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PR 08 CHE XII SALT NH4Cl

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17 views3 pages

PR 08 CHE XII SALT NH4Cl

Uploaded by

heroimastersandip
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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|CHEMISTRY| PRACTICAL NOTES

Expt. No- Date-

Identification of cation & anion of the given


unknown salt
Aim of Experiment- To identify the cation and anion present in a given salt.

Salt number:

Colour: White

Structure: Crystalline

Solubility: Cold water

Dry test for basic radicals

 Test tube heating:

Experiment Observation Inference


+
A pinch of salt was taken in a A white sublimate was NH4 may be present.
clean and dry test tube and it formed at the cooler part of
was heated strongly. the test tube.

 Soda lime Test:

Experiment Observation Inference


+
A pinch of salt was taken in a A strong smell of ammonia NH4 may be present.
dry test tube soda lime was was observed.
added to it.
Dry test for acid radicals
I. Dilute H2SO4 test

Experiment Observation Inference


A pinch of salt was taken in a No effervescence took place. CO32-, SO32-, S2-, NO2- were
clean & dry test tube. Then absent.
2ml of dil. H2SO4 was added
to it.

II. Conc. H2SO4 test

ODM Educational Group Page 1


|CHEMISTRY| PRACTICAL NOTES

Experiment Observation Inference


The given salt was taken in a Effervescence took place Cl- may be present.
clean & dry test tube. Then with the evolution of a gas
1ml of Conc. H2SO4 was having pungent smell. White
added to it. fumes were produced when
a glass rod dipped in NH4OH
was shown to the evolved
gas.

III. MnO2 test

Experiment Observation Inference


-
A pinch of MnO2 was added Greenish-yellow gas was Cl may be present.
to the above test tube & evolved.
heated

Wet test for acid radicals


 Chromyl chloride test

Experiment Observation Inference


-
The given salt solution was  Yellowish orange cl may be
mixed with three times its vapors evolved. confirmed.
weight of K2Cr2O7 and 1ml  Yellow ppt. was
Conc. H2SO4 was added to it obtained.
and heated. The evolved gas
was passed through NaOH
solution followed by
acidification with acetic acid
and about 2ml of lead
acetate solution was added.
 Silver Nitrate test

Experiment Observation Inference


-
2ml of salt solution was A white ppt. was formed cl is confirmed.
acidified with dil.HNO3 and 1 which was soluble in dil.
ml of AgNO3 solution were HH4OH solution.
added to it.

ODM Educational Group Page 2


|CHEMISTRY| PRACTICAL NOTES

(Chromyl chloride)

Wet test for basic radicals

Experiment Observation Inference


1. NaOH solution was A smell of ammonia comes NH4+ is confirmed.
added to the salt and out and white fumes of
it was warmed. A NH4Cl are formed.
glass rod was dipped
in the HCl and was
shown to the mouth
of the test tube.
2. NaOH was added to A reddish brown ppt. was NH4+ is confirmed.
the solution & then formed.
Nessler’s reagent was
added.

(Reddish brown)

Conclusion

The given salt contains anion Cl- & cation NH4+

ODM Educational Group Page 3

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