INTERNATIONAL IS0

STANDARD 10123
First edition
1990-l 2-01

Adhesives - Determination of shear strength of

anaerobic adhesives using pin-and-collar
specimens

Ad/&ifs - DHermination de /a r&sistance au cisaillement des ad/-&ifs

anakobies SW- assemblage type axe-bague

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Reference number
IS0 10123:1990(E)
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 IS0 10123:1990(E)

Foreword

IS0 (the International Organization for Standardization) is a worldwide

federation of national standards bodies (IS0 member bodies). The work
of preparing International Standards is normally carried out through IS0
technical committees. Each member body interested in a subject for
which a technical committee has been established has the right to be
represented on that committee. International organizations, govern-
mental and non-governmental, in liaison with ISO, also take part in the
work. IS0 collaborates closely with the International Electrotechnical
Commission (IEC) on all matters of electrotechnical standardization.

Draft International Standards adopted by the technical committees are

circulated to the member bodies for voting. Publication as an lnter-
national Standard requires approval by at least 75 o/‘o of the member
bodies casting a vote.

International Standard IS0 10123 was prepared by Technical Committee

ISO/TC 61, Plastics.

Annex A of this International Standard is for information only.

0 IS0 1990
All rights reserved. No part of this publication may be reproduced or utilized in any form
or by any means, electronic or mechanical, including photocopying and microfilm, without
permission in writing from the publisher.
Intern ational Organizati on for Standardiz ation
Case Postale 56 l CH-1 21 1 Genkve 20 l Switzerland
Printed in Switzerland

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ii
Copyright International Organization for Standardization
Provided by IHS under license with ISO
No reproduction or networking permitted without license from IHS Not for Resale
 INTERNATIONAL STANDARD IS0 10123:1990(E)
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Adhesives - Determination of shear strength of anaerobic

adhesives using pin-and-collar specimens

1 Scope 3 Principle

This International Standard specifies a method for The force required to shear the adhesive joint
the determination of the shear strength of formed between a metal pin and a metal collar is
anaerobic-curing liquid adhesives used for retaining determined. The static shear is calculated from this
cylindrical assemblies, pin-and-collar type, or for force.
locking and sealing threaded fasteners.

This test method may also be used for other ad-

4 Apparatus
hesives.
4.1 Universal testing machine, complying with
The test is for ranking and quality control of ad- IS0 7500-1, which will produce failure in the test
hesives. The result does not necessarily reflect the specimen at between 10 % and 80 % of the scale
performance of the materials in service and the test range. The response time of the machine shall be
is not suitable for providing numerical data for de- short enough for it not to affect the accuracy of
sign purposes. measurement of the force being applied at the time
of failure.
NOTE 1 Numerical design data may be obtained from
tests using the materials and configurations used in the The registered force shall differ by no more than
actual structure. 1 % from that actually applied.

The machine shall have a system for applying a

compressive force directly or indirectly. An example
2 Normative references of a compression cage for use on a tensile testing
machine is shown in annex A.
The following standards contain provisions which,
through reference in this text, constitute provisions 4.2 Test specimen support, made of hardened
of this International Standard. At the time of publi- steel, as shown in figure 1, for positioning the test
cation, the editions indicated were valid. All stan- specimen on the universal testing machine.
dards are subject to revision, and parties to
agreements based on this International Standard 4.3 Test specimen curing rack, as shown in
are encouraged to investigate the possibility of ap- figure 2, or equivalent.
plying the most recent editions of the standards in-
dicated below. Members of IEC and IS0 maintain
registers of currently valid International Standards. 5 Preparation of test specimens

IS0 683-9:1988, Heat-treatable steels, alloy steels Assemble not less than five specimens for each test
and free-cutting steels - Part 9: Wrought free- as described below.
cutting steels.
5.1 Each specimen shall be comprised of a pin
IS0 4588:1989, Adhesives - Preparation of metal of diameter (12,675 -&) mm and a slip collar
surfaces for adhesive bonding. (12,700 +;qo25) mm in in&de diameter and II,10 mm
+ 0,05 mm in width, both components being finished
IS0 7500-1:1986, AJetallic materials - Verification of k 0,8 pm to I,6 pm (see figure 3). The material used
static uniaxial testing machines - Part I: Tensile for the collar and pin shall be stated in the test re-
testing machines. port.

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 IS0 10123:1990(E)

NQTE 2 Unless there is a specific requirement to test Place the pin-and-collar assembly in the steel spec-
the adhesive with a specific material, low-grade carbon- imen support and place the support on the test de-
steel (complying with grade 2 of IS0 683-9) is generally vice (see figure4). Load the specimen smoothly
used and has been found to be satisfactory.
using a constant crosshead speed between
1 mm/min and 2 mm/min.
All components of the cutting oil used in the manu-
facture of specimens shall be completely soluble in Record the maximum load in newtons. Calculate the
the solvents used for degreasing and shall contain static shear strength T, expressed in megapascals,
no lanolin. using the equation
I
z=- F
5.2 Vapour-degrease all pins and collars (see LS
IS0 4588), store them in a desiccator at
23 “C + 2 “C, and keep them clean. Use de- where
greased specimens within four days or discard
F is the maximum load, in newtons;
(oxidation affects the test results after this period of
time). It is permissible to soak or wash hard-greased S is the bond area, in square millimetres.
or waxed parts in solvent prior to vapour-
degreasing. Do not prime or activate unless speci- Test not fewer than five specimens.
fied for the material to be tested (if the specimen is
primed or activated, state this in the test report).

5.3 Pre-assemble pins and collars before appli- 7 Precision

cation of the adhesive, to ensure a smooth and
sliding fit. The precision of this test method is not known be-
cause inter-laboratory data are not available. lnter-
Disassemble the parts. Apply sufficient adhesive to
laboratory data are being obtained and a precision
the surface of each pin, beginning at one end, to
statement will be added at the next revision.
completely cover a length corresponding to the
width of the collar in its final position. Also apply
sufficient adhesive to completely cover the interior
of the collar.

Slip the collar over the pin completely, with a 8 Test report
helicoidal back-and-forth movement (this operation
shall not take longer than 6 s). The test report shal include the following infor-
mation:

5.4 Rack the assembly with the fillet upwards so a) a reference to this International Standard;
that the collar does not slip out of the bond area.
Take care that the rack is at the required tempera- b) a complete identif -ication of the adhesive tested,
ture, and do not place on a hot or cold surface. including type, form, source, date manufactured
There shall be excess material on the leading edge and manufacturer’s code number;
of the collar; if not, apply sufficient adhesive to cre-
ate a fillet. c) a complete identification of the material used
and the method of cleaning and surface prepa-
ration prior to bonding;
5.5 Before application of the adhesive, an activator
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may be applied as recommended by the manufac- d) the adhesive-application and bonding conditions
turer. If an activator is used, rack the assembly with used in preparing the specimens;
the fillet up and, using a clean cloth, carefully wipe
off excess material on the leading edge of the collar. e) the conditioning procedure used for the speci-
mens prior to testing;

5.6 Cure the adhesive in accordance with the f) the number of specimens tested;
manufacturer’s instructions.
g) the crosshead speed;

6 Procedure h) the average value of the maximum load and the

standard deviation, as well as the average value
After allowing for cure and any predetermined en- of the shear strength.
vironmental conditioning, determine the static shear
strength as follows:

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No reproduction or networking permitted without license from IHS Not for Resale
 IS0 10123:1990(E)

Dimensions in millimetres

Dimensions in miliimetres
(except where otherwise stated)

Chamfers 1 x 45’ M pm 5:
g g
Wym 88
a R
I
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-e-,----II I 10
0,254x45' ’
SO,2 0,127 x 45’
40‘8

Figure 1 i Test specimen support

a) Pin

Dimensions in millimetres

b) Collar

Figure 3 - Pin-and-collar assembly

Figure 2 - Test specimen curing rack

l Upper compresslon plate

Specimen

Specimen support

lower compresslon plate

Axls of ceU for measurement

of breaking straln

Figure 4 - Test device

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Copyright International Organization for Standardization

Provided by IHS under license with ISO
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 IS0 10123:1990(E)

Annex A
(informative)

Example of adaptor for tensile testing machine

‘T
Applied foru
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@ ht. 15 mm

fi

AppCled force

Figure A.1 - Jig for compression testing on tensile testing machines

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Provided by IHS under license with ISO
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Copyright International Organization for Standardization

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No reproduction or networking permitted without license from IHS Not for Resale
 IS0 10123:1990(E)

UDC 678.061:621.792.3.052:620.176:620.179.4
Descriptors: plastics, adhesives, adhesive bonded joints, tests, adhesion tests, shear tests.

Price based on 4 pages

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Copyright International Organization for Standardization

Provided by IHS under license with ISO
No reproduction or networking permitted without license from IHS Not for Resale