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Separation of Turpentine Oil

The document describes an experiment to separate turpentine oil from a water-turpentine oil mixture using steam distillation. Key steps include adding the mixture to a flask, heating it with steam, collecting the condensate, separating the oil and water layers, measuring weights, and calculating recovery ratios and efficiency. Observations and calculations are presented, and a bar graph compares simple and steam distillation methods.

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Unnati Patel
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235 views4 pages

Separation of Turpentine Oil

The document describes an experiment to separate turpentine oil from a water-turpentine oil mixture using steam distillation. Key steps include adding the mixture to a flask, heating it with steam, collecting the condensate, separating the oil and water layers, measuring weights, and calculating recovery ratios and efficiency. Observations and calculations are presented, and a bar graph compares simple and steam distillation methods.

Uploaded by

Unnati Patel
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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bottomed flask

placed in the 250 ml round


Steam Distillation
turpentine oilis
1. Fifty mlof is added to the
above flask. remaining
2. 100 ml of water flask) is filled with water. The
round bottom
3. The steam-can (or shown in Figure 9.
assembling is done as simultancously, so that steam flows
flask are heated
4. Both the stem-can andmixture.
uniformlythrough the
After sometime it starts boiling.
5. The mixture gets heated. occurs is noted.
which boiling
6. The temperature (T; "C)atof oil and passes into the condenser where condensation
7. Steam carries the vapours
takes place.
into the receiver.
8. Condensate (50 ml) is collected funnel.
9. Oil is separated from water using separating
water (w)) layers are noted.
10. The weights of turpentine oil (w2) and (wlw;) is calculated and reported.
recovery ratio of oil and water as
11. The practical distillation on x-axis and boiling point
12.A bar graph is plotted taking method of
J-axis.

OBSERVATIONSAND CALCULATIONS
pure turpentine oil by simple distillation= I60 (T, °C)
1) Boiling temperature of by steam distillation = 1 (T °C)
2) Boiling temperature of the mixture
Decrease in boiling point, T;=(T-T;) 63 °C
3) turpentine oil to water = 1.32:1
4) Theoretical recovery ratio of
g= 25 6 4
5) Weight of water obtained = wi g= IS. 8
6) Weight of turpentine oil obtained = W2oilto water =o. 6|66
turpentine
7) Practical recovery ratio of distillation=
8) Percent efficiency of steam
(Practical recovery) x 100
Theoretical recovery eaaated om mixtue
ecl u
REPORT
JTwpti
ny o team dia'lation 46. 7|%
The puunte
QUESTION BANK

1. List the applications of steam distillation distillation with a suitable example.


2. Describethe principle involved in the steam
3. Define distillation and steam distillation.
Cal elallon

W 5.8 o. 6 |66
25.6 4
W

lucnt yiiny og tam di'latk,


Pacal secove
Thesu i cal ecoey
O.6l66 XOo
|. 3

46. 7!/o
Compandion op aimple and Mea
ditialon mthod
Date:24 o
24

23
22o24
22
Sca
21

20

19

18

17

16

15 T

14

13

12

11

10

8 O

MMh atn
1 2 3 4 5 6 7 8 14 15 16 17 18
9 10 11 12 13

Lalwani's
AIM

To separate turpentine oil from water-turpentine oil mixture by


distillation process.

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