Comprehensive

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Instrument Summary:
Instrument Name: iCAP RQ
Serial Number: Undefined

LabBook Summary:
Path and filename: _Application Data\Workspace\LabBooks\20220416_B2chem practical.imexp
LabBook created by: DESKTOP-T1D935E\iCAP RQ
Based on Template:
Experiment Configuration: iCAP RQ auto
Evaluation: eQuant
Qtegra version (last saved): 2.10.4345.136
LabBook started: 4/16/2022 2:31:51 PM
LabBook finished: 4/16/2022 5:15:40 PM

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Method Summary:
Isotope Mode Dwell time [s] No. of channels Spacing Resolution Internal Standard
7Li STD 0.01 3 0.1 Normal 115In
9Be STD 0.01 3 0.1 Normal 115In
11B STD 0.01 3 0.1 Normal 115In
23Na STD 0.01 3 0.1 Normal 115In
24Mg STD 0.01 3 0.1 Normal 115In
27Al STD 0.01 3 0.1 Normal 115In
39K STD 0.01 3 0.1 Normal 115In
44Ca STD 0.01 3 0.1 Normal 115In
51V STD 0.01 3 0.1 Normal 115In
52Cr STD 0.01 3 0.1 Normal 115In
55Mn STD 0.01 3 0.1 Normal 115In
57Fe STD 0.01 3 0.1 Normal 115In
59Co STD 0.01 3 0.1 Normal 115In
60Ni STD 0.01 3 0.1 Normal 115In
63Cu STD 0.01 3 0.1 Normal 115In
66Zn STD 0.01 3 0.1 Normal 115In
71Ga STD 0.01 3 0.1 Normal 115In
75As STD 0.01 3 0.1 Normal 115In
77Se STD 0.01 3 0.1 Normal 115In
85Rb STD 0.01 3 0.1 Normal 115In
88Sr STD 0.01 3 0.1 Normal 115In
95Mo STD 0.01 3 0.1 Normal 115In
107Ag STD 0.01 3 0.1 Normal 115In
111Cd STD 0.01 3 0.1 Normal 115In
115In STD 0.01 1 0.1 Normal
125Te STD 0.01 3 0.1 Normal 115In
137Ba STD 0.01 3 0.1 Normal 115In
205Tl STD 0.01 3 0.1 Normal 115In
208Pb STD 0.01 3 0.1 Normal 115In
238U STD 0.01 3 0.1 Normal 115In

Isotope Mode Dwell time [s] No. of channels Spacing Resolution

115In STD 0.01 1 0.1 Normal

No. of sweeps Time per sweep [s] Time per main run [s]
10 0.880000000000001 8.80000000000001

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Calibration Curves:

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Standards:
Analysis Index: 7
Analysis Name: 250ppb
Analysis Type: STD
Analysis Started at: 4/16/2022 2:55:17 PM
Standard (Stock): 250 ppb
Standard DF: 1

Category Concentration average Concentration RSD Standard Concentration

7Li 511.073 ppb 500.000 ppb
9Be 5,287.898 ppb 5,000.000 ppb
11B 5,206.818 ppb 5,000.000 ppb
23Na 503.404 ppb 500.000 ppb
24Mg 517.334 ppb 500.000 ppb
27Al 516.578 ppb 500.000 ppb
39K 500.187 ppb 500.000 ppb
44Ca 50,528.593 ppb 50,000.000 ppb
51V 475.899 ppb 500.000 ppb
52Cr 495.476 ppb 500.000 ppb
55Mn 477.099 ppb 500.000 ppb
57Fe 4,888.512 ppb 5,000.000 ppb
59Co 485.844 ppb 500.000 ppb
60Ni 505.384 ppb 500.000 ppb
63Cu 513.775 ppb 500.000 ppb
66Zn 5,886.695 ppb 5,000.000 ppb
71Ga 495.005 ppb 500.000 ppb
75As 5,205.452 ppb 5,000.000 ppb
77Se 6,122.140 ppb 5,000.000 ppb
85Rb 476.843 ppb 500.000 ppb
88Sr 477.056 ppb 500.000 ppb
95Mo 474.433 ppb 500.000 ppb
107Ag 519.159 ppb 500.000 ppb
111Cd 536.150 ppb 500.000 ppb
115In 92.217 %
125Te 623.325 ppb 500.000 ppb
137Ba 485.514 ppb 500.000 ppb
205Tl 492.698 ppb 500.000 ppb
208Pb 508.823 ppb 500.000 ppb
238U 467.786 ppb 500.000 ppb

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Sample List Summary:

Instrument Name: iCAP RQ

Index: Label: Main Survey Start time: User name:

runs: runs:
9 1000ppb 1 0 4/16/2022 3:03:06 PM DESKTOP-T1D935E\iCAP RQ

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Sample Summary
Instrument Name: iCAP RQ

Analysis index: 9
Analysis name: 1000ppb
Analysis started at: 4/16/2022 3:03:06 PM
User name: DESKTOP-T1D935E\iCAP RQ

Category Concentration average Concentration RSD Standard Concentration

7Li 989.963 ppb 1,000.000 ppb
9Be 10,006.461 ppb 10,000.000 ppb
11B 10,078.469 ppb 10,000.000 ppb
23Na 971.982 ppb 1,000.000 ppb
24Mg 984.115 ppb 1,000.000 ppb
27Al 1,010.370 ppb 1,000.000 ppb
39K 988.108 ppb 1,000.000 ppb
44Ca 98,379.103 ppb 100,000.000 ppb
51V 967.950 ppb 1,000.000 ppb
52Cr 962.986 ppb 1,000.000 ppb
55Mn 944.423 ppb 1,000.000 ppb
57Fe 9,384.269 ppb 10,000.000 ppb
59Co 968.743 ppb 1,000.000 ppb
60Ni 966.863 ppb 1,000.000 ppb
63Cu 974.969 ppb 1,000.000 ppb
66Zn 10,459.785 ppb 10,000.000 ppb
71Ga 968.025 ppb 1,000.000 ppb
75As 9,994.202 ppb 10,000.000 ppb
77Se 10,891.234 ppb 10,000.000 ppb
85Rb 968.205 ppb 1,000.000 ppb
88Sr 967.189 ppb 1,000.000 ppb
95Mo 946.280 ppb 1,000.000 ppb
107Ag 997.200 ppb 1,000.000 ppb
111Cd 1,022.598 ppb 1,000.000 ppb
115In 89.056 %
125Te 1,118.793 ppb 1,000.000 ppb
137Ba 960.001 ppb 1,000.000 ppb
205Tl 997.319 ppb 1,000.000 ppb
208Pb 1,032.055 ppb 1,000.000 ppb
238U 971.101 ppb 1,000.000 ppb

Category Concentration Intensity average Intensity RSD

average
7Li 2,002.503 ppb 111,360,791 cps N/A
9Be 19,923.804 ppb 246,540,931 cps N/A
11B 19,916.747 ppb 371,128,788 cps N/A
23Na 2,014.569 ppb 194,370,163 cps N/A
24Mg 2,005.269 ppb 117,128,877 cps N/A
27Al 1,990.974 ppb 152,224,440 cps N/A
39K 2,006.844 ppb 212,627,271 cps N/A
44Ca 200,693.982 ppb 699,227,996 cps N/A
51V 2,027.345 ppb 250,420,360 cps N/A
52Cr 2,019.492 ppb 224,647,024 cps N/A
55Mn 2,037.963 ppb 386,537,658 cps N/A
57Fe 20,373.119 ppb 84,738,657 cps N/A
59Co 2,022.586 ppb 260,441,300 cps N/A
60Ni 2,017.519 ppb 52,978,039 cps N/A
63Cu 2,009.455 ppb 126,837,551 cps N/A
66Zn 19,481.092 ppb 436,160,460 cps N/A
71Ga 2,020.463 ppb 185,005,186 cps N/A
75As 19,956.763 ppb 417,647,766 cps N/A
77Se 19,188.460 ppb 35,867,950 cps N/A
85Rb 2,026.393 ppb 367,432,612 cps N/A
88Sr 2,027.745 ppb 503,221,210 cps N/A
95Mo 2,038.854 ppb 81,694,470 cps N/A
107Ag 1,997.519 ppb 216,829,633 cps N/A
111Cd 1,979.120 ppb 54,582,854 cps N/A
115In 82.694 % 1,262,512 cps N/A
125Te 1,909.451 ppb 10,101,318 cps N/A
137Ba 2,030.282 ppb 80,518,259 cps N/A
205Tl 2,008.397 ppb 553,163,890 cps N/A
208Pb 1,985.298 ppb 357,378,998 cps N/A

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Category Concentration Intensity average Intensity RSD

average
238U 2,029.801 ppb 1,077,285,286 N/A
cps

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