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Heat of fusion and vaporization 10(a) Separate by sublimation Separate iodine from a mixture of
crystals of iodine and sodium chloride. It is accordingly important that an assessment of a student’s
knowledge and understanding of Chemistry should contain a component relating to practical work
and experimental skills. Examples of indicators include; Methyl orange Phenolphthalein Methyl red
Bromothymol blue The pH scale A much more useful measure of the strength of an acid solution was
worked out by the Danish biochemist S. Sorensen. He worked in the laboratories of the Carlsberg
breweries and was interested in checking the acidity of beer. The endpoint should be approached
slowly, a drop at a time. Let the water cool and read the temperature again when the steady stream of
bubbles ceases. Use a magnifying glass to measure temperature values precisely. The electrodes are
connected to a safe DC supply with a small bulb in series. QUALITATIVE ANALYSIS Qualitative
analysis is mainly about identification of substances. Issuu turns PDFs and other files into interactive
flipbooks and engaging content for every channel. Note whether carbon dioxide forms. (ii) Make a
sugar solution and half fill a jar with this solution. Repeat the experiment with other fruit juices and
vinegar. Put 10 mL of molar copper sulphate solution in a small beaker. Add some clear saturated
solution and weigh again, w2. Find the volume of fifty drops by running oil from the burette drop by
drop and counting the drops. You can do this with a rapid spin of a Teflon stopcock or by partially
opening the stopcock and rinsing the partial drop into the flask with a wash bottle. Note that the
thermometer used for calorimetry differs from the less accurate one in your glassware drawer. It can
be used with all abilities and comes with a help sheet (worth ?1) and answers. Since both reactants
and products are colourless, an indicator is used to find the neutralisation point or end point i.e. the
point at which the acid has been neutralised. Marketing Marketing The technical storage or access is
required to create user profiles to send advertising, or to track the user on a website or across several
websites for similar marketing purposes. Test whether the receiver test-tube is full by holding a piece
of red litmus paper at the opening. It is one of the gases responsible for air pollution. Social Posts
Create on-brand social posts and Articles in minutes. Weigh a crucible plus lid, put the pieces of
magnesium ribbon in the crucible and weigh again. Investigate the effect of Universal Indicator on
the solutions above. When cool, weigh the crucible plus lid plus contents. To do this, put 2 or 3 drops
of the reaction mixture into a small test-tube. Write a review Update existing review Submit review
Cancel It's good to leave some feedback. Problems of an investigatory nature, possibly including
suitable organic compounds. Filtration. Identification of ions and gasses as specified in the
curriculum. Instead of using marble chips you can use granulated zinc. Or, if the masses of chemicals
reacting together are known then amounts can be calculated and the balancing numbers deduced
from the amounts reacting together. 2.4 Titration Experiment Titrations can be used to find the
concentration of an acid or alkali from the relative volumes used and the concentration of one of the
two reactants.
Nucleation and growth process of sodalite and cancrinite from kaolinite rich. Disconnect the delivery
tube when you stop heating to avoid a suck back of water onto the hot porous pot. Nucleation and
growth process of sodalite and cancrinite from kaolinite rich. This rise of temperature in not affected
by the volume of 0.2 M copper sulphate used for the experiment. No marks can be awarded for an
incorrect answer without working but a correct method followed by an incorrect answer will receive
credit. All substances should be regarded as being potentially toxic and hazardous. GENERAL
EXAMINATION REQUIREMENTS Apparatus List This list given below has been drawn up in
order to give guidance to schools concerning the apparatus that is expected to be generally available
per student for examination purposes. Every 4 seconds, raise the lid to allow more air to enter but do
not allow any white magnesium oxide smoke to escape. The acid is contained in a thistle funnel and
a tap controls the flow on to sodium sulphite in a suitable flask. Fill a jar (with a screw-on lid) with a
solution of the salt less than saturation strength before you put the seed crystal in position. Drop a 3
mm diameter piece of sodium into the kerosene. See other similar resources ?6.00 5.00 1 review
BUY NOW Save for later Not quite what you were looking for. Within the booklet are a range of
different activities for students to work through to help them remember the content. Check the
quantity of the pipette as indicated on the bulb of the pipette and remember to record it in the
appropriate place. This vapour will break down over the hot porous pot to produce ethene gas and
water vapour. Keep this crystal in place by dropping other crystals on it. After a while, look carefully
for a white ring which will form where the ammonia gas and the hydrogen chloride gas meet after
diffusing through the air towards each other. CALCULATIONS Usually calculations will be
structured. It is accordingly important that an assessment of a student’s knowledge and
understanding of Chemistry should contain a component relating to practical work and experimental
skills. QR Codes Generate QR Codes for your digital content. The volumes stamped on the sides are
approximate and accurate to within about 5%. (c) Graduated Cylinders Graduated cylinders are
useful for measuring liquid volumes to within about 1%. Clocks (or wall-clock) to measure to an
accuracy of about 1s. (Where clocks are specified, candidates may use their own wristwatch if they
prefer) Wash bottle Test tubes (some of which should be Pyrex or hard glass). Moist pH paper No
change Red rose petals No change Specific test A glowing match or wooden spill will relight when
placed in oxygen gas. Support the glass tubing vertically so that the seed crystal at the end is
immersed in the solution of the salt. If you wish to buy ALL Science Required Practicals, click here:
Please Comment if you have found useful. Take care that no drops of liquid are in the neck of the
flask above the mark. At the first sign of burning, place the lid on the crucible and remove the
Bunsen burner. Note the actual temperature of the solutions when cool. Insert the copper wire into
the hole from above and pull it right through the stopper until the screening wire is also pulled a little
way into the hole. Measure the approximate area over which it spreads.
The axes must be clearly labelled with the quantity being plotted e.g. mass and its units e.g.
kilograms The points plotted may be joined with a straight line or a smooth curve. Identify the liquid
as water by its action of turning white anhydrous copper sulphate to blue hydrated copper sulphate.
You may need to lift up on the funnel slightly, to allow the solution to flow in freely. Scrape and
clean the electrodes between each test. (ii) Test ethanol, or methylated spirits, acetone, carbon (IV)
chloride, vinegar, sugar solution, copper (II) sulphate solution, sodium chloride solution, and other
substances dissolved in water. Some useful questions but don't think the risk assessments are that
relevant. To do that, we must use values of relative atomic masses expressed on a periodic table. Put
one drop of lemon juice on to the spot then note any change of colour. QUALITATIVE ANALYSIS
Qualitative analysis is mainly about identification of substances. The residual gas does not support
combustion of a lighted splint. 13 COLOURED EXTRACTS FROM FLOWERS AS INDICATORS
OF ACIDS AND BASES (a) Extract coloured substances from plants Select brightly coloured
flowers, such as the purple and red bougainvillaea, or coloured leaves. Obtain four balloons and blow
them up several times to stretch them. After a while, look carefully for a white ring which will form
where the ammonia gas and the hydrogen chloride gas meet after diffusing through the air towards
each other. The technical storage or access that is used exclusively for anonymous statistical purposes.
This works better than a funnel for the small, 10 mL burettes. One pot synthesis of chain-like
palladium nanocubes and their enhanced electr. Before you take any reading from the burette after
filling it, first allow the solution to run out to fill the tap and jet of the burette, and then you begin
taking your readings. Keep this crystal in place by dropping other crystals on it. The tip should be
clean and dry before you take an initial volume reading. One pot synthesis of chain-like palladium
nanocubes and their enhanced electr. The electrodes should project about 2 cm into the cylinder and
also 2 cm below for attaching the leads to the battery. Ammonia is the less dense gas and the white
ring of ammonium chloride should form nearer to the hydrogen chloride end than from the ammonia
end of the tube. (c) Diffusion of liquids (i) Place a crystal of potassium dichromate, potassium
dichromate (VI), or ammonium dichromate at the bottom of a beaker of water. Deliver solution to
the titration flask by turning the stopcock. Add baking powder in a test-tube with vinegar or lemon
juice (acetic acid). Put 5 mL of bench hydrochloric acid into each of the four balloons and slip the
mouth of the balloon over the top of the tube without letting any acid into the tube. An air flow over
the solution surface given by a fan will also hasten crystal growth. Thanks for looking chalky1234567
300 KS4 AQA GCSE Science Revision Tasks ? 3.00 ( 0 ) This resource is a set of over 300 revision
activities that will enable students to put together their own revision flashcards. PROCEDURE
DURING TITRATION Titrations require continuous shaking of the conical flask and its contents.
Add 3 mL of Fehling’s solution and warm this mixture almost to boiling point. Put pieces of Perspex
or polystyrene in a hard glass test-tube. Tube 2: Put a few pieces of anhydrous calcium chloride or
silica gel in the bottom of a dry test-tube, and also two nails. If two moles are dissolved in 1litre
(1dm 3 ), the resulting solution is 2M and so on.
Repeat the experiment using 30 mL, 20 mL and 10 mL of this sulphate mixed with 20 mL, 30 mL
and 40 mL of distilled water. Used in light bulbs and thermometers because it is not reactive.
Reading from an angle, rather than straight on, results in a parallax error. Calculate the increase in
mass of the magnesium. (b) Substances that lose mass when heated (i) Weigh a test-tube containing 1
cm potassium permanganate crystals and a 1 cm plug of cotton wool at the mouth to prevent loss of
any solid during heating. Thanks for looking chalky1234567 KS4 AQA GCSE Chemistry (Science)
Bonding Revision Knowledge Organiser ? 2.00 ( 0 ) This resource is a 2 page knowledge organiser
covering the bonding content in the 2015 AQA Chemistry specification. Leave in moist air or on a
window ledge for a few days and note the effect of the rust on the longer arm of the lever. The
collecting test-tube must be cooled thoroughly with cold water, as the fumes are harmful. The tip
should be clean and dry before you take an initial volume reading. When all the copper sulphate
crystals have changed to white and the tube has cooled, hold the tube in your hand and pour the
liquid back on to the white crystals. Add some clear saturated solution and weigh again, w2. For
phenolphthalein, the endpoint is the first permanent pale pink. Use a rubber band to attach the tube
containing inflammable and capillary tube to the bulb of a thermometer. The change in temperature is
determined by measuring the initial temperature, T 1, of the reactants, and the maximum
temperature, T 2, of the contents of the calorimeter during the exothermic reaction. Video Say more
by seamlessly including video within your publication. Add 3 mL of Fehling’s solution and warm
this mixture almost to boiling point. You will see the indicator change colour when the titrant hits the
solution in the flask, but the colour change disappears upon stirring. All substances should be
regarded as being potentially toxic and hazardous. The electrodes are connected to a safe DC supply
with a small bulb in series. Don’t pick up tare containers with bare hands since your fingerprints add
mass. It reacts with water to form a weak acid called carbonic acid. The volume of oil put on the
water can be calculated and an estimate made of the thickness of the oil layer, about 10 -6 mm.
When the glass tubing cools, drop seed crystals on its end until one catches in the smaller hole. This
experiment is called the glowing splint test. (iii) Use an L-shape piece of nichrome wire with a shield
to fit on the top to protect your hand. Burettes are used primarily for titration, to deliver one reactant
until the precise end point of the reaction is reached. Show the values that can be averaged to obtain
an acceptable value for use in calculations (only those values within 0.2 cm 3 should be averaged).
This resource hasn't been reviewed yet To ensure quality for our reviews, only customers who have
purchased this resource can review it Report this resource to let us know if it violates our terms and
conditions. In this experiment the concentration of sodium thiosulphate is made variable, whilst the
concentration of acid is kept constant. When hydrogen ignites in a dry test-tube, note any vapour or
mist on the sides of the test-tube. (iv) Investigate whether hydrogen is lighter than air by “pouring”
the gas into a test-tube held either above the first tube or below it. Sodium chloride dissolves readily
in water but not so readily in alcohol DETERMINATION OF DENSITY 9(a) Density of a solid The
density of a solid is the ratio of mass to volume. Boiling point of water We can identify a pure
substance from its melting point or boiling point.