

+ 0.1M KMnO4

0.5M Na2SO3 (0.5 pts)

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+ 6M NaOH

+ 0.1M KMnO4

0.5M Na2SO3 (0.5 pts)

+ H2O

+ 0.1M KMnO4

Comments: (0.25 pts)

5. A. Reactions of Fe3+

Reaction Observation Chemical Equation

0.5M FeCl3 (0.25 pts)

+ 2M KOH

0.5M FeCl3 (0.25 pts)

+ 2M NH4OH

Comments: (0.25 pts)

5. B. Reactions of Fe2+

Reaction Observation Chemical Equation

0.5M FeSO4 (0.25 pts)
+ 2M KOH

0.5M FeSO4 (0.25 pts)

+ 2M NH4OH

Comments: (0.25 pts)

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6. Reactions of Al3+

Reaction Observation Chemical Equation

0.5M Al2(SO4)3 (0.5 pts)

+ 2M NaOH

0.5M Al2(SO4)3 (0.5 pts)

+ 2M NaOH

+ 2M HCl

0.5M Al2(SO4)3 (0.5 pts)

+ 2M NaOH

+ 2M NaOH

Comments: (0.25 pts)

7. Flame test (0.75 pt)

Solution Dominant flame Wavelength Frequency Photon energy

color (nm) (s1) (J)
LiCl

NaCl

KCl

CaCl2

BaCl2

Note: 0.15 pts for the calculation of each chemical

Comments: (0.25 pts)

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IV. Conclusions (1 pt)

(conclude all your performance in this report)

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REPORT
EXPERIMENT 2: pH AND BUFFERS

Group: _____________ Section: _______2_______ Date: ____________

Group members:

Seq. Full name Student ID % contribution Signature Score

(total = 100%)
1

Total score: ________/15__

Present well: 1 point

Clear picture: 1 point

Total = 15 points

The report must be typed and handed in together with the signed data sheet by the deadline
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CHEMISTRY LABORATORY

I. Introduction (1 pt)
(Introduce what experiments you do in this report)

II. Experimental (1 pt)

(Describe what experiments you did in this report, write down each step of your
experiments)

III. Results and discussion

1. pH OF DEIONIZED WATER

Observed pH
Time
1st 2nd Explanation
(second)
(Group___) (Group___)
0 (2 pts)
20
40
60
80
100
120
140
160

Comments: (0.5 pts)

2. pH OF STRONG ACID

Measured pH
Theoretical
Solution Comments/ Explanation
pH 1st 2nd
(Group___) (Group____)
(1 pt)
10 mL of 0.1M HCl

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Add 90 mL of distilled
water

Add 10 mL of
0.1M NaOH

Add 90 mL of
0.01M NaOH
Comments: (0.5 pts)

3. pH OF WEAK ACID

Measured pH
Solution 1st 2nd Ka Comments/ Explanation
(Group___) (Group____)
(1 pt)
0.1M acetic acid

0.01M acetic acid

0.001M acetic acid

Comments: (0.5 pts)

4. pH OF SALTS

Measured pH Explanation
Predicted
Solution 1st 2nd
pH
(Group____) (Group____)
(1 pt)
0.1M NaCl

0.1M CH3COONa

0.1M NH4Cl

Comments: (0.5 pts)

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CHEMISTRY LABORATORY

5. pH OF BUFFERS (3 pts)

Volume (mL) Volume (mL) Measured pH

Calculated
Buffer 0.1M 0.1M Acid Base
pH 1st 2nd
CH3COOH CH3COONa
(Group__) (Group__)

A 10.0 40.0

B 40.0 10.0
Calculation pH: (0.5 pts)
Comments: (0.5 pts)

 Part I: Addition of 10 drops 0.1 M HCl

pH after Total volume HCl (drops)

pH from the
Buffer adding 10 to change pH by one unit Comments/ Explanation
start, pHo
drops HCl (pHo-1)

A (0.5 pts)

C
Comments: (0.5 pts)

`
 Part II: Addition of 10 drops 0.1 M NaOH

pH after Total volume NaOH

pH from the
Buffer adding 10 (drops) to change pH by Comments/ Explanation
start, pHo
drops NaOH one unit (pHo+1)

A (0.5 pts)

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C
Comments: (0.5 pts)

IV. Conclusions (1 pt)

(conclude all your performance in this report)

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REPORT
EXPERIMENT 3: REDOX TITRATION

Group: _____________ Section: ______3________ Date: ____________

Group members:

Seq. Full name Student ID % contribution Signature Score

(total = 100%)
1

Total score:________/15__

Present well: 1 point

Well reading burettes (accuracy) + Clear picture: 2 points

Total = 15 points

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 International University, Vietnam National University - HCMC 13
CHEMISTRY LABORATORY

I. Introduction (1 pt)
(Introduce what experiments you do in this report)

II. Experimental (1 pt)

(Describe what experiments you did in this report, write down each step of your
experiments)

III. Results and discussion

1. TITRATION OF KMnO4 SOLUTION WITH STANDARD H2C2O4 SOLUTION (3 pts)

Calculation: (1.5 pts)

Normality of the standard H2C2O4 solution, N(H2C2O4) = ___________________

Volume of the standard H2C2O4 solution used, V(H2C2O4) = ___________________

Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of KMnO4 (N)

1 -

2 -

Average Normality of KMnO4 = ____________ ( )

Comment: (1.5 pts)

2. TITRATION OF UNKNOWN CONCENTRATION H2C2O4 SOLUTION WITH STANDARD

KMnO4 SOLUTION

Calculation: (1.5 pts)

Normality of the standard KMnO4 solution, N(KMnO4) = ___________________

Volume of the unknown H2C2O4 solution used, V(H2C2O4) = ___________________

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CHEMISTRY LABORATORY

Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of H2C2O4 (N)

1 -

2 -

Average Normality of H2C2O4 =_______ ( )

Comment: (1.5 pts)

3. TITRATION OF UNKNOWN CONCENTRATION FeSO4 SOLUTION WITH STANDARD

KMnO4 SOLUTION

Calculation: (1.5 pts)

Normality of the standard KMnO4 solution, N(KMnO4) =___________________

Volume of the unknown FeSO4 solution used, V(FeSO4)= ___________________

Trial # Burette reading(mL) Volume of KMnO4 (mL) Normality of FeSO4(N)

1 -

2 -

Average Normality of FeSO4 =_______ ( )

Comment: (1.5 pts)

IV. Conclusions (1 pt)

(conclude all your performance in this report)

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 International University, Vietnam National University - HCMC 15
CHEMISTRY LABORATORY

REPORT
EXPERIMENT 4: CHEMICAL EQUILIBRIUM

Group: _____________ Section: ______4________ Date: ____________

Group members:

Seq. Full name Student ID % contribution Signature Score

(total = 100%)
1

Total score: ________/15__

Present well: 1 point

Clear picture: 1 point

Total = 15 points

I. Introduction (1 pt)
(Introduce what experiments you do in this report)

II. Experimental (1 pt)

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CHEMISTRY LABORATORY

(Describe what experiments you did in this report, write down each step of your
experiments)

III. Results and discussion

1. ACID/BASE EQUILIBRIA

Equilibrium System: 2CrO42 + 2H+(aq) ⇌ Cr2O72 + H2O(l)

Description of Predicted Observation Explanation

conditions outcome

(0.5 pts)

Initial solution

(0.5 pts)

+ Conc. HCl

(0.5 pts)

+ 6 N NaOH

Comment: (0.75 pts)

2. EQUILIBRIA OF ACID/BASE INDICATORS

Equilibrium System: H(MV)(aq) + H2O(l) ⇌ H3O+(aq) + MV(aq)

Addition Predicted Observation Explanation

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CHEMISTRY LABORATORY

outcome

(0.5 pts)

None (control)

(0.5 pts)

6 M HCl

(0.5 pts)

6 M NaOH

(0.5 pts)

6 M HCl

Comment: (0.75 pts)

3. EQUILIBRIA OF PRECIPITATION REACTIONS

Equilibrium System: Ca2+(aq) + C2O42(aq) ⇌ CaC2O4(s)

Predicted
Addition Observation Explanation
outcome

Test tube 1: (0.5 pts)

0.1 M Na2C2O4

Test tube 2: (0.5 pts)

+ 0.1 M H2C2O4

Test tube 2: (0.5 pts)

+ 6 M HCl

Test tube 2: (0.5 pts)

+ 6 M NH4OH

Comment: (0.75 pts)

4. TEMPERATURE EFFECTS ON EQUILIBRIA

Equilibrium System:Co(H2O)62+(aq) + 4Cl(aq) ⇌ CoCl42(aq) + 6H2O(l)

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Description of Predicted
Observation Explanation
conditions outcome

Nothing changed (0.5 pts)

(control)

(0.5 pts)

Hot water bath

(0.5 pts)

Ice-water bath

Comment: (0.75 pts)

IV. Conclusions (1 pt)

(conclude all your performance in this report)

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 International University, Vietnam National University - HCMC 19
CHEMISTRY LABORATORY

REPORT
EXPERIMENT 5: FACTORS AFFECTING
REACTION RATE

Group: _____________ Section: ______5________ Date: ____________

Group members:

Seq. Full name Student ID % contribution Signature Score

(total = 100%)
1

Total score: ________/15__

Present well: 1 point

Clear picture: 1 point

Total = 15 points

The report must be typed and handed in together with the signed data sheet by the deadline
 International University, Vietnam National University - HCMC 20
CHEMISTRY LABORATORY

I. Introduction (1 pt)
(Introduce what experiments you do in this report)

II. Experimental (1 pt)

(Describe what experiments you did in this report, write down each step of your
experiments)

III. Results and discussion

1. EFFECT OF CONCENTRATION ON REACTION TIME (5 pts)

Reaction 1:

__________________________________________________

Reaction 2:

__________________________________________________

Calculate the initial concentrations of I- and S2O82- ions:

Mixture # 5:

(1 pt)

[I-] =

[S2O82-] =

Mixture Iodide ion Peroxydisulfate Time in seconds

1 0.08 0.04

2 0.068 0.04

3 0.056 0.04

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4 0.044 0.04

5 0.032 0.04

6 0.02 0.04

Mixture Iodide ion Peroxydisulfate Time in seconds

7 0.08 0.034

8 0.08 0.028

9 0.08 0.022

10 0.08 0.016

11 0.08 0.01

Plotting the concentration of iodide ion versus time: [Note: X – axis: time; Y – axis:
concentrations].

- Mixtures # 1-6: Graph (1 pt)

The order of reaction with respect to iodide ion? (0.5 pts)

Comments: (0.5 pts)

- Mixtures # 1, 7, 8, 9, 10, and 11: Graph (1 pt)

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The order of reaction with respect to peroxydisulfate ion? (0.5 pts)

Comments: (0.5 pts)

2. EFFECT OF TEMPERATURE ON THE REACTION RATE (2 pts)

Reaction System:

Description of Predicted Observation Reaction Explanation

conditions outcome time

Room (0.5 pts)

temperature

(0.5 pts)

500C

900C (0.5 pts)

Comment: (0.5pt)

3. EFFECT OF A CATALYST ON THE REACTION RATE (3 pts)

Reaction System:

Trial Description of Predicted Observation Explanation

conditions outcome (Reaction rate)

1 + MnCl2 (0.25 pts)

2 + MnO2 (0.25 pts)

3 + NaCl (0.25 pts)

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4 + CaCl2 (0.25 pts)

5 + Zn (0.25 pts)

6 + KNO3 (0.25 pts)

7 + Fe(NO3)3 (0.25 pts)

The order of catalyst activity: (0.5 pts)

Comments: (0.75 pts)

IV. Conclusions (1 pt)

(conclude all your performance in this report)

The report must be typed and handed in together with the signed data sheet by the deadline