Technical Proposal of Cryogenic Air Separation Unit

（Double-Tower）
1. Device Overview
1. Project overview

According to the friendly negotiation between both parties, the responsibilities are divided as follows:

1.1. Scope of responsibility of the Seller in the boundary area of the air separation unit：

（1） Process design, instrument electrical design, equipment design and engineering design of the air separation unit.

（2） The supply scope of the process equipment is as follows：One self-cleaning filter, one centrifugal compressor, two air precooling

units, one secondary water separator, one molecular sieve purification system (including molecular sieve and alumina), one fractionator

system (including pearl sand), two expansion systems, one liquid nitrogen storage vaporization system, one decompression system,

instrument control system, electrical system, spare parts and special tools used by the above process equipment; see "Scope of Process

Equipment and Instrument" for details。

（3） The installation materials supplied by the seller within the air separation unit area include: process pipelines, cryogenic liquid

pipelines from cold boxes to cryogenic storage tanks, steel structure pipe galleries and brackets, steel structure equipment and valve

maintenance platforms, cable trays, Power cables, instrument cables, instrument root valves, instrument sampling pipes (made of

stainless steel), anti-corrosion and insulation materials, cutting gas, solder and other auxiliary materials required for installation work.

（4） The installation work within the boundary of the air separation unit includes the following: the installation of the equipment

mentioned in serial number (3), the installation of ancillary electrical instruments, the installation of process pipelines, steel structure

pipe galleries and brackets, the installation of steel structure equipment and valve maintenance platforms, Installation of power cables

and instrument cables, installation of cable trays, anti-corrosion insulation work, filling work of molecular sieve purification system

fillers, filling work of pearlescent sand, the insulation material in the cold box, linkage test run work, formal start-up work, flaw
detection, including the above Installation tools required for installation work.

（5） Handover Point：The high and low voltage cable transfer point is bounded by the incoming line end of the seller's high and low

voltage cabinet; the circulating water is connected by the buyer to 1 meter outside the boundary area of the air separation unit; the

product liquid transfer point is at the liquid nitrogen storage tank; nitrogen is the buffer tank in front of the outbound area Interface；

（6） Performance assessment, document delivery, technical services and after-sales services related to air separation units.

（7） Assist the buyer to complete other work related to the air separation unit.

1.2. The buyer assumes the scope of responsibilities within the boundary of the air separation unit：

（1）Responsible for the preliminary survey and detailed survey of the land within the boundary of the air separation unit and the

three connections and one leveling work within the boundary.

（2） Responsible for the civil construction work within the air separation unit area (mainly including pile foundation works, equipment

foundations, workshops, road hardening and greening work, central control room, power distribution room, pipe trenches and cable

trenches), compressor workshops and pump rooms Design, materials and construction of driving and electrical professional lightning

protection and anti-static, factory lighting, equipment lighting and telecommunications, structure, water supply and drainage,

inspection and testing, security monitoring, HVAC and fire protection engineering.

（3） Water, electricity, gas for pressure testing and mechanical materials used for test and start-up of the air separation unit.

The production process of this air separation unit is domestically advanced, and the main equipment uses imported or domestic

advanced products. The unit has many advantages such as high safety, reliable operation, strong operability, and low energy

consumption.
 1.Basic conditions of the device design

Atmospheric conditions design point

atmospheric pressure 96kPa(A)

atmospheric temprature 21℃

relative humidity 78.5%

Atmospheric oxygen content 20.95%O2

Atmospheric temprature

annual temperature 17.8℃

extreme maximum temperature 40.9℃

extreme minimum temperature -15.2℃

Summer average temperature ℃

winter average emperature ℃

seismic intensity 6度（中国烈度）

Sea Level m

Raw material air impurity conditions

 CO2 ≤400 ppm（design point）

SO2 ≤0.44 mg/m3

H2S ≤2.3 mg/ m3

CH4 ≤5mg/ m3

C2H2 ≤1 ppm

CnHm（EXP C2H2 ） ≤5 ppm

DUST CONTENT ≤10mg/m3

Circulating water 循环水

Inlet temp 30℃

Inlert pressure 0.4 MPa(G)

The maximum pressure drop 0.2 MPa(G)

maximum temperature rise 10℃

Cooling water turbidity 12 mg/L

PH 7.2
 Electrical Condition

HV 10,000V±5%三相三线制

LV 380V/220V±5%交流三相四线制

Frequency rate 50±0.5HZ

User for backup instrument air (use on unit start)

pressure 0.5 MPa(G)

temp ≤30 ℃

Dew point ＜-40℃

Flow ～100m3/h

Request 无油
2.Main technical performance parameters

2.1 Yield and purity (out of cold box):

Product Output(Nm3/h) Purity Pressure

（MpaG）
Worki ≤1ppm O2 Dew point：-65℃
ng Nitrogen 3000Nm³/h 0.3
condi
Liquid 50L/h ≤1ppm O2 Dew point：-65℃ 0.6
tion
nitrogen
Note: Nm3/h refers to the volume at 0 ℃ and 101.3KPa (the same below)。

2.2 Equipment operation

Operating cycle (interval between two large heating cycles) ≥2 years

Device heating and thawing time ～36 h

Device startup time (from the start of the expander to the purity ～24 h
index of the nitrogen product)
Range of device load regulation 50～105%
 2.3 Water and electricity consumption table

Cooling
No. Equipment Rated power Shaft power Voltage Remarks
water
（kW） （kW） level（V） volume T/h

1. Raw material air filtration and compression system

1.1 Self-cleaning 1 1 380/220V /

filter
1.2 Raw material 400HP×2 276.32×2 10KV/380 34T×2 2 units
air compressor
2. Hot pry system

2.1 Air pre cooling 2×17.34 2 ×9.85 380/220V 2×9 2 units, 1

unit for use, 1
for backup
2.2 Regenerated gas 33 90 380/220V /
electric heater
3 Total 620.32 2984 380.4

Note: The power of the water pump and cooling tower for production circulating
water is not included in the statistics, and it is shared with the production
circulating water system of Party A.
 3.Process brief

The KDN-3000-50Y air separation equipment adopts a full low-pressure process. The process introduction is as follows:

This device uses product twin towers to produce pure nitrogen process flow

After the raw air has dust and mechanical impurities removed in the filter AF, it enters the centrifugal compressor, which compresses the

air to ~0.83MPaG.

The compressed air enters the precooling unit, is cooled to about 10°C, and then reaches saturation.

The saturated compressed air enters the alternately used molecular sieve adsorber MS, where impure substances such as moisture, CO2,
C2H2, etc. in the raw air are adsorbed by the molecular sieve.

In the nitrogen tower I, the air is separated into medium-pressure nitrogen and liquid air by rectification. After the medium-pressure
nitrogen enters the main exchanger and is reheated, it enters the expander. After expansion, it enters the main exchanger and is reheated,
and then enters the user pipe network as product nitrogen. ; The liquid air is subcooled by the cooler and then throttled into the
condensation evaporator of nitrogen tower I. Most of it is vaporized by the pure nitrogen of nitrogen tower I to obtain oxygen-rich liquid
air and oxygen-rich air, which enters nitrogen tower II to continue distillation. In the nitrogen tower II, low-pressure nitrogen, liquid
nitrogen and liquid air with higher oxygen purity are obtained. After the low-pressure nitrogen is reheated by the cooler and the main
exchanger, it enters the user pipe network as product nitrogen, and the liquid nitrogen is discharged from the cold box as product. After
throttling, the liquid air enters the condensation evaporator of nitrogen tower II and is vaporized by the pure nitrogen of nitrogen tower
II. The obtained oxygen-rich air is reheated by the cooler and main exchanger and then discharged as cold air.
4.Detailed Scope of Supply Self-Cleaning Machine System

原料空气过滤器 Raw air 2set

filter
型 号 Model Self-cleaning

处理气量Processing capacity 100m3/MIN

型 式 Type Vertical arrangement

过滤精度 filter fineness 2μm（保证值 ≥99.99%）

过滤阻损 filtration resistance 保证值P初≤200Pa

loss
防 腐 期 Anti corrosion period ≥2年2 year
自洁系统工作可靠性：脉冲电磁阀.PLC性能可靠，能保证系统长期运
行。
Self-cleaning system reliability: pulse solenoid valve, PLC reliable
performance, to ensure the long-term operation of the system.
过滤器本体（含楼梯平台） Filter body (including stair landing)
就地仪电控制柜（生产厂家成套供货）On-site instrument electrical control cabinet (complete set supplied by manufacturer) 管道.阀门 Pipes,
valves
 空气压缩系统 Air Compressed Sysyem

主空压机
Main Air Compressor 2 Set
制 造 厂 Manufacturer Ingersoll Rand
型 号 Model As design
型 式 Type Water cooling type
压缩介质 Compressed medium 空气air
压缩级数 Compression stage 2级 2level
吸入压力(绝压)
100KPa(G)
Suction pressure(Absolute pressure)
额定排气压力Rated discharge pressure 0.73 MPa(G)
排气量（吸入状态） Exhaust volume(Suction
2700 m3/h
state)
额定功率 Rated power 280kW
各级排气温度 Discharge temperature ≤160℃
冷却后气体温度Cooling gas temperature ≤40℃
润滑油温度 Oil temperature ≤70℃
冷却方式 Cooling mode Water cooling type
水耗 Water Consumption 35T/h
机组重量 Unit weight As Design
机组外形尺寸 Unit dimensions As Design
供货范围（注：以最终厂家实际供货为准） 数量
Scope of supply（Note: Final design shall Qty.
 prevail）
主电机 Main motor 1*2
压缩机本体 Compressor 1*2
电控柜 Electronic control cabinet 1*2
随机备件 Spare parts 1*2
末级冷却器 Final cooler 1*2
图片（注：以厂家实际供货为准，此图片仅供参考）
Picture（Note : The picture for reference only, take material object as
standard）

预冷系统 Air Pre-Cooling System-GAYL-2700/8

Flow Rate流量 2700Nm3/h

Pressure压力 0.73Mpa
Air Inlet Temperature进气温度 ≤40 ℃

Air Outlet Temperature出气温度 ＜10℃

Cooling Water Consumption循环水耗 9T/hr

Shaft Power轴功率 16kW

Refrigeration compressor (Inlet) 制 冷 压 缩 机 1Set

（进口）

Condenser 冷凝器 1Set*2

Evaporator 蒸发器 1Set*2

Internal piping and valves内部管道和阀门 1Set*2

Control System控制系统 1Set*2

Electronic drain电动排水器 1Set*2

Standalone Water Separator独立水分离器 1Set*2

Cabinet 机壳 1Set*2

Manufacturer 生产商 Jia Lian or Shanli

纯化器系统 Air Purification System -HXK-2700/8

纯化器 Air purification system 一套1 Set

制造厂 Manufacturer Youchi
2700m3/h
处理空气量Air flow rate
0.73MPa（G）
工作压力Working pressure
12℃
空气进纯化吸附器温度Suction temperature

4h
切换周期Switching Period
再生气进吸附器温度Temperature of resurgent gas 170℃
inlet adsorber
再生气出吸附器温度Temperature of resurgent gas
100℃
outlet adsorber
电加热器功率Electrical heat power
空气CO2含量：Air CO2 content <1ppm
 供货范围（注：以最终厂家实际供货为准）
数量
Scope of supply（Note: Final design shall
Qty.
prevail）
分子筛吸附筒（含分子筛）Molecular sieve
2
vessel(incl. M/S)
电加热器 Electrical heater 1
过滤器 Filter 1
消音器silencer 1
管道阀门Pipe valves 1
系统阀门及附件System valves and accessories 1
保温材料 heat insulating material SS304
注：以上为一整体撬装框式设计，产品图片仅供参考，以厂家实际供货为准
Note :Above is skid-mounted frame design.The picture for reference only, subject to
the actual supply of the manufacturer.

Fractionation System-FN-3000-300Y分馏塔系统

分馏塔Fractionation column 一套1 Set

制造厂 Manufacturer Youchi

 FN-3000-300Y
型号Model
双塔塔精馏Double column
型式Type

2000×2300×26800mm
外型尺寸Dimension

供货范围（注：以最终厂家实际供货为
数量
准）
Qty
Scope of supply（Note: Final
design shall prevail）
主换热器 Main heat exchanger 2
下塔(含主冷) Lower tower (including main cooling) 1
上塔 upper column 1
过冷器 Sub-cooler 1
冷凝蒸发器Condensation evaporator 2
精馏塔Fractionating column 1
保冷箱Cold box 1
管道及附件piping and accessories 1
Equipment bracket.pipe rack,valve rack设备支架.管架.阀
1
架
楼梯平台stair platform 1
珠光砂 perlite Full
注：产品图片仅供参考，以厂家实际供货为准
Note : The picture for reference only, subject to the actual
supply of the manufacturer.
 Turbo expander System-PLPK-4.67/0.72-0.45膨胀机系统
透平膨胀机Gas bearing turbine expansion 2Set，One use and one preparation 2套，一用
unit 一备
供应商Supplier Xida西达
型号Model PLPK-4.67/0.72-0.45

风动.带可调喷嘴
型式Type
pneumatic with adjustable nozzzle

工作介质Working medium 空气Air

流量Flow rate ～2750Nm3/h
～0.72MPa(A)
进口压力Inlet pressure

出口压力Outlet pressure ～0.45MPa(A)

进气温度Inlet temperature 130K

制动方式Brake mode 风机制动Fan

绝热效率Adiabatic efficiency ≥83%
供货范围（注：以最终厂家实际供货为准）
Scope of supply（Note: Final design 数量Qty.
shall prevail）
透平膨胀机本体Turbo expander 2
膨胀伸缩节Expansion joint 4
膨胀机进气过滤器Expander inlet filter 2
精过滤器Refine filter 1
空气滤清器Air filter 2
消声器Silencer 2
注：与分馏塔一整体框式设计，产品图片仅供参考，以厂家实际供货为准。
Note : Integral frame design with fractionator.The picture for reference only, subject to the actual supply of the manufacturer.

Back-Up System
Cryogenic Liquid Nitrogen

Medium LIN
Volume 170m3
Inlet pressure 15kpa
 Working pressure 16（bar）
Vaporization and voltage regulation
≤55（℃）
equipment
Storage tank booster Sikd 500Nm3/h
Air temperature gasifier 4000Nm3/h
Double-way pressure regulating valve
3000Nm3/h
group

Outlet pressure 0.9Mpa

5. Instrument and control system

5.1 Design principles

1. The control unit shall be able to effectively monitor the production process of the whole device to ensure the long-term, stable and
reliable operation of the device and convenient operation and maintenance.

2. In order to meet the needs of the process, the control unit adopts DCS control, combined with the side panel instrument and local
instrument control, the whole instrument control system to ensure reliable and advanced. The display, trend record, historical event
record, alarm, control, printing, tabulation and flow chart dynamic display of the main process parameters of the complete set are all
completed by the DCS system.
3. DCS control control points (AI, AO, DI, DO, RTD) shall have 15% margin. The upper machine adopts 2 workers
As a station (and operator station), equipped with color liquid crystal display, and through the public network to implement remote
monitoring and operation. The network is under the responsibility of the demander.

4. The analyzer is set in the analysis cabinet for complete sets, and the process parameters for online analysis shall be 4~20mA. DC
enters the PLC system for display, record, alarm, etc.

5. All interlocking circuits are designed according to ISA standard and adopt the principle of power loss and line break safety to ensure
the safe shutdown under the state of power loss and line loss.

6. The power supply of DCS system control system is supplied by UPS uninterrupted power supply, and the capacity is not less than 6KVA,
driving the automatic control system and monitoring workstation, and the backup battery capacity is not less than 30 MINS
(maintenance-free lead-acid battery).
7. Site instrument protection level: not less than IP55 for machinery, and not less than IP65 for electronics. Protection level of local
instrument cabinet: no less than IP20 indoor, not less than IP55 outdoor.

8. Control unit power supply: 220VAC and 24VDC.

5.2 Instrument type selection

name brand

DCS System (JX-300XP)

The UPS has an uninterrupted power supply Supplier (except as indicated by the buyer)

on line analyzer

Pressure, differential pressure, and flow transmitter

Normal temperature control valve, switch valve, switch

butterfly valve

Low-temperature control valve and switch valve

Valve locator, limit switch

Two three-way, two five-way solenoid valve (24V.DC)

orifice meter

Pt100 Platinum thermal resistance, bimetal thermometer, spring pipe pressure gauge

5.3 Scope of supply (Note: excluding the field instruments and control valves of air pre-
quantity
cooling and purification system and cold skid system, the quantity and specifications shall be
subject to the final design and supply)
PLC control system (including I / O cabinet, power distribution cabinet, 224 " color LCD monitor, host,
operation console, various I / O cards, communication card between the compressor, supporting terminal A set
board and communication cable, system software)

UPS uninterruptible power supply (6 KVA, 30 MIS maintenance-free backup battery) A set

On-line analyzer, including:

CO 2 Analyzer (0-10 ppmCO2) A

Dew-point Analyzer (-80~20℃) A

Product (0-10 ppm O 2) A

For zer (0-10 ppm O 2) A

Pressure, differential pressure, flow transmitter (with display head) ~6 Taiwan

Control valve (room temperature, low temperature) ~6 Taiwan

Pt100 Platinum thermal resistance (three-wire system, regas heating temperature and temperature
Four
measurement point in the cold box with double branch)
orifice meter Two sets

Bisetal thermometer, spring pipe pressure gauge A set

Online analyzer cabinet (with pretreatment system, standard gas, etc.) A set

Other instruments (including bimetallic thermometer, pressure gauge, three-valve set, low-temperature
A set
heater)

6. Electronic control system

6.1 Design principles

1. Under the condition of meeting the design and process requirements, the electronic control system must ensure the safe and reliable
operation and convenient operation and maintenance of the equipment.
2. The control, protection, metering and signal devices of motor and other electrical equipment shall comply with the provisions of
relevant national electrical standards or specifications.

3. The high voltage power supply is an incoming line, and the owner is responsible for leading the incoming cable to the receiving end of
the high voltage incoming line switch cabinet.

4. The low-voltage power supply is an incoming line, and the owner is responsible for leading the incoming cable to the receiving end of
the low-voltage incoming line switch cabinet.

5. When the high voltage motor starts, the voltage drop is less than 85%.

6. When the low voltage motor starts, the low voltage bus voltage drop is less than 15%.
 7. Integrated control of instrument and electricity is adopted. The control, operation, interlocking and signal display of the main motor
and electrical equipment are all completed in the PLC system. According to the process needs, set up the machine side operation
(control) box on site, set up the necessary operation elements and signal instructions. The protection level of the outdoor side box is
not lower than IP55.

8. Operation, protection and signal power supply of high voltage switch cabinet adopts dc power screen DC220V, maintenance-free lead-acid
battery.

9. The regas electric heater adopts the control mode of group cutting and single group power adjustment of contactors.

10. The low voltage cabinet has about 10% standby loop except the distribution of electrical equipment provided by the device.

11. There is no reactive power compensation device for high voltage and low voltage, which shall be considered by the superior power
distribution system.
12. The demander shall provide the power grid system diagram, short-circuit capacity and single-phase ground capacitor current value
related to the device within one week after the contract becomes effective.

6.2 Design scope

1. The supplier is responsible for designing the electrical single line diagram, electrical control schematic diagram and terminal diagram
of all the electrical equipment in the nitrogen manufacturing device, and its main ones
The contents include: air compressor, air pre-cooling, purification system, fractionator, expander, process liquid nitrogen pump, standby
liquid nitrogen chain, etc.
2. Equipment layout, power and control wiring, lightning protection, grounding, lighting, and installation materials, supports, etc., as
required by the project

It belongs within the scope of engineering design and the supplier.

6.3 Scope of supply (Note: Quantity and specifications shall be subject to the final design and supply)

brand

10KV inlet line and metering high voltage switch cabinet (including comprehensive guarantee) A set

10KV PT high-voltage switch cabinet A

10KV air compressor running switch cabinet + solid-state soft start cabinet Three sets

direct current cabinet A

Local compensation cabinet A

LV inlet line and feed cabinet Two sets

7. The division of responsibilities between both parties in the on-site gas production mode

responsible party
order project name remarks
number deman supplier
der

one Inspection procedures

1 √
Project approval and construction
application of nitrogen production
The supplier shall provide the required
workshop (if required)
information, including the pressure vessel
2 √ qualification certificate and the
Government safety record of nitrogen
manufacturing workshop (if required) operation certificate of relevant
3 √ personnel, which shall be handled together
Nitrogen production workshop workshop in the name of the demander.
fire control acceptance
4 √
Safety and environmental assessment
related to the nitrogen production
devices
5 √
Handling of the pressure vessel
license in the nitrogen production
workshop
6 √
Handling of the pressure pipeline
license in the nitrogen production
workshop
7 √
License for pressure pipe / container
in the user workshop

two Part of the project

1 √ √
ED
2 √
Plant building, foundation and civil
 construction

3 Nitrogen production workshop, driving, √

lighting, fire, communication

Wind, decoration and other

construction
4 √
The roof of the nitrogen production
workshop is sealed and waterproof
5 √
Procurement and installation of the
nitrogen production device and
equipment
6 √
Main materials and auxiliary materials
installed in the nitrogen production
device
7 √
Nitrogen production device and
equipment transportation, unloading
and positioning
8 √
Commissioning of the nitrogen
production equipment
9 √
Installation and acceptance of
flowmeter to gas point pipeline

three Operation management and equipment

maintenance of the nitrogen production
device
1 √
Responsible for the production safety
of nitrogen production device
throughout the year
2 √
Responsible for the daily gas supply
and operation of the nitrogen
 production unit

3 √
Responsible for the maintenance and
maintenance of the nitrogen production
device and equipment
4 √
Ensure the purity, pressure and
temperature of nitrogen supply
5 √
Training of relevant personnel
6 √
Periodic inspection of the pressure
vessels and pipelines of the nitrogen
production device
7 √
Periodic inspection of the pressure
gauge and safety valve of the nitrogen
production device
8 Supply of vulnerable parts related to √
nitrogen production device
 Supplier supply
Normal temperature and low HangOxytooling, Wuxi KELK
temperature control valve
Supplier supply
locator Azbil.SIEMENS.ABB.YTC
Supplier supply
Solenoid valve (24VDC) ASCO.SMC
Supplier supply
Analyzer complete set Beijing Hankway

Pressure and differential Yokogawa EJA, Rosemount (2051 series) Supplier supply
pressure transmitter with
gauge head
Supplier supply
orifice meter Hangzhou Seiko, Hangzhou throttle, Jiangyin Tower south
Supplier supply
flowrator Anhui Tiankang, Shangziyi, Xiyi, Chengde Delong
Supplier supply
Platinum thermoelectric Anhui Tiankang, on the instrument, Xiyi
resistance, the pressure
gauge
high tension switchgear:
Shanghai Reynol, Changshu Switch Factory, Zhejiang Nankai vacuum
circuit breaker:
Zhongang Electric, Shanghai People, Changshu Switch Factory,
Comprehensive Insurance:
Shanghai Nanzi, Nanrui, Hangzhou Huaguang transformer:
9 Electric control high-pressure section Supplier supply
freshman mutual, Nutek solid state soft rise:
system
Shanghai Reynol, Zhejiang Nankai, Huidi Electric DC screen:
Shanghai Renol, Zhejiang Nankai, Shanghai Eku, Hangzhou
State exhibition
Low voltage switchgear: Shanghai Renor, Changshu Switch Factory,
Zhejiang Nankai, Shanghai Eku, Huidi Electric
low-pressure section Supplier supply
Main components: Reynol, Shanghai People, Changshu Switch Factory