20 Chemistry Practical Samples-2
20 Chemistry Practical Samples-2
SAMPLES [MSCE]
SUMMER LESSONS
Materials:
Identical evaporating dishes (2), substances A and B (one is covalent and the other
one is ionic but not necessarily in that order), source of heat, spatula.
Procedure:
a. Put a spatulaful of substance A into one evaporating dish and heat it for 1 minute.
Note whether it melts or not and record the results in the table of results.
b. Put a spatulaful of substance B into the other evaporating basin and heat for 1
minute. Note whether it melts or not and record your results in the table of results
Table of results
substance Observation
A
B
From the results, the substance which has melted / melted faster has low melting point
and the one which takes time to melt / does not melt within the time limit given has high
melting point.
Since covalent substances have low melting points and ionic substances have high melting
points, it means that the substance which has low melting point in the experiment is
covalent and the one which has high melting point is ionic.
Materials:
Conducting wires (3), an ammeter, beaker with holed rid, carbon rods (2), power
supply, solutions A and B (one is sodium chloride [common salt] solution and the
other is sucrose [common sugar] solution but not necessarily in that order).
b. read and record the ammeter reading in the appropriate space in the table of results
c. replace solution A with solution B (remember to rinse the electrodes with distilled
water followed by solution B)
d. read and record the ammeter reading in the appropriate space in the table of results
Table of results
Solution Ammeter
Reading
A
B
The solution which registers a reading is ionic and the one which does not register a
reading is covalent. This is so because ionic substances dissociate in water to give out ions
which can conduct electric current while covalent substances do not dissociate in water to
give out ions which can conduct electric current.
If the solution conducts, it means that it is salt and if it does not conduct it means it is
sugar. This is so because salt is ionic and sugar is covalent.
Materials:
Procedure:
a. put sodium carbonate solution in one test tube and lime water in the other
b. set up the apparatus as shown below
c. Add hydrochloric acid (5ml) and 5 drops of litmus solution to the beaker containing
sodium carbonate solution through the thistle funnel and carefully remove the thistle
funnel. The set up will look as shown below
d. observe what happens in the test tubes and record in the table of results
TABLE OF RESULTS
TEST TUBE OBSERVATION
With sodium carbonate solution ,HCl and litmus
solution
With lime water
If the mixture of sodium carbonate, hydrochloric acid and litmus solution turns from red to
colourless, it means that the acid has all reacted (there is no more acid in the reaction
vessel). On the other hand, if the lime water turns milky, it means one of the products of
the reaction is carbon dioxide. The whole process can be represented in an equation form
as follows:
2HCl(aq) + Na2CO3(aq) → 2NaCl(aq) + H2O(l) + CO2(g)
Materials:
Sugar, a tin, tripod stand, wire gauze, a gas or ethanol burner, matches and balance.
Procedure:
a. Weigh the empty tin and record the mass in the table below.
b. With the tin still on the balance, add sugar until the mass increases by
approximately 10g.
c. Record the mass of sugar in the table below.
d. Heat the sugar in the tin until a dry, black solid (carbon) is formed.
e. Weigh the tin + the black substance.
f. Heat and reweigh several times until the mass is constant.
g. Record the mass of tin + carbon in the table of results.
h. Calculate the mass of carbon [(mass of tin + carbon) – mass of empty tin].
i. Record mass of carbon in the table.
TABLE OF RESULTS
item Mass(g)
Empty tin
Tin + sugar
Sugar
Tin + carbon
Carbon
To calculate the percentage composition by mass of carbon in the sugar, the formula below
is used:
Where n means number of moles, m means mass and M means molar mass. The mass of
the carbon is taken from the table of results and molar of carbon is 12g/mol.
SAMPLE RESULTS
Item Mass(g)
Empty tin 30
Tin + sugar 40
Sugar 10
Tin + carbon 34.1
Carbon 4.1
Materials:
Measuring cylinder (100ml), volumetric flask (250ml) with a stopper, distilled water,
standard solution (3M NaOH solution), balance.
Procedure:
a. Find the volume of the standard solution to be diluted to give the molarity required.
i.e. use the dilution formula,
C1 V1 = C2V2
V1 = C2V2/C1
= (2M X 250ml) / 3M
= 167ml
b. Measure the volume of the standard solution found from the calculation (167ml)
using the measuring cylinder.
Materials:
Balance, sodium chloride crystals, beaker (20 cm3), volumetric flask (250 cm3),
distilled water.
Procedure:
a. calculate the mass of the sodium chloride which is going to be contained in 500 cm3
of 0.2M sodium chloride solution by following the steps below:
- Finding number of moles
n NaCl = c NaCl x v NaCl
= 0.2M X 0.5dm3
= 0.1mol
- Finding mass
m NaCl = n NaCl x M NaCl
= 0.1mol x 58.5gmol-1
= 5.85g
b. Weigh 5.85 g of NaCl using the balance
c. Dissolve it using a little distilled water in a small beaker
d. Transfer the solution into a 500 cm3 volumetric flask i.e
e. add distilled water into the volumetric flask up to the mark i.e.
Procedure:
a. calculate the number of moles which is going to be contained in 250 cm3 of 1M
copper sulphate solution by following the steps below:
- find the percentage mass of CuSO4 in the compound:
160/250 х 100% = 64%
- then find the mass of CuSO4 needed to prepare 250 cm3, 1M solution:
n CuSO4 = 1 mol/l х 0.25l = 0.25 mol
mCuSO4 = Mn = 160g /mol х 0.25 mol = 40 g
- if 40g is 64% of the mass of the compound, the mass of the whole
compound will be found as follows
m CuSO4.5H2O = 100/64 х 40 g = 62.5 g
b. Weigh 62.5 g of CuSO4.5H2O using the balance
c. Dissolve it using a little distilled water in a small beaker
d. Transfer the solution into a 250 cm3 volumetric flask i.e.
e. add distilled water into the volumetric flask up to the mark i.e.
Materials:
a burette, clamp and clamp stand, measuring cylinder, conical flask, phenolphthalein
indicator, 0.1M sodium hydroxide solution (NaOH) and hydrochloric acid (HCl) of
unknown concentration.
Procedure:
a. Fill the burette to the mark with the hydrochloric acid (HCl)
b. Record the volume of HCl.
e. Add the HCl gradually, in small amounts, from the burette into the conical flask.
f. Shake the conical flask as the HCl is being added gradually
g. Stop adding the HCl when a colour change is observed in the flask (note that only
one drop of the acid is responsible for the colour change).
h. determine the volume of the HCl used (titre) by subtracting the final volume of the
HCl from the initial volume and record in the spaces below.
Initial volume of HCl = ________
Final volume of HCl = ________
Volume of HCl used (titre) = ________
Where (a) means acid and (b) means base and Va is the volume of HCl used (titre), Vb is the
volume of the base used, which is 10ml, Cb is the concentration of the base, which is 0.1M,
and Ca is the concentration of HCl.
Materials:
a burette, clamp and clamp stand, measuring cylinder, conical flask, phenolphthalein
indicator, sodium hydroxide solution (NaOH) of unknown concentration and 0.2M
hydrochloric acid (HCl).
Procedure:
a. Fill the burette to the mark with the sodium hydroxide (NaOH)
b. Record the volume of the NaOH in the table of results.
c. Measure 10 ml of the 0.2 HCl using the measuring cylinder and transfer it into the
conical flask.
d. Add two drops of phenolphthalein indicator into the conical flask and set up the
apparatus as shown below..
e. Add the NaOH gradually, in small amounts, from the burette into the conical flask.
f. Shake the conical flask as the NaOH is being added gradually
g. Stop adding the NaOH when a colour change is observed in the flask (note that only
one drop of the base is responsible for the colour change).
h. Determine the volume of the NaOH used (titre) by subtracting the final volume of the
NaOH from the initial volume and record in the spaces below.
Initial volume of NaOH = ________
Final volume of NaOH = ________
Volume of NaOH used (titre) = ________
Where (a) means acid and (b) means base and Va is the volume of HCl = 10ml, Vb is the
volume of the base used (titre), Ca is the concentration of HCl and Cb is the concentration
of the base.
na = 1 and nb =1(coefficients of HCl and NaOH in the balanced equation above
respectively)
Materials:
Test tubes (2) in a rack, a measuring cylinder, stirring rod, thermometer, spatula, tap
water and substances A and B.
Procedure:
a. Pour 5 cm3 of tap water into one test tube.
b. Measure the temperature of the water in the test tube and record in the table of
results
c. Add half a spatula of substance A into the test tube and stir gently using the stirring
rod.
d. Measure the temperature of the solution and record it in the table of results.
e. Remove the thermometer from the test tube and rinse it with water.
f. Repeat steps (a) to (d) with substance B.
g. Rinse the thermometer with distilled water, dry and return it into its case.
TABLE OF RESULTS
SOLUTION INITIAL FINAL CHANGE IN TEMPERATURE (0C)
TEMPERATURE (0C) TEMPERATURE (0C) (Final – Initial)
A
B
For the exothermic reaction, the change in heat energy is said to be negative because there
is loss of heat energy to the surroundings (-ΔH). For the endothermic reaction, the change
in heat energy is said to be positive because there is gain of heat energy from the
surroundings (+ΔH).
Note: Be careful when interpreting change in temperature and change in heat energy.
Positive change in temperature (+ΔT) means negative change in heat energy (-ΔH) and
negative change in temperature (-ΔT) means positive change in heat energy (+ΔH).
Energy level diagrams to illustrate the reactions in the solutions of A and B respectively are
shown over below;
When using energy profile diagrams like the ones shown above, the energy change is found
by the formula: ΔH = H2 – H1
Materials:
thermometer, test tubes (2) in a rack, a piece of magnesium ribbon, potassium
hydrogen carbonate or sodium hydrogen carbonate, dilute hydrochloric acid solution,
spatula or tea spoon and a measuring cylinder.
Procedure:
a. Pour 2 cm3 (or 2cm column) of hydrochloric acid into a test tube.
TABLE OF RESULTS
Liquid in the Initial Substance Final temp. Temp. Other changes
tube temp. added reached during change observed during
reaction reaction
Hydrochloric Magnesium
acid ribbon
Hydrochloric Potassium
acid hydrogen
carbonate
or sodium
hydrogen
carbonate
If the final temperature reached exceeds the initial temperature i.e. if the change in
temperature is positive, then the reaction is exothermic (this means heat is released into
the surroundings). On the other hand, if the final temperature reached is less than the
initial temperature i.e. if the change in temperature is negative, then the reaction is
endothermic (this means heat is absorbed from the surroundings).
For the exothermic reaction, the change in heat energy is said to be negative because there
is loss of heat energy to the surroundings (-ΔH). For the endothermic reaction, the change
in heat energy is said to be positive because there is gain of heat energy from the
surroundings (+ΔH).
Note: Be careful when interpreting change in temperature and change in heat energy.
Positive change in temperature (+ΔT) means negative change in heat energy (-ΔH) and
negative change in temperature (ΔT) means positive change in heat energy (+ΔH).
Energy level diagrams to illustrate the two reactions are shown below
Note: ΔH = H2 – H1
Materials:
test tubes in a rack (2), measuring cylinder (5cm3), thermometer, spatula/ tea spoon,
sodium hydroxide pellets (NaOH(s)), hydrochloric acid (HCl(aq), 1M), Ammonium
nitrate crystals (NH4NO3(s)), distilled water.
Procedure:
a. Pour 5 cm3 of distilled water into one test tube.
TABLE OF RESULTS
SOLUTION INITIAL TEMP. FINAL TEMP. CHANGE IN TEMP.
(Final – Initial)
Ammonium nitrate
+ water
Sodium Hydroxide
+ hydrochloric acid
If the final temperature reached exceeds the initial temperature i.e. if the change in
temperature is positive, then the reaction is exothermic (this means heat is released into
the surroundings). On the other hand, if the final temperature reached is less than the
initial temperature i.e. if the change in temperature is negative, then the reaction is
endothermic (this means heat is absorbed from the surroundings).
For the exothermic reaction, the change in heat energy is said to be negative because there
is loss of heat energy to the surroundings (-ΔH). For the endothermic reaction, the change
in heat energy is said to be positive because there is gain of heat energy from the
surroundings (+ΔH).
Note: Be careful when interpreting change in temperature and change in heat energy.
Positive change in temperature (+ΔT) means negative change in heat energy (-ΔH) and
negative change in temperature (ΔT) means positive change in heat energy (+ΔH).
The process that takes place when ammonium nitrate and water are mixed is ionization i.e.
NH4NO3 + H2O →NH4+(aq) + NO3- (aq) and it is an endothermic process. On the other
hand, the reaction between hydrochloric acid and sodium hydroxide will be exothermic.
Energy level diagrams to illustrate the two reactions are shown below;
Materials:
beakers (4), distilled water , a measuring cylinder, sand paper, solutions of copper
sulphate, zinc sulphate, iron sulphate and magnesium sulphate, pieces of copper,
zinc, iron and magnesium metal.
Procedure:
a. Pour about 2 cm3 of copper sulphate solution into each of the four beakers.
b. Clean the copper, zinc, iron and magnesium metals using sand paper.
c. Put a piece of each metal into each of the four beakers containing copper sulphate
solution.
d. Observe the contents of the beakers for 2 to 3 minutes.
e. Record the results in the table below by indicating “Reaction” or “No reaction”.
f. Rinse the beakers with distilled water.
g. Repeat steps (a) to (f) using solutions of zinc sulphate, iron sulphate and magnesium
sulphate, respectively.
TABLE OF RESULTS
Where it is marked reaction, it means the metal has been displaced from solution and is
less reactive than the metal which has displaced it. In this case, copper has been displaced
by 3 metals, iron has been displaced by 2 metals, zinc has been displaced by 1 metal only
and magnesium has not been displaced by any of the metals. It follows, therefore, that
copper is the least reactive and magnesium is the most reactive. The metals can be
arranged in the order of increasing reactivity as shown over leaf.
Materials:
Test tubes (7), HCl (aq) of pH from 1 to 7, Iron nails (7).
Procedure:
a. label the test tubes 1 to 7
b. Put the HCl (aq) of different pHs in respective test tubes.
c. Put the iron nails in all the test tubes
Expectedly, the degree of corrosion will decrease as the pH increases from 1 to 7. But the
increase in pH is a decrease in acidity; hence the degree of corrosion is directly proportional
to acidity i.e. the iron nail will corrode/ rust more if the solution in which it is put is more
acidic.
Materials:
Test tubes (7), NaOH (aq) of pH from 8 to 14, Iron nails (7).
Procedure:
a. label the test tubes 8 to 14
b. Put the NaOH (aq) of different pHs in respective test tubes.
c. Put the iron nails in all the test tubes
d. Leave the test tubes at a safe place for a week.
e. Observe the degree of corrosion / rusting of the iron nails and arrange the test tubes
in order of decreasing corrosion of the iron nail.
Expectedly, the degree of corrosion will increase as the pH increases from 8 to 14. But the
increase in pH is also an increase in basicity; hence the degree of corrosion is directly
proportional to basicity i.e. the iron nail will corrode / rust more if the solution in which it
is put is more basic.
Materials:
Iron nails (3), test tubes (3), distilled water, boiled but cooled water, distilled water,
Anhydrous calcium chloride, cotton wool, oil, glass wool, rubber bung
Procedure:
a. Set up the apparatus as shown below
TABLE OF RESULTS
Test tube Observation
1
2
3
Expectedly, there will be rusting in test tube 1 and no rusting in test tubes 2 and 3. In test
tube 1, there is both oxygen (from the air) and water but in test tube 2, there is no oxygen
and in test tube 3, there is no water.
Hence the necessary conditions for rusting are oxygen and water.
Materials:
Test tubes (4), Iron nails (4), dilute sodium hydroxide, dilute hydrochloric acid, dilute
sodium chloride solution and water.
Procedure:
a. set up the apparatus as shown below
Expectedly, there will be more rusting in the other test tubes; hence acids, bases and salts
affect rusting
Materials:
Universal indicator, test tubes (3), solutions A, B and C
Procedure:
a. Put 2ml of liquid X in one test tube
b. Add 4 drops of universal indicator in the test tube in which liquid X has been put
c. Obverse the colour change and record in the table of results
d. Repeat steps (a) to (c) for the solutions Y and Z
TABLE OF RESULTS
SOLUTION OBSERVATION (COLOUR) ACID/BASE
X
Y
Z
The solution is acidic if the colour changes to either red, orange or yellow; the solution is
basic if the colour changes to either blue, violet or purple and the solution is neutral if the
colour changes to green.
To determine the strength of the acid or base, a pH scale is used. The colour of the solution
is matched against the colour on the scale. The scale is shown below
Colour of Red orange Light yellow green Green Light Dark Violet Purple
universal orange blue blue blue
indicator
Ph 0-2 3-4 5 6 7 8 9 10 11 - 12 13 - 14
Materials:
Test tubes (4), distilled water, bromine solution, sodium hydroxide solution and
phenolphthalein indicator, unknown liquids labeled W, X, Y and Z which are hexane,
ethanol, cyclohexene and ethanoic acid but not necessarily in that order.
Procedure:
a. Perform the tests given in the flow diagram in the figure below and complete the
diagram by filling in the letters W, X, Y and Z in the appropriate boxes.
Materials:
Dilute sodium hydroxide, phenolphthalein indicator and bromine solution in dropper
bottles, four test tubes (in a rack) containing substances P, Q, R and S and distilled
water in a wash bottle.
Procedure:
a. On each substance, perform the tests shown in the table below and record the
observations in the appropriate space. Wash the test tubes after use.