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ABSTRACT:
A herbal soap and hand sanitizer was formulated using the leaf and bark extract of Azadirachta indica, Ocimum
tenuiflorum, Sapindus mukorussi and Acacia concinna powder. Ayurvedic cosmetics are also known as the herbal
cosmetics the natural content in the herbs does not have any side effect on the human body most herbal
supplement are based on several botanical ingredients with long histories of traditional or folk medicine usage.
Among the numerous botonical ingredients available in the market today. Numerous chemical toxins
microorganism present in the atmosphere may cause chemical infection and damage to skin cosmetics alone are
not sufficient to take care of skin and body parts. Neem (Azadirachta indica) tree has attracted worldwide
prominance owing to its wide range of medicinal properties, neem leaves and its constituents have been
demonstrated to exhibit anti-inflammatory, antihyperglycemic, antiulcer, antimalarial, antifungal, antibacterial,
antimutagenic and anticarcinogenic properties. This study was conducted to evaluate the effect of aqueous,
ethanolic and ethyl acetate extract from neem leaves. Herbal soap ingredients were used reetha, neem, shikekai
and tulsi., in which neem leaf and seed were found effective against some dermatophytes. Shikeki and Reetha
acts as a detergent andhaving cleaning and foaming activity and Tulsi shows antiviral activity.
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*Herbal soap preparation is a medicine or drugs it contain Antibacterial and antifungal agents which mainly uses
of part of plants such as like leaves, stem, roots andfruits to treatment for a injury or disease or to achieve good
health6. This preparation possess antimicrobial property are administered topically and available to apply in
various forms like creams, lotion gel, soap, solvent extract or ointment. The variety of creams and soap properties
have been used to treat various skin disorders7. Mostly skin infection are caused by fungi, staphylococcus aureus
and streptococcus species6. Ethnomedically, juiceand extract from leaves of the plants are topically applied as
antimicrobial and anti-inflammatory agents in treatment of skin disease including eczemas, ringworm and
pruritus8. The succulent gel form is used to disorders of psoriasis. Crude preparation of soapy plant are able to
soften the skin epidermis enhance greater penetration and cleaning acne and also promote healing and resolution
in quickly in time.
In this review article herbal soap containing neem, tulsi, shikekai and reetha as natural plant ingredients and this
content gives or shows antibacterial antifungal and anti-inflammatory activity. In this soap, neem is main
compound, and shows medicinal properties. Neem leaf and its extract exhibit immunomodulatory anti-
inflammatory, antiulcer antimalarial, antifungal antibacterial antioxidant anticarcinogenic property. Tulsi has got
the greatest medicinal value. tulsi to be effective for diabetis they reducing blood glucose level tulsi also used in
severe acute respiratory syndrome. Juice of its leaves gives relief in cold fever bronchitis and cough. Tulsi reduce
stress, enhancestamina relief inflammation and also shows antifungal activity so tulsi is also used as main
compound in this herbal soap. The main antifungal activity of Tulsi serves to be beneficial in soap formulation9.
Reetha is an exceptional cleanser. Hence it’s a perfect substitute for soap and facewash due the presence of
saponin. It is also good for use on sensitive skin. A combination of Reetha and Chickpeas gives a gentle and
enriching experience to the skin it has conditioning properties, therefore, it keeps skin moisturized and cool.
Reetha prevents the skin from drying and keeps it soft and supple it also helps to treat eczema and psoriasis.
Shikekai is quit effective in treating various skin infection like scabies and also used as a antiwrinkles property9.*
In ancient time the written information on ayurveda like charaka samhitha and varnya kashaya has explained the
usage of herbs in getting glowing complexion. The herbs used were chandana, nagkeshara, padmak, khus,
yashtimadhu, manjistha, sariva, payasya, seta (sweta durva) and lata (shyama durva). These ayurvedic herbs are
used to purify blood and eliminate vitiated doshas like (vata, pitta, kapha) from the body as they are mainly
responsible for skin disorders and other diseases. The herbs mentioned in khushthagna mahakashaya effective in
skin disorders, include khadira, abhaya, amalaki, haridra, bhallataka, saptaparna, karavira, vidanga and jati. Some
of the natural products used in ancient times include, the use of indigo and raktachandan as bindi/tika, madder
root for beautifying lips and cheeks, aloe as skin protectant, chandan, vetiver and haldi as face packs. The use of
ayurvedic herbs adds cosmetic value to the products. The ayurveda is well known for the permanent cure for
ailments and it is likely evident from the present market trends that the herbal cosmetic product will succeed in
capturing the market. The knowledge about the structure and basic function of the skin and its appendages and
knowledge of natural or herbal care or remedies for its problems will help to widen the importance of herbal
cosmetics. The skin hasthe natural ability in continuously repairing to maintain its normal function. In young age
the common skin problem are greasy skin and acne and during old age the skin becomes dry. To have a better
skin, it is important to understand how our skin functions and to take proper precautions to maintain it. The skin
are classified into 4 groups and for each class appropriate ingredients should be used to maintain its natural
functionality (Table - 1) 10-11.
Herbal soap
Herbal soap preparation is a medicine it contain antibacterial, anti-ageing anti-oxidant, anti-septic properties
which mainly uses of part of plant like seeds, rhizomes, nuts and pulps to treatment for an injury or disease or to
achieve health.[5] Herbal soap do not contain the artificial colours,flavours, fluorides etc., when compared to the
content of commercial soap.[6] Herbs are the natural productsmostly found in the treatment of almost all diseases
and skin problems owing to their high medicinal value, cost effective ness, availability and compatibility.[7]
SOAP
Soap is common cleansing agent well known to everyone. Many authors defined soap indifferent ways. Warra,19
regarded it as any cleaning agent, manufactured in granules, bars, flakes, or liquid form obtained from by reacting
salt of sodium or potassium of various fatty acids that are of natural origin (salt of non-volatile fatty acids). Soap
can also be said to be any water-soluble salt of fatty acids containing eight or more carbon atoms. Soaps are
produced for varieties of purpose ranging from washing, bathing, medication etc. The cleansing action of the soap
is due to the negative ions on the hydrocarbon chain attached to the carboxylic group of the fatty acids20. The
affinity of the hydrocarbon chain to oil and grease, while carboxylic group to water is the main reason soap is
being used mostly with water for cleaning purposes21.
In addition to basic raw materials, other substances are added to the composition in order to improve its
application. For examples soap made for medicinal purposes other medicinal importance ingredients are added
to it to produce medicated soaps22. In addition to potassium and sodium salt, other metals such as calcium,
magnesium and chromium are also used to produce metallic insoluble soap that are not used as cleaning agents,
but are used for other purposes22. Other properties of the soap such as hardness are function of the metallic
element present in the salt. For example soap made up of Sodium salts shows little hardness compare to
potassium salts soaps, provided the same fat or oil is used in both cases23. These are characteristically different
from soaps made from divalent metals such as magnesium, calcium, aluminum or iron which are not water
soluble, Soaps are use for laundry and cleaning purposes, though the used of calcium soap in the formulation of
animal feed have been reported 24. It is generally known that soap is produced by the saponification of a
triglyceride (fat or oil). In the process the triglyceride is reacted with a strong alkali such as; potassium or sodium
hydroxide to produce glycerol and fatty acid salts.
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The Discovery and the Art of Soap-making up to 1660. Soap, in the sense of the product obtained by the action of
a base on fats and oils, has played an important part in the history of civilization, but its discovery was quite
accidental and its usefulness but slowly appreciated. It is quite impossible, therefore, to follow the lead of Liebig
and others and try to assess past civilizations by reference to their knowledge or ignorance of soap. Were it
otherwise, the Fanti of West Africa and the Gauls of the first century A.D., who apparently discovered soap
independently, had reached a higher degree of civilization than the Egyptians or the Greeks, to both of whom
soap was unknown.
Both the Egyptians and Greeks, however, were acquainted with medicinal preparations in which alkalis, tallow
and various vegetable oils were present, together with several other ingredients. The Papyrus Ebers records the
use of such ointments for herpes and for removing fat round the eyes25. Many kinds of lead plasters were also
known. Again, the Berlin Papyrus gives instructions for making an ointment with natron and tallow27, and
Hippocrates used mixtures of oil and soda as ingredients of purgatives26. According to early manuscripts the
Assyrians used a mixture of castor-oil and alkali as a head wash27 In addition to this knowledge the proparation
of alkaline lyes from the ashes of plants was well known to nearly all nations from very early times; but their use
in the manufacture of soap appears to have taken place at any rate not earlier than the Christian era.
Skin
Skin is very important for all health care professionals to have basic information about the structure and function
of human skin. Skin is also called cutaneous membrane. In adults the skin has a surface area rangingfrom1.2
to2.2m2. Skin has two types, hair -bearing skinthat coversmuchof the body and hairless skin as that of palms
ofHands and so les of feet.[1] Skin is the most exposed part of the body to the sunlight, environmental pollution
and also used to some protection against the pathogen.
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Extraction:
The Azadiricta indica, Ocimum tenuiflorum, Sapindus mukorossi and Acacia concinna powder was extracted with
water by decoction process. 9 gm of above stated powder was taken in conical flask and extracted with water for
four hours with occasional agitation. Then filtered.
Formulation of herbal soap:28
To obtain extract of Azadiracta indica, Ocimum tenuiflorum, Sapindus mukorossi and Acacia concinna powder was
incorporated into a soap formulated with basic glycerin soap and which contain 1 gm stearic acid, 0.70gm soft paraffin.
Weighed 1gm of stearic acid, 0.70gm soft paraffin, 5ml ethanol was taken. Glycerin basic soap was melted first and to it 1gm
stearic acid, 0.70gm soft paraffin, 5ml ethanol were added. Extract was incorporated into melted solution with continuous
agitation for 30 minutes until molten mixture became homogeneous. The semisolid mixture was poured into a mould and
allowed to solidify.
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Neem
Botanical name:Azadiracta indica
Color: Green
Description: Compound alternate, rachis 15-25cm long, 0.1cm thick, leaflet with oblique, serrate, 7-8.5 cm long and 1-1.7
cm wide slightly yellowish green in color.
Constituents:- Flavonoids, Alkaloids, Azadirone, Nimbin, Nimbidin, Terpenoids, Steroids, Margosicacid, Vanilic acid,
Glycosides, B-sitosterol, Nimbectin, Kaempeerol, Quercursertin are present in Neem Leaf
TULSI
Botanical name: ocimum tenuiflorum
Color: Green
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RITHA
Botanical name: sapindus mukorossi
Colour: Brown
Description:- The fruit is a small leathery skinned drup 1 to 2 cm in diameter, yellow ripening blackish , containing 1 to 3
seeds
SHIKEKAI
Biological name:- Acacia concinna
Colour:- Brown
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Evaluations30,31
The herbal soap formulated was evaluated
1. Organoleptic evaluation:
i. Colour: brown
2. Physical evaluation32,33
The herbal soap formulated was evaluated for the following properties:
a) pH: the pH was determined by using pH paper, the pH was found to be basic in nature
b) Foam retention: 25ml of the one percent soap solution was taken into a 100ml graduated measuring cylinder the cylinder
was covered with hand andshaken 10 times. the volume of foam at 1 minutes interval for 4 minutes was recorded. it was
found to be 5 minutes.
d) Antimicrobial test: there was various study conducted on antimicrobial activity of neem and hence according to research
paper by antimicrobial activity of Azadiricta indica leaf, bark and seed extract.
CONCLUSION:
The plant Azadiricta india, Ocimum tenuiflorum, Sapindus mukorossi and Acacia concinna were extracted using water and
subjected to various evaluation test according to previous research the antimicrobial activity of Neem was studied. the
prepared formulation when tested for different test gave good results. It does not give any irritancy to skin it was determined
by using these soap by few volunteer hence it is proved that soap does not give any irritancy to skin. Furthermore the
prepared soap were standardized by evaluating various physico chemical properties such as pH appearance odour in which
the exhibit satisfactory effect.
ACKNOWLEDGEMENT
It is great pleasure for us to undertake this project. We feel highly doing the project entitled- “Formul ion nd evaluation of
polyherbal soap”.We sincerely express our deep sense of gratitude to The Management, Sree Abirami Institutions and
Charitable Trust for providing the required facilities regarding this research and also for their support. We are highly
indebted to Dr. M. Senthil Kumar, Principal, Sree Abirami College of Pharmacy who is our inspiration to pursue this
undertaking. We are also obliged to our mentor and colleagues. This work would not have been possible without their
worthy experience and enormous help.
REFERENCES:
1. Hughes, G.R., J.Soc. Cosmet. Chem., 1959, X, 159.
3. Kapoor.V.P., Herbal Cosmetics for Skin and Hair Care, Natural Product Radiance, p 306-314.
4. Harry R.G, In: Modern Cosmeticology, Vol 1(Revision Eds), Wilkinson J.B., Clark.R., Green E., Mclaughlin T.P., 1962,
Leonard Hill (Books) Ltd, London.
JETIR2212444 Journal of Emerging Technologies and Innovative Research (JETIR) www.jetir.org e326
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5. Sankholkar.D.S, Current Regulations and Suggested Way Forward, The Pharma Times, Vol.41, No.8,2009, p 30-31
6. Kareru, P. G., Keriko, J. M., Kenji, G. M., Thiong’o, G. T., Gachanja, A. N., and Mukiira, H. N. (2010). Antimicrobial
activities of skincare preparations from plant extracts. African Journal of Traditional, Complementary and Alternative
Medicines, 7(3).
7. Bandyopadhyay, U., Biswas, K., Sengupta, A., Moitra, P., Dutta, P., Sarkar, D., ... and Banerjee, R. K. (2004). Clinical
studies on the effect of Neem (Azadirachta indica) bark extract on gastric secretion and gastroduodenal ulcer. Life Sciences,
75(24), 2867-2878.
8. Sharma, J., Gairola, S., Sharma, Y. P., and Gaur, R. D. (2014). Ethnomedicinal plants used to treat skin diseases by Tharu
community of district Udham Singh Nagar, Uttarakhand, India. Journal of Ethnopharmacology, 158, 140-206.
9. Kapoor, V. P. (2005). Herbal cosmetics for skin and hair care.4(4). 306-315.
10. Charaka Samhita, Handbook on Ayurveda, Editor, Gabriel Van Loon, 2002-2003 Vol 1.
11. Prashant, L., Kole et al, Cosmetics potential of herbal Extracts, natural Product Radiance, Vol 4(4), 2005, p 315-321.
12. The Wealth of India: A Dictionary of Indian raw Materials and Industrial products- Raw materials Series, Publication and
Information Directorate, CSIR, New Delhi, Vols I-XI, 1948-1976; Revised Series IA, 1985; 2B, 1988; 3 Ca-Ci, 1992.
13. Chopra R.N., Nayar S.I., Chopra I.C., Glossary of Indian Medicinal Plants, Publications and Information Directorate, CSIR,
New Delhi, 1956.
14. D’Amelio F.S, Sr, In: Botanicals A Phytocosmetic Desk Reference (Ed. FS D’Amelio, Sr), 1999, CRC Press, London.
15. Kumar S, Medicinal Plants in Skin Care Director, Central Institute of Medicinal and Aromatic Plants, Lucknow, 1994.
16. Thakur R.S., Puri, H.S., Hussain, A, In: Major Medicinal Plants of India, 1989, CIMAP, Lucknow.
17. The British herbal Pharmacopoeia, British Herbal Medicine Association, 1996.
18. Ceres A, The healing power of herbal teas. Thorsons Publishers, London, 1984.
19. Warra, A. A. (2013) Soap making in Nigeria using indigenous technology and raw materials, African Journal of Pure and
Applied Chemistry, 7(4): 139-145
20. Okeke, S. U. N. (2009) Home economics for schools and colleges, Onitsha: Africana First publishers Plc Nigeria
21. Adaku, U. and Melody, M. (2013) Soap Production Using Waste Materials of Cassava Peel and Plantain Peel Ash as an
Alternative Active Ingredient, Implication for Entrepreneurship, IOSR Journal of VLSI and Signal Processing,3(3): 2319 – 4197
22. Antezana, W., Calve, S., Beccaccia, A., Ferrer, P., Blas, C. D., Rebollar, P. G. and Cerisuelo, A. (2015) Effects of nutrition
on digestion efficiency and gaseous emissions from slurry in growing pigs: III. Influence of varying the dietary level of calcium
soap of palm fatty acids distillate with or without orange pulp supplementation, Animal Feed Science and Technology, 209:
128-136
23. Phanseil, O. N., Dueno, E. and Xianghong, W. Q. (1998) Synthesis of exotic soaps in the chemistry laboratory, Journal of
Chemistry Education, 75(5): 612
24. Kuntom, A., Siew, W. L. and Tan, V. A. (1994) Characterization of Palm acid oil, Journal of American Oil and Chemical
Society, 71: 525-528
25. C. P. Bryan, The Papyrus Ebers, London, 1930, 12, 139, etc.
26. J. R. Partington, Origine and Development of Applied Chemistry, London, 1933, 198.R. vun Grot, Historische Studion
aus dem Phannabologischen Institut, Hallo, 1889, i, 94
27. R. C. Thompson, Assyrian Herbal, London, 1924, 191, 270. Pliny, Natural History, lib. XXVIII, emp. 51.
28. Panda, H. (2011). Herbal soaps and detergents handbook. NIIR Project Consultancy Services
JETIR2212444 Journal of Emerging Technologies and Innovative Research (JETIR) www.jetir.org e327
© 2022 JETIR December 2022, Volume 9, Issue 12 www.jetir.org (ISSN-2349-5162)
29. Reddy, Y. R. R., Kumari, C. K., Lokanatha, O., Mamatha, S., and Reddy, C. D. (2013). Antimicrobial activity of Azadirachta
Indica (neem) leaf, bark and seed extracts. Int. J. Res. Phytochem. Pharmacol, 3(1), 1-4.
30. Joshi, M. G., Kamat, D. V., and Kamat, S. D. (2008). Evaluation of herbal Handwash Formulation.7 (5), 413-15.
31. Kumar, K. P., Bhowmik, D., Tripathi, K. K., and Chandira, M. (2010). Traditional Indian Herbal Plants Tulsi and Its
Medicinal Importance. Research Journal of Pharmacognosy and Phytochemistry, 2(2), 93-101
32. Afsar, Z., Khanam, S., and Aamir, S. (2018) Formulation and comparative evaluation of polyherbal preparations for their
Disinfectant Effects, 1 (1), 54-65.
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