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SS EN 934-6 : 2008 (2015)

(ICS 91.100.99)

SINGAPORE STANDARD

Specifications for admixtures for

concrete, mortar and grout
– Part 6 : Sampling, conformity control and
evaluation of conformity
(This national standard is the identical implementation of EN 934-6 : 2001 and is adopted with
permission of CEN, Avenue Marnix 17, 1000 Brussels)

Confirmed 2015

Published by
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SS EN 934-6 : 2008 (2015)

(ICS 91.100.99)

SINGAPORE STANDARD
Specifications for admixtures for
concrete,mortar and grout
– Part 6 : Sampling, conformity control and evaluation of
conformity

All rights reserved. Unless otherwise specified, no part of this Singapore Standard may be
reproduced or utilised in any form or by any means, electronic or mechanical, including
photocopying and microfilming, without permission in writing from SPRING Singapore at the
address below:

SPRING Singapore
1 Fusionopolis Walk
#01-02 South Tower, Solaris
Singapore 138628
Email : standards@spring.gov.sg

ISBN 981-4154-96-2
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This Singapore Standard was approved by the Building and Construction Standards Committee on
behalf of the Standards Council of Singapore on 11 December 2008.

First published, 2008

The Building and Construction Standards Committee appointed by the Standards Council consists of
the following members:

Name Capacity
Chairman : Mr Goh Peng Thong Member, Standards Council
st
1 Dy Chairman : Mr Lee Chuan Seng Member, Standards Council
nd
2 Dy Chairman : Mr Tan Tian Chong Member, Standards Council
Secretary : Mr James Choo SPRING Singapore
Members : Mr Boo Geok Kwang Singapore Civil Defence Force
Er. Chan Ewe Jin Institution of Engineers, Singapore
Mr Chan Yew Kwong Ministry of Manpower
Mr Paul Fok Land Transport Authority
Mr Goh Ngan Hong Singapore Institute of Surveyors and
Valuers
Mr Anselm Gonsalves National Environment Agency
Mr Desmond Hill Singapore Contractors Association Limited
Mr Benedict Lee Khee Chong Singapore Institute of Architects
Ms Andris Leong Building and Construction Authority
Assoc Prof Leong Eng Choon Nanyang Technological University
Dr Lim Lan-Yuan The Association of Property and Facility
Managers
Mr McDonald Low Real Estate Developers’ Association of
Singapore
Mr Larry Ng Lye Hock Urban Redevelopment Authority
Assoc Prof Gary Ong Khim Chye National University of Singapore
Mr Davis Ong Wee Choon Singapore Manufacturers’ Federation
Er. Shum Chee Hoong Housing & Development Board
Dr Tan Guan Association of Consulting Engineers,
Singapore
Mr Tang Pei Luen JTC Corporation
Co-opted
Member : Dr Tam Chat Tim Individual Capacity

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The Technical Committee on Building Structure and Sub-structure appointed by the Building and
Construction Standards Committee and responsible for the preparation of this standard consists of
representatives from the following organisations:

Name Capacity

Chairman : Dr Tan Guan Member, Building and Construction

Standards Committee
Co-Chairman : Mr Chew Keat Chuan Building and Construction Authority
Secretary : Ms Lee Hiok Hoong SPRING Singapore
Members : Er. Chan Ewe Jin Institution of Engineers, Singapore
Dr Chen Enyi Cement and Concrete Association of
Singapore
LTC Cheok Poh Chin Singapore Civil Defence Force
Dr Sujit Ghosh Ready Mix Concrete Association of
Singapore
Dr Ho Nyok Yong Singapore Contractors Association Ltd
Mr Ho Wan Boon Singapore Structural Steel Society
Assoc Prof Gary Ong Khim Chye Singapore Concrete Institute
Mr Song Siak Keong Land Transport Authority
Mr Sze Thiam Siong Setsco Services Pte Ltd
Ms Angeline Tan Bee Hoon Housing & Development Board
Mr Tan Jui Teck CPG Corporation Pte Ltd
Assoc Prof Tan Kiang Hwee National University of Singapore
Assoc Prof Tan Teng Hooi Nanyang Technological University
Mr Tang Pei Luen JTC Corporation
Co-opted
Member : Dr Tam Chat Tim Individual Capacity

The following Technical Experts contributed in their individual capacity to the preparation of this
standard:

Dr Tam Chat Tim (Co-Taskforce Leader)

Mr Willie Kay (Co-Taskforce Leader)
Dr Sujit Ghosh
Mr Michael Ho
Mr Jiang Jia Biao
Mr Lim Huay Bak
Mr Lu Jin Ping
Dr Ravi Prasad
Mr Seow Kiat Huat
Dr Arvind K Suryavanshi
Mr Tan Tze Tiong
Mr Yeo Peng How

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The organisations in which the experts are involved are:

Admaterials Technologies Pte Ltd

BASF Construction Chemicals Singapore Pte Ltd
Cement and Concrete Association of Singapore
Holcim (Singapore) Pte Ltd
Housing & Development Board
Mapei Far East Pte Ltd
Meinhardt Infrastructure Pte Ltd
National University of Singapore
Setsco Services Pte Ltd
Singapore Concrete Institute
WAK Consultants Pte Ltd

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Contents

Page

National Foreword 6

CLAUSES

1 Scope 7
2 Normative references 7
3 Terms and definitions 7
4 Sampling 8
5 Conformity control and evaluation of conformity 10

ANNEXES

A (informative) – Certification of factory production control 12

B (informative) – Calibration of measuring equipment 13

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National Foreword
This Singapore Standard was prepared by the Technical Committee on Building Structure and Sub-
structure under the purview of the Building and Construction Standards Committee.

This standard is a result of the review of SS 320 : 1987 – ‘Concrete admixtures’. The SS EN 934
series of standards replaces SS 320.

This standard is identical to EN 934-6 : 2001 – ‘Admixtures for concrete, mortar and grout – Part 6 :
Sampling, conformity control and evaluation of conformity’, incorporating CEN Corrigendum No.1 and
A1>
Amendment No.1 (2005) denoted by , and adopted with permission of CEN, Rue de Stassart 36, B-
1050 Brussels.

Attention is drawn to the following:

1. Where reference is made to European Standards, it has been replaced by ’Singapore

Standard’ where applicable.

2. The comma used as a decimal marker has been replaced by a full point on the baseline.

3. The National Foreword replaces the Foreword of EN 934-1.

This standard is a part of the series SS EN 934 `Admixtures for concrete, mortar and grout’ which
additionally comprises the following parts:

– Part 1 Common requirements

– Part 2 Concrete admixtures - Definitions, requirements, conformity, marking and labelling
– Part 4 Admixtures for grout for prestressing tendons – Definitions, requirements, conformity,
marking and labelling

This Singapore Standard is used with the standards of the EN 480 series which comprises test
methods for admixtures (listed in Clause 2).

At the time of publication, this standard is expected to be used as a reference in the Building and
Construction Authority’s ‘Approved Document – Acceptable Solutions’.

Attention is drawn to the possibility that some of the elements of this Singapore Standard may be the
subject of patent rights. SPRING Singapore shall not be held responsible for identifying any or all of
such patent rights.

NOTE

1. Singapore Standards are subject to periodic review to keep abreast of technological changes and new
technical developments. The changes in Singapore Standards are documented through the issue of either
amendments or revisions.

2. Compliance with a Singapore Standard does not exempt users from legal obligations.

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SS EN 934-6 : 2008 (2015)

Specification for admixtures for contrete, mortar and grout –

Part 6 : Sampling, conformity control and evaluation of conformity

1 Scope
This Singapore Standard specifies procedures for sampling, conformity control and evaluation of
conformity, for admixtures according to the series SS EN 934.

2 Normative references
This Singapore Standard incorporates by dated or undated reference, provisions from other
publications. These normative references are cited at the appropriate places in the text, and the
publications are listed hereafter. For dated references, subsequent amendments to or revisions of any
of these publications apply to this Singapore Standard only when incorporated in it by amendment or
revision. For undated references the latest edition of the publication referred to applies (including
amendments).

SS EN 934-1, Admixtures for concrete, mortar and grout – Part 1: Common requirements

SS EN 934-2, Admixtures for concrete, mortar and grout – Part 2: Concrete admixtures - Definitions,
requirements, conformity, marking and labelling.

EN 934-3, Admixtures for concrete, mortar and grout – Part 3: Admixtures for masonry mortar –
Definitions, requirements, conformity, marking and labelling

SS EN 934-4, Admixtures for concrete, mortar and grout – Part 4: Admixtures for grout for
prestressing tendons – Definitions, requirements, conformity, marking and labelling.

EN 934-5, Admixtures for concrete, mortar and grout – Part 5: Admixtures for sprayed concrete –
Definitions, requirements, conformity, marking and labelling

3 Terms and definitions

For the purposes of this standard, the following terms and definitions apply.

3.1 Batch

A quantity of admixture which can be considered to have a uniform composition

Note – A tank load can be considered as the equivalent of a batch.

A1>
3.2 Responsible person

Person appointed by the manufacturer whose duties include implementation of all or a defined part of
the production control manual

3.3 Manufacturer

Organisation having full control and responsibility for the delivered admixture, including carrying out
<A1
the factory production control testing .

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4 Sampling

4.1 General
A1>
Sampling of admixtures shall be carried out in such a way that the resulting sample is
<A1
representative of the batch to be inspected.
A1>
The following procedures shall be used:

– for initial type testing and in case of dispute 4.2;

– at time of delivery 4.3;
– for factory production control 4.4
<A1
If required, sampling shall be carried out in the presence of all parties concerned.

4.2 Sampling from the manufacturer's stock

4.2.1 General

Each sample shall represent not more than one batch. For continuous production of an admixture one
sample taken from up to 25 t may be regarded as representative.

4.2.2 Powder admixture (in packages)

The sample shall be composed of sub-samples from 6 packages (bags) or if the total number of
packages (bags) is less than 6, from all packages (bags). The sub-samples are to be taken from
packages (bags) distributed at random throughout the consignment.

One of the following procedures shall be applied:

– Where the packages contain up to 500 g take all the contents of each package.

– Where the packages contain more than 500 g, use one of the following methods:

a) insert a sampling tube, which takes a core not less than 25 mm in diameter, into the packages
so that it takes a core of the material from substantially the entire length of the package.

b) empty one of the packages to be sampled on to a clean dry surface and mix the material.
Take at least three portions of not less than 125 g each from different parts of the heap.

The method given in a) is the preferred method, but if a sampling tube is not available, the method
given in b) shall be used.

Repeat the procedure with each of the other packages to be sampled and thoroughly mix the sub-
samples obtained to form one bulk sample. If the bulk sample exceeds 3 kg it shall be reduced to 3
kg, either by coning and quartering or by use of a sample splitter.

Divide the sample into three equal parts and place each part in a clean, air tight, labelled container. At
least one container holding 1 kg shall be kept for future reference. Store container(s) in a place that is
protected from moisture, heat and light for one year or until the use-by date whichever is the shorter
period.

4.2.3 Liquid admixture

4.2.3.1 General

In order to achieve representative samples of liquid admixtures one of the following procedures shall
be applied.

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4.2.3.2 Sampling of a liquid admixture from containers

The sample shall be composed of sub-samples taken from 6 containers or if the total number of
containers is less than 6 from all containers. The sub-samples are to be taken from containers
distributed at random throughout the consignment.

Agitate the admixtures in the containers to disperse all lightly settled material. Disregard all deposits
which are not readily brought into suspension by such agitation.

Without delay, take sub-samples from the selected containers by one of the following procedures:

a) where containers hold up to 0.5 l, take the total contents;

b) Where containers hold more than 0.5 l take 0.5 l of the liquid from each container, combine
the sub-samples obtained in this way and mix them thoroughly to form one bulk sample.

4.2.3.3 Sampling of a liquid admixture from a tank load

When the load is agitated one sample may represent the entire tank load of up to 25 000 l. The bulk
sample shall be at least 3 l.

Otherwise three samples shall be taken as follows: one from the top level, one within ± 300 mm of the
mid-level of the fluid and one within 400 mm of the bottom of the tank. Each sample shall be not less
than 1 l. Thoroughly mix the three samples until they form one homogeneous bulk sample.

4.2.3.4 Division of sample

The bulk sample obtained by one of the procedures described above (4.2.3.2 or 4.2.3.3) shall be
divided into 3 equal samples. Place in three clean bottles, label and tightly stopper. At least one bottle
shall be kept for future reference for one year or until the use-by date, whichever is the shorter period.

Store the bottle(s) in a place that is protected from heat, frost and light.

4.3 Sampling at delivery

When sampling of a consignment of an admixture is required, the sampling shall be carried out before
unloading at the point and time of delivery. The method of sampling shall be agreed between the
supplier and the customer. If there is no agreement between them, the methods described in 4.2.2
and 4.2.3 shall apply.
A1>
4.4 Sampling for factory production control

Sampling procedures for factory production control shall be documented in the production control
manual. The procedure shall ensure that a representative sample is obtained.

NOTE – As a guide, at least one sample should be taken per bath or, in the case of continuous production, at
not more than 25 t intervals. After testing a sample of not less than 250 ml should be retained for at least one
year or the shelf life of the product, if longer. If the normal admixture dosage exceeds 2 %, a larger sample
<A1
should be retained.

A1>
4.5 <A1 Record
All information relevant to the sampling shall be recorded, in particular:

a) date of sampling;

b) name of the product;

c) type of admixture;

d) name of the manufacturer;

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e) manufacturer's batch identification number;

f) quantity of batch represented by the sample;

g) physical state;

h) colour;

i) names of persons present and organizations represented during sampling.

5 Conformity control and evaluation of conformity

5.1 General

This procedure is intended to evaluate conformity of admixtures with the relevant parts of the series
SS EN 934.

5.2 Conformity criteria

Composition and performance requirements and the related checks and test methods are given in the
relevant parts of the series SS EN 934. When tested in accordance with these methods each result
shall conform to the relevant requirement.

5.3 Initial type testing

Initial type testing shall be carried out to prove the conformity of the admixtures to the requirements of
the relevant part of the series SS EN 934, in the following circumstances:

a) when a new formulation or type of admixture is produced;

A1>
b) when there is a change in formulation which may have significant effect on the
performance of the admixture or which affects the manufacturer's stated values for the
<A1
product as listed under general requirements in the relevant part of the SS EN 934 series;

A1>
c) when there is a change in the raw materials which may have a significant effect on the
performance of the admixture or which affects the manufacturer's stated values for the
<A1
product as listed under general requirements in the relevant part of the SS EN 934 series.

Initial type testing shall include all tests relevant for a specific type of admixture.

5.4 Factory production control

5.4.1 General
A1>
The manufacturer shall operate production control at each factory where admixtures are produced.
Production control shall include control of raw materials, production processes and the finished
product. The production control procedures shall be contained in a production control manual for each
<A1
factory.
A1>
5.4.2 Production control manuals

Each production control manual shall specify the procedures to ensure that admixtures supplied from
each factory conform to the requirements of EN 934 Parts 2 – 5. As a minimum the following items
shall be included:

a) training for production and quality control operatives including the level of training necessary;

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b) procedures for the identification, sampling, approval, traceability, storage and expiry dates of
raw materials;

c) procedures for servicing and calibrating all manufacturing and test equipment (see annex B);

d) manufacturing and sampling instructions;

e) procedures for FPC testing at the frequency required by the relevant parts of the SS EN 934
series;

f) details of FPC acceptance limits, linked to the manufacturer's stated values for the current ITT
documentation;

g) action to be taken in case of non-compliance of raw materials, intermediate and finished

products;

h) instructions for packaging, storage, labelling and delivery of finished products;

i) procedures to ensure that only admixtures which conform to the relevant part of the SS EN
934 series of standards are labelled as complying;

j) records to be prepared and period for which they shall be retained (5.4.3).

Individual responsibilities shall be defined in the production control manual. Each responsible person
shall report to a senior manager who has the authority to ensure that the procedures in the production
control manual are fully implemented.

Where appropriate, the production control manuals shall be supplemented by additional documented
<A1
instructions relating to the items listed above.
A1> <A1
5.4.3 Production control records

The following details shall be recorded clearly and in chronological order:

A1>
a) results of checks on measuring equipment used in production and testing, including
<A1
calibration reports;

b) raw materials identification and test results;

c) production data (type and marking of the admixture, batch identification number, quantity
produced, date of production and any production code);
A1> <A1
d) sampling in accordance with clause 4;

e) date and results of production control tests and checks, comparison with requirements and,
where appropriate, action taken;
A1> <A1
f) signature of the responsible person

These records shall be stored for at least 5 years.

5.5 Certification of factory production control

A1>
Where certification of factory production control is required by Annex ZA in EN 934 Parts 2 – 5, a
notified body appointed by the manufacturer shall carry out an initial inspection for each factory
producing admixtures within the scope of EN 934 Parts 2 – 5. Subsequently, there shall be an annual
<A1
surveillance of each factory by the notified body (see Annex A).

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Annex A
(informative)

Certification of factory production control

A1>
The notified body should carry out further visits if serious non-conformities in the factory production
control are identified. The manufacturer should inform the notified body of any change in the factory
production control procedures.

Initial type testing is the responsibility of the manufacturer but the notified body should be informed if
additional type testing has been carried out as a result of changes in the product or in the factory
<A1
production control.

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A1>
Annex B
(informative)

Calibration of measuring equipment

All measuring equipment used in production and testing should be calibrated if it can have a significant
effect on product quality or testing. The production control manual should include a procedure for
identifying measuring equipment which has to be calibrated and state the frequency of checking and
calibration.

Calibration procedures should comply with European, International or National standards where
applicable, otherwise normal good practice should be followed. All calibration should be performed
using weights and measures which have calibration certificates identifying their relationship with
<A1
international or national standards for weights and measures.

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ABOUT SPRING SINGAPORE

SPRING Singapore is an agency under the Ministry of Trade and Industry responsible for helping
Singapore enterprises grow and building trust in Singapore products and services. As the national
standards and accreditation body, SPRING develops and promotes an internationally-recognised
standards and quality assurance infrastructure. SPRING also oversees the safety of general
consumer goods in Singapore. As the enterprise development agency, SPRING works with partners to
help enterprises in financing, capability and management development, technology and innovation,
and access to markets.

SPRING Singapore
1 Fusionopolis Walk
#01-02 South Tower, Solaris
Singapore 138628
Tel: 6278 6666
Fax: 6278 6667
E-mail: enterpriseone@spring.gov.sg
Website: http://www.spring.gov.sg

3. ABOUT THE NATIONAL STANDARDISATION PROGRAMME

Under the national standardisation programme, SPRING Singapore helps companies and industry to
meet international standards and conformity requirements by creating awareness of the importance of
standardisation to enhance competitiveness and improve productivity, co-ordinating the development
and use of Singapore Standards and setting up an information infrastructure to educate companies
and industry on the latest developments.

SPRING Singapore is vested with the authority to appoint a Standards Council to advise on the
preparation, publication and promulgation of Singapore Standards and Technical References and
their implementation.

Singapore Standards are in the form of specifications for materials and products, codes of practice,
methods of test, nomenclature, services, etc. The respective committee or working group will draw up
the standards before seeking final approval from the Standards Council or the relevant Standards
Committee. To ensure adequate representation of all viewpoints in the preparation of Singapore
Standards, all committees appointed consist of representatives from various interest groups which
include government agencies, professional bodies, tertiary institutions and consumer, trade and
manufacturing organisations.

Technical References are transition documents developed to help meet urgent industry demand for
specifications or requirements on a particular product, process or service in an area where there is an
absence of reference standards. Unlike Singapore Standards, they are issued for comments over a
period of two years before assessment on their suitability for approval as Singapore Standards. All
comments are considered when a technical reference is reviewed at the end of two years to
determine the feasibility of its transition to a Singapore Standard. Technical References can therefore
become Singapore Standards after two years, continue as Technical References for further
comments or be withdrawn.

In the international arena, SPRING Singapore represents Singapore in the International Organization
of Standardization (ISO), the Asia-Pacific Economic Co-operation (APEC) Sub-committee for
Standards and Conformance (SCSC) and in the ASEAN Consultative Committee on Standards and
Quality (ACCSQ). The Singapore National Committee of the International Electrotechnical
Commission which is supported by SPRING Singapore, represents Singapore in the IEC.

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The Singapore Standardisation

Programme is managed by
SPRING Singapore
1 Fusionopolis Walk
#01-02 South Tower, Solaris
Singapore 138628
Tel : +65 6278 6666
Fax : +65 6278 6667
www.spring.gov.sg