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Practical File

This document describes three experiments to determine: 1. The strength of sodium hydroxide (NaOH) solution by measuring its conductivity. 2. The rate constant of the separation of ethyl acetate in a conductivity experiment. 3. The rate constant of the separation of oxalic acid in a NaOH solution by measuring conductivity over time. Procedures, observations, calculations, and results are presented for each experiment. Graphs and tables of conductivity measurements are included.

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Nargis Ruhi
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0% found this document useful (0 votes)
37 views22 pages

Practical File

This document describes three experiments to determine: 1. The strength of sodium hydroxide (NaOH) solution by measuring its conductivity. 2. The rate constant of the separation of ethyl acetate in a conductivity experiment. 3. The rate constant of the separation of oxalic acid in a NaOH solution by measuring conductivity over time. Procedures, observations, calculations, and results are presented for each experiment. Graphs and tables of conductivity measurements are included.

Uploaded by

Nargis Ruhi
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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AimTo detenine the

ConYot Cci

Req+tnent Cond o t e , condoci h c, kta


e , StCndad NGn
Pee

aci
obseavOh on vol st
NCOH
Date:

Exhermteat-1
Armi Io detexmae the S t e g h af eo
Sakstian (apaox Nlin) tictingitgia
SkCndc.d ie, Nl daoH suluion conduttornRii¢el

ThtoLet a d s ( H ) i a taea ia the taacex-


Snibee Gtea heboaettes_

on odding naoH the highl osbile wiond


ose&e}lcted aloLs asniaqNa iondand

ShGapl c hee
àealAn highl osbile.

HC Maol

added, he

of_condotGne allue
Hente

Fe equlya\R nte o l a t

conduchoaR t Condridit C,
Reçtmentà
pipR\Leand urtitR SEGdad NGOY
eceY
So s a lucl So".

Teacher's Signature
Obse G i o n tOle

SNO

2
oOm

2
3 6-

16

Colc)oons.

o 12 N
Date

RxaCdme
dekiniR uolovne Ci. Lomo aosal) sf
addin aiailed ac.te
\hc \he elechaude atcoadchisiia

t Ssloisa. s_Conntch i o coadclomRkt


Ciad o he cadochance

daLdSska.Sm of NGOHSol faom he


boate into beesa CoakiaingH sai

Condvcr Cnce
Cune of
ARRdatog ConAsctanse_ageiask
alane

Dax aalitnof sTCdcad NoH N

caleoian
Le h nd ssintica at solane Va

using
o )
Teacher's Signature
nvoph

ReSLE St enh of 4c1 Nomcs X eq ot o 1 t


Date

Res - _statngth oSaisn uilsal


Sal"condoaomttticcl s

Teacher's Signature.
Aim To dererrent the Serengh of g e n o a e cid iee c oy

on Sol"
co b itrGtng Ggcinc cndard trona hase C
ordurDt ritoll

AR aeme nds- condsttio ridg ,co ne chs e chstout


stGrdcrd Oree ette, al

dbseruoti ons

volomt of Giutn CHCoðn


ormalit o f sto ndGvd NGOh co" - N
for otrtIAGHn Vod
vol omt of NCOM Yeqved
Tublt
obcered cond uttcne
S-o added inel) Coh )

I34X2oXro

O S xao *io

6
6 x aoXIO
T

-O 6 8 N?*t

8 XoXo

7-
x2oXro
ExheaimEnt-2
Date

To dakrarmiag the Staength of siutn uacis ctid


Lie Hoou Sa b aciog accast stndkrd
aang sda (sGau) sa oaductam&itall

pcatl ioniced

condNkanRof the sal is Saci sn addina Nosh


Sodism aR¥C.¥Ri foeeL
o i i r folloLSAaeatiin.

Ssdiasn aFG_ Somed is S o n eilalgH

into he sal ndauxidk ian haur lae ualue

Req ment Cond ctiuit balaR alutii .


Sta ndcd nGoh cs RoyR}FR_

Teacher's Signature _
Caldioions - N Nvi
(Chtoon) (G on )

O r o p h

Resut sirtngh sivtn atee cud so


Sol

:0 orb x
6 o 349
Date

ttiin Se dip in the so,

hR ohteàrd_cond ocrcncR

CoodXCnre ol of NGsld odded to çiad ostsolu

calralahda
cacouh)

Teacher's Signature
Aim 0eternine the rGte constcnt of he scpan:tiCHon of
ehylaceYGAe ConductOme tricGA'

Set+R , °iette, conitc Flceie (SecicevS


xherimtnt-3
Date:

Aim Dekermiane thR xaleConskaat o thesahoniitckieg


af Rhylateka NGOH csaducknmelritally

A a G t s Re rtd £hlacetale Sal" (Nas)saou (dDs


Later arid NLo 9xalieatid condush.oatktr s
ConducEit ulL Buree Piprttecoaital fiasi

Theo n the RxRStnte of baseNaOd, thahadralsS


ofcu coo ester Faueg Rlae o RYoduce H Caa-a

he 2no ordar iaetis Th


Ihe xin folloLas
xateof the * c a n en b
Rate eSex) ulester Con
dt

odtr Yoke_conskantin unit


uharR u

intsaxoksà eupression o f _ o ordtr a e


h
equahoa- C a n be giuen as
aCa-

LJhey a niial Lanttakrotionot recctanh


cancialratioa af Rradut at att.
contelrtatian af Ehe Yemahnin
x eattaat ak i n t
Teacher's Signature
Date

a thR aboue y*a hydroidr inn ragrissiual


ConSmtdbyaetateoa: siat thriooic
nabilitu
uch higher han chcoo ion (a,209 hR
ondickance af \he mixturR PragressiRl-

ataSartmea ak thr * i u r thus xside


nRanS af sstinatiaa af the amoust af-
theseions resent hence allous us rO ainor

I the condurtanCe of the * mitore cre


s s s at e beenning cto an ntr

Kat

CE-C

SIabeaf 1KIa Since thRintia conteateHon

fxoro thtSLofe Dhls i s de Fey mlned P


the ntaSrRnlatl o cornduc tanse aE diff.
Teacher's Signature.
Date

taurinq th canduttante otamiitu


ok Ssal hasing Same oncltrationof ao
SAcoH For de YmneHoo of_ ol aa
Sol of samR Conseotriàn need to bentaco.

Procedure -
xihar AkLon af exatt No sxalic acid sedad.ard soS
SCnd Ardizaion aR~ho naOH g n) wirh Rrebored
oxalicatid sol?,

4Soml (oasn esctt in atekate s s 2rtlartd.|


S MR SiorR theConduCEC nce of Soml Nlas NaoH_

6Pxefcxe\he_xAN miiture by addina soml af

1Skar tang canducka.ncRYiGding using candts


cell_conneeEe d o cocdurtiht l t l r T e cagd
ctiait aetr shod he calibeated betors

dIEC. i e t Shod hr nuted n 1ahl Ahis

9|AFLe ahudh lhaur (Ohea uoriadan a t sandutne

eo cooled ad Conducnce
Teacher's Signature.
obsersation Table s

S. no ime Condottance -Ct)|(CE-C) (Co-Ct) C

nSttt) ThS S CC-c) a (

\ o o31 6

S o ooAS

O olo4
o 6 o04O

R O O13 OOoI| 36

On
23 o oo27

O03R -6
Date:

Yeadinq is Fauen in a sa R Laau ThiSeadlo

Londckant ot sa contoinlnq Sml ar

obseraddns abaratoru temp 3


LARigs s t sxalic acid taxea a:4sg
Sxenathot R Rrsh.ard amaxalic_atid

Tae shandardizcEaa ak NasH sa" b iratina


agains standard oxalie aid Sa" dom in

ndicctar used = heoolphEbalela


adRoiat
S-mo Titial readingEiacvtadin aluat s f s

Calcolohons AvatEETa OXae acid NaOH

Teacher's Signature.
Graph

Resut The YGt tongiGnt (e) o r b e t oc on) ceelsed d

oR eh ateklt at 1Gb m{390) Locs found lo be


(lo
Date:

obserucddn Fakle for coadddance

DeRrmine khe sLahr of S ine i a qraph


SLope2
ALi. slohe/a : : 2 / o ouy 1 R? mai mn

Resubik Thr xat congECal ( ) for basR CNao)


catalyse d hy drolusis of eth acerake a t

ma"Lmin.
1R2

Teacher's Signature
reiGtive ui SC oCih of a eniqud u.

Him To DeteY n e the

To SuC

Rotte PPernar

Lor

toD

caRinar

obserahionS Cal(ulaHns
(a)
weight of empry b o t e C o : 1-67

weight of tmph R.D bottle t wt of Jater (wa) o

tof acetone CuwI) : sR o3

Densih of

qid diss

3819
Exkermeat-
Date

Aim Io detriine he latiue uiseacit ofa aiuza


NhSAmeter

*|HppCrctus Reqired SEab atch actala' S viscon¢ter


RkndmRker ipee Hh iquid

eox -ostald' uiscontttr is_a -shahd

bulb A is coanatcte d Liith a fint capilar hR


isLrsad at he _csiilar is connecked wih aa
-Shaked ube RodideA withn a laa blb B|

mainaa thR hydroskcti.c Sxagsre durina los of

ARASrable shRed.
formla2nR tde
F d
ro cedirei

cleaa the siscomtler ith chramic acid s hentui


istmeA LJCtex pint ith altahal or ether s Bhendied
aasceicient ual af disruea Lsadar is intradred bu
pipe the in bulb S,Sa Hhdt beod Rosuthon af Eube s
h ar a ime more than heif of hllbA are

Teacher's Signature
6) Deter mindtion of Jiscocity
+aee n b y Cetone
atn o
Sdo Time toen bu rom A 3
ftoS r om

min o.oS Sec


36 Se
37o sec
min Se
36 4 7 Sec
3

o O1 Se
Meon ime th saten z m i n o07 Sec

uid 36 16 sec

the relahon ,

3 6 6 xo-8o x o
:tadaxnu
td

Poise
n: o.sou830

The loot dist otiu of neaiguid R1


Result
Date:

3
Clamp he isomtter a strrical eositian
Yutbtr uhr _atkached ta sotr arm
thraign ths
sf bulb A. SucKtht
Oer undl ix xise obour thR
upber atrks allo
Fo CloL) undar tS oLan
urigntha liar of loud of
Lsaker from ckn ois mtoagured b
Storrina thR sho
ssa n e Laatch as ha miniseus ius Rasses

|TaL atleagt 4 Fof reading s ith uater s hdn


ük&
Harir mRan ualuR
Tne uater fxom uiscomeler g druit
inbeadure in bulb

loLs of nil as before TaKe GHeast 3-y Yeading SEALe

NDLA uach s dr he fuadmekRr oX R:D bottle & theo Lrigh


mp shen SinitLitn distiltd Lcter &eigh it
ondnaatmaut ht Lstter drtha eiutaamtersshta
nitiim experimtatal iquid s_ighit NaLe this on

Resuit-ne rRlakiue siscocity of thaiquid


LO at xoom a s p i s 0oyR3a Raise

PYecauhong
sa ol of Liaten S of liqui shauld be kaeen insigcomt
Teacher's Signature

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