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Govt Approval Hi Tech Iso 17088 Full Report

This document provides test results for a sample submitted by HI-TECH INTERNATIONAL. Testing was conducted between October 2020 and June 2021 according to ISO 17088 standards. The sample was identified as a blend of poly lactic acid, poly butylene adipate co-terephthalate, and starch. Test results showed the sample had an 8.2% dry mass remaining after 84 days, 90.04% ultimate aerobic biodegradation after 133 days, and over 90% seed emergence for rice and radish plants.

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Mukul Sareen
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0% found this document useful (0 votes)
131 views9 pages

Govt Approval Hi Tech Iso 17088 Full Report

This document provides test results for a sample submitted by HI-TECH INTERNATIONAL. Testing was conducted between October 2020 and June 2021 according to ISO 17088 standards. The sample was identified as a blend of poly lactic acid, poly butylene adipate co-terephthalate, and starch. Test results showed the sample had an 8.2% dry mass remaining after 84 days, 90.04% ultimate aerobic biodegradation after 133 days, and over 90% seed emergence for rice and radish plants.

Uploaded by

Mukul Sareen
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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ftrte: ekd.

{e dq wrfum
qnd
ffifr CIPET : INSTITUTE OF PLASTICS TECHNOLOGY
(Ministry of Chemicals & Fertilizers, Govt. of lndia)
t{sEr qd da6 iTrdrq, rrdR)
f,rq,.d i* - eoo o:2. Guindy, Chennai - 600 032.
.ia . v-qq-zzzs ctol-6 +Eq : g1-44-222s4707 crperltta fel:91-44-2225 47 01-6 Fax :91 - 44 -22254707
l-fi : chennai@cipet.gov.in d'rr{a : wwwcipet.gov.in E-mail : chennai@cipet.gov.in Website : www.cipet.gov.in

+lssued
qrt/ .rfr{q fidrJ/rssr nrPonr
to :
s.€ / sr. No. , Z.T tZB
HI.TECH INTERNATIONAL
Near Airport, Sahnewal, Ludhiana '1410'lO,
fidrJ { /REPoRr no.' 64058
1q-<ro/Dare: 10{6-2021
Pages.............Nos. Part.A,B,C&D
riEd / customer Let. Ref :
qdqnr qr++. wr * eqvn ctq"r fi+J i rEST REpoRTAs pERTEsr STANDARD : Refer Part C

$I[IT - ifi"/PART.A
Yqa *fue ar fuq{ur / PARTICULARS OF SAMPLE SUBMITTED .

sr) tft-o or rre / a) Name of the Sample .' Dr Bio Compostable Polymer & Film - as
stated bythe party

qr) tfue ctq d+ 41 drfrs/ b) Date of Receipt of sampte 27-10-2020

v) i-s,/r6n/€[r6R/fi / c) Grade / variety / type / size / class Nil

t) dft-d r1fl / d) Declared value, lf any : Nit

B) +i< d. / e) code No. . Nit

s) +s {. \t{ ftqfq ilfrq/ D Batch No. and Date of Manufacture: Nit

E) cr{r / g) Quantity : 1.5 kg

\) tf{i'I 61 tFd / h) l\.4ode of Packing :


Packed in Aluminium foil cover

t) ct6{ dE qr rd / i) Sealed or not : Not Sealed

$,1 +t{ er< gt-+11; nny other information :

qFI _ tI /PART-B
OTST{$, qfiTE7 SUPPLEMENTARY INFORMATIONS

u) tfrftir rtffi fu ri+f I a1 Reference to sampling procedure : Sampling not done by this lab
) qrq q-G ki ieq rtq Erq-+ <<r+q qq vrq cRqrc
rqr
: AsgiveninPartC
bi Supporting documents forthe measurement taken and result derived
q) ridnrc +'d lriilf t t{tifR( * ergvn vft<.r tf( * 6t{ rFn-dl
c) Deviation from the test method as prescribed in relbvant work instructions, if any : No deviation from the standard
25001 to 30000 / AVP I 23.07.2020 1of
fufc : EReq{e dq qrkm tddidf CIPET : INSTITUTE OF PLASTICS TECHNOLOGY
F{m r{$
qq qrrdq, qfld {rdR) (Ministry of Chemicals & Fertilizers, Govt. of lndia)
ffi na 600 03r. Guindy, Chennai - 600 032.
sh :91-44-2225 4701-6 dEa . v-qq-ZZZSqtOt crPEr flq t. fel:9144-2225 47 01-6 Fax : 91 - 44 -22254707
i t-d : chennai@cipet.gov.in aq# : wwwcipet.gov.in E-mail : chennai@cipet.govin Website : vr.!vw.cipet.gov.in

qTTqM ffiITCST REPORT


fir+J { / REPoRT 1{o. : 64r jF'.{ / st. No. 27123
10-06-2021
R{ro / Date :

qTTI _ TI / PART.C
qtHur qftUrlc / TEST RESULTS
Test Duration: 28.10.2020 to 10.06.2021

Sl.No Name of the Test


Test Method/ Specified
Unit Results Obtained
Standard Requirements
Blend of Poly Lactic
Acid (PLA) and Poly
1 Material ldentification FTIR & DSC Butylene Adipate Co-
Terephthalate (PBAT)
with Starch
Disintegration (Dry
mass remains in 2
tso
2 17088:2012 I o/o No more than
mm Sieve after 84 8.2
10o/o
lS 17088:2008
days)

Ultimate aerobic > 90 (at the


Biodegradation (with tso 9O.O4o/o end of the test
3 reference to 100% 17088:2012 I -lo (at the end of 133 period not
degradation of lS 17088:2008 days) more than 180
positive reference) days.)
Plant GroMh study

Monocotyledon
4 (Rice) tso -/o 92 >90
% Seed emergence 17O88:2012 I
Dicotyledon (Radish) lS 17088:2008
% Seed Emerqence
o/o
91 >90
The detailed observation on biodegradability test is enclosed as Annexure

Contd.

2ol

AUTHORI IGNATORY RISED SIGNATORY


ftrte'edfrO-td-sz.
CIPET : IPT- Chennaisz.
crpe r lt i e Continuation Sheet

fistJ ri / nePonr *o. cfrqur cRqTq /TEST RESULTS frqrq- / Date :


' 6405g 1046-2021

PARTC.TESTRESULTS

Test Method/ Specified


Sl.No Name of the Test Unit Results Obtalned
Standard Requirements*
E Heavy metals
concentration
a. Arsenic (As) 0.002 20
b. Copper (Cu) 0.095 500
c. Nickel (Ni) BDL(DL-0.005) 100
'd. Zinc (Zn) ISO 17088:20121 0.099 2500
e Cobalt (Co) lS 17088:2008 mg/L o.228
f. Chromiurh (Cr) o.176 300
Molybdenum (Mo) 0.845
h. Mercury (Hg) BDL(DL-0.0006) 1;
i. Cadmium (Cd) 0.002 20
j. Lead (Pb) 0.'t87 500
k. Selenium (Se) 0.022
* Based on Municipal waste (Management and Handling) Rules, 1999 notified on 27th September, 1999
by
Ministry of Environment and Forests, Government of lndia. Note that concentration of metals like cobalt,
molybdenum, and selenium is not mentioned in the notification.
Note: BDL - Below Detection Limit; DL - Detection Limit

PART D. REMARKS
NIL
Note
1. This Test Report / Certificate is issued only for the samples submitted to the laboratory.
2. The results stated above related only to the items tested.
3. The quality ofthe subsequent production lot has to be ensured by the purchaser.,
4. This Test Report shall not be reproduced except in full without the written approval of the laboratory.
5. Any anomaly/discrepancy in this report should be brought to the notice of the laboratory within 30 days
from the date of issue.
6. Subcontracted Tests (if any):Nil

Contd.,

ruroxnrseo sffironv ISED SIGNATORY


ANNEXURE
frrfe, err$ fr O-fi-sz.
CIPET : IPT- chennai-32.
crperitiz Continuation Sheet

*o. qfrqq qfturrq / TEST RESULTS


f<qtJ ri I nrPonr f<tro / Date :
' 6405g 1046-2021

"*'l::::i :wffi;t,,,:_: { 7088 : 2ol z s'


^*':*'

2 ;'::;#;ffi
3
=i,"ii#Hi,Hiry,$,?;*,:,:Y.*
.(D Xffi-T:T,""*on*,**
origin of Compo.t' Lir".t""k ffi, municipal and vegetabte waste
Reaction Temperature (oC) :58
Dry Solid (%) : 54.6
Voldtile content (%) : 13.6
CO2 evolved during first 1odays in blank
vessels (mg/g of volatile content of : 74.2mglg
compost)
Test duration (days) : 133 days
Reference material : Cellulose
Volume of reaction vessel (mL) : 3000 ml
(ii) pH of test medium
S.No. Compost Vessel pH (Before) pH (After)
1 Blank 1 7.2 7.1
2 Blank 2 7.2 7.1
3 Blank 3 7.2 7.1
4 Cellulose 1 7.4 7.2
5 Cellulose 2 7.4 7.2
Cellulose 3 7.3 7.'l
7 Negative 1 7.2 7.',|
Negative 2 7.2 7.1
9 Negative 3 7.2 7.1
10 Sample '1 7.3 7.1
11 Sample 2 7.3 7.1
12 Sample 3 7.2 7.2

Contd.,

AUroHR,sEo',\[tJ-' ISED SIGNATORY


ftrfe qr{ O O-fi-ez.
'
GIPET : IPT- Chennai-32. Continuation Sheet

fiHtJ Ii / REPoRT *o, qtsq qRunq /TEST RESuLTS


f<qrfi' / Date :
'6405g 10-06-2021

Result: Percentage biodegradation relative to positive reference


Sample (Mean) : 90.04o/o at the end o[133 days
The reference Material - cellulose : .- lOOo/o
100

90

so

z 70
IF
50
o
E 50
o
IIJ
o 40
o
6 30
s 20

10

0
40 60 80 100
tNcuBAT|oN'lIuE (DAYS)

Visual Observation of Sample


Descriotionr: wd6ki3 Week 6 Week 9
rragmen( :d
Structure Film sample Film sample
oieces
Adequate
Moisture Adequate moisture Level Adequate moisture Level
moisfi rre I evFl
)olour White Dirty rirty
Funqal Development None one
Smell Orsanic/dirt like Organic/dirt like )rqanic/dirt like

Description Week 12 Week 15, Week 19


Fragmented
Structure Fragmented pieces Fragmented pieces .
oieces
Adequate
Moisture Adequate moisture Level Adequate moisture Level
moisture Level
)olour Dirty rtv rty
Funqal Development None None None
=-----------:---
anic/dirt like
Smell )roanic/dirt like Oroanic/dirt like

Contd.,

AUroHRSEDs,r,4|"
frte:qr€fifr-d-az.
CIPET : IPT- Chennai-32.
crper ft t e Continuation Sheet

ft+Jri/REPoRT o.: vfiqTq qftWq /TEST RESULTS frrm' / Date :

64058 10-06-2021

Visual Observation of Compost

Week6 ''i I, iWeek9


Structure Fine Particles Fine Particles Fine Particles
Adequate
Moisture Adequate moisture Level Adequate moisture Level
moisture Level
Colour Dark Brown Dark Brown Dark Brown
Funqal Development Nit Nit Nit
Smell Organic/dirt like Organic/dirt like Organic/dirt like

Description I
Week 12 Week 15 ',I '''Week 19
Structure Fine Particles Fine Particles Fine Particles
Adequate
Moisture Adequate moisture Level Adequate moisture Level
moisture Level
Colour Dark Brown Dark Brown Dark Brown
Fungal Development Nit Nit Nit
Smell Organic/dirt like Organic/dirt like Orqanic/dirt like

7 FTIR Analysis
Sample Details (As stated by Party): Dr Bio compostable Polymer & Film

Contd.,

AUroHRrsED.lh"-" ISED SIGNATORY


ftrte, qr{ fi O-fi-sz.
GIPET : IPT- Chennai-32.
crper ft i c Continuation Sheet

firilJ rirneponr*o.,6405g c-0frur cRunq /TEST RESULTS R'ttt[' / Date :

10-06-2021

FTIR lnterpretation

Wave number (cm'l) Nature of Bond


29't7 CH2 asymmetric stretching
17',to C=O in PLA and PBAT
1457 -CH2 Plane Bending
1267 C-O bonds of PBAT
1117 C-O bonds of PBAT
1080 C-O bonds of PBAT
872 O-CH-CH3 of ester
726 CH plane of benzene ring

DSG Analysis

Comment: The above DSC & FTIR analysis indicates the above sample is
Blend of Poly Lactic Acid (PLA) and Poly Butylene Adipate Co-Terephthalate (PBAT) with Starch

Contd.,

ouror*,rrr asro*" w
AUTHORISED SIGNATORY
frfe'edfrO-fi-sz.
CIPET : IPT- Chennai-32.
crprr It i z Continuation Sheet

qfrqol TRunq /TEST RESULTS


ffiJ(lnePonr*o.,6405g f,{tm / Date :
10-06-2021
' l,'

Disintegration After 12 Weeks

Before Disintegration After Disintegration

The disintegration of the supplied sample by passing through 2 mm sieve aflet 12 week in composting
condition as per ISO 17088-2O12llS 17088: 2008 was found not more than 10% of original dry mass
remain.

10 Seed Germination & Plant growth study

Rice Compost (Control) Rice Compost (Sample)

Contd.,

ISED SIGNATORY
a
ftte: er$ fi E-iri-sz.

fidJ ri I nrPonr *o. '6405g cnqur cRrnq /TEST RESuLTS k{H' i Date :
10-06-2021

Radish Compost (Control) Radish Compost (Sample)

The percentage of seed germination rate is found to be greater than 90% for both Rice and Radish

AUT ED SIGNATORY
^,,,o*,.=,(frAroRy

aufoHRlsErr$G*x+env= TgRI
4IIIHOBTSED-STGN

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