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Purity of Hyudrochloric Acid

This work instruction outlines the procedure for determining the purity of commercial-grade hydrochloric acid using titration with standard sodium hydroxide. It details the necessary reagents, equipment, and safety precautions, as well as the calculation method for purity. The document is part of the QESH Management System and adheres to ISO and OHSAS standards.

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Ajay Patel
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195 views2 pages

Purity of Hyudrochloric Acid

This work instruction outlines the procedure for determining the purity of commercial-grade hydrochloric acid using titration with standard sodium hydroxide. It details the necessary reagents, equipment, and safety precautions, as well as the calculation method for purity. The document is part of the QESH Management System and adheres to ISO and OHSAS standards.

Uploaded by

Ajay Patel
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOC, PDF, TXT or read online on Scribd
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BHARAT ALUMINIUM COMPANY LTD

CAPTIVE POWER PLANT-540MW


QESH MANAGEMENT SYSTEM
WORK INSTRUCTION :QESH/CPP2/CLB/WA-17 DETERMINATION OF PURITY HYDROCHOLIC ACID
ISO : 9001 ISO :14001/OHSAS :18001
ELEMENT NAME : Monitoring and Measurement of Process
ISO : 9001 ISO :14001/OHSAS :18001
ELEMENT NUMBER : 8.2.3, 4.4.6
REV.NO.01 VERSION NO.00 W.I. NO : QESH/CPP2/CLB/WA-17 Page 1 of 2

1.0 Purpose: Determination of purity of Hydrochloric acid

2.0 Scope: This test covers the determination of hydrochloric acid, commercial grade.

3.0 Input: Hydrochloric acid & reagents

4.0 Output: purity of hydrochloric acid

5.0 Responsibility: Chemist/Analyst

6.0 Summary of Test method:

Known weight of hydrochloric acid is taken in a conical flask containing approximately


50ml of water and titrated against standard sodium hydroxide solution, using
phenolphthalein indicator. The end point is the appearance of pink color.

7.0 Reagents:

Standard Sodium Hydroxide solution 1N:

Phenolphthalein Indicator: Dissolve 0.5gm of Phenolphthalein in 100ml of ethanol.


Add a few drops of sodium hydroxide solution until the indicator faintly pink.

8.0 Procedures:
Place about 100ml of DM water in a 250ml conical flask. Weigh accurately about 2 to3
grams of the acid in a stopper weighing bottle reweigh the weighing bottle after adding
the acid to the flask. Shake and mix the contents of the flask thoroughly, allow to cool
and add 2 drops of phenolphthalein indicator and titrate to the end point by means of
standard sodium hydroxide solution. Gloves must be used.

PREPARED BY: APPROVED BY:

PANKAJ NIGAM R.K.DHANCHOLIA


Asst Manage (QA) AGM (O), CPP 540 MW
Sign & Date Sign & Date
BHARAT ALUMINIUM COMPANY LTD
CAPTIVE POWER PLANT-540MW
QESH MANAGEMENT SYSTEM
WORK INSTRUCTION :QESH/CPP2/CLB/WA-17 DETERMINATION OF PURITY HYDROCHOLIC ACID
ISO : 9001 ISO :14001/OHSAS :18001
ELEMENT NAME : Monitoring and Measurement of Process
ISO : 9001 ISO :14001/OHSAS :18001
ELEMENT NUMBER : 8.2.3, 4.4.6
REV.NO.01 VERSION NO.00 W.I. NO : QESH/CPP2/CLB/WA-17 Page 2 of 2

9.0 Calculation:

Purity as Hydrochloric acid = V*N*3.645/W

Where,

V= volume in ml of standard sodium hydroxide solution


N= Normality of standard sodium hydroxide solution
W= weight in gram of sample taken for the analysis

10.0 Reference Standard:

Vogel textbook of inorganic Quantitative analysis.

Specification of Hydrochloric acid IS:.

11.0 QMS ensure the running of equipment is within the rated parameters

12.0 EMS:

Wear apron, nose mask & safety goggle to protect you

13.0 OHSAS:

1. Take care from injury due to Chemical spillage


2. Take care of injury due to glass material
3. Take care from burn due to chemicals

14.0 RECORD: RECORD IS MAINTAINED WITH IN THE LAB

PREPARED BY: APPROVED BY:

PANKAJ NIGAM R.K.DHANCHOLIA


Asst Manage (QA) AGM (O), CPP 540 MW
Sign & Date Sign & Date

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