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Chem Lab Exp1

Diploma sem 1 lab exp 1

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Swarup Mondal
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33 views1 page

Chem Lab Exp1

Diploma sem 1 lab exp 1

Uploaded by

Swarup Mondal
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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lXPf RIM[ NT NO I (a)

Narni.' ot r~peri111e 111 Prepara1ion of Standard Oxalic acid Solut ion

theor, Formula of oxalic acid C1H10, 2H10

Molecula1 we1gh1 of oxalic acid ; (2xl2+2xl+4xl6+2xl8) gm=l26 gm


Solution of one lit re oxalic acid Con tains one gm molecular weight of l he substance.

To prepare 0.1 (M) oxalic acid solution 12.6 gm of crystal oxalic acid is required.

Necessary equipmen ts and chem icals:

1) Chemical balance
11) Watch glass
iii) Weigh t box
iv) Volumetric flask (1000ml)
v) Glass rod
vi) Wash bottle
vii) Funnel
viii) Oxalic acid
ixl Distilled wa ter
amoun t of clean and dried
Procedure: Take a watch glass, wash it with distilled water and dry It, weight of the exact
acid and record this
watch glass and record its nole book. Weigh t correctly on the watch glass 12.6 gm of oxalic
watch glass into a clean and
weight in the note book. Using a funnel, transfer oxalic acid softly and Carefully from the
slick to it into the foam
dry volumetric flask. Wash the watch glass with distilled wa ter to move the particles that
sticking Particles into the
with the help of a wash bottle. wash funnel several times with distilled water. To move the
to the volumetric fla sk
measuring flask using wash bottle, using wash bottle, thoroughl y add enough distilled water
until lower meniscus level just
just below the etched mark on It. Add few ml of distilled water drop into the flask
solution uniform.
touches the mark. Put the stopper on the mouth of flask and shake softly to make the entire

Observation:

weight of watch glass weight of watch glass ➔ W, gm

Weight of watch glass+ oxalic acid ➔ (W, +12.6} gm

weight of oxalic acid ➔ 12.6 gm.

volume of the solution ➔ 1000 ml. (oxalic acid+ distilled wate r)

Resul t 1000 ml O.l (M) solution of oxa lic acid in prepared.

Precaution

I) weighine of oxalic acid crystals need weigh ts of (10 g+2g+SOO mg+ 100 mg).
watch glass.
2) wash the wa tch glass carefully so that even a Single crystal of oxalic acid is not left on the
of distilled waler above
3) l,;sl few drops of distilled wa ter should be added hy using d ropper to avoid extra addition
the mark on the neck of the volumetric flask

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