The document discusses different types of packings used in distillation columns. It describes random packings which are packed randomly and structured packings which are arranged in blocks. Common materials for packings include metal, ceramic, and plastic. Newer types of packings like grid trays have been introduced to handle fluids with solids. The optimal packing provides a high surface area to volume ratio with low pressure drop. Design considerations for column internals like trays and supports are also outlined.
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PPTX, PDF, TXT or read online on Scribd
0 ratings0% found this document useful (0 votes)
65 views41 pages
BVCOE Navi Mumbai: Types of Packings
The document discusses different types of packings used in distillation columns. It describes random packings which are packed randomly and structured packings which are arranged in blocks. Common materials for packings include metal, ceramic, and plastic. Newer types of packings like grid trays have been introduced to handle fluids with solids. The optimal packing provides a high surface area to volume ratio with low pressure drop. Design considerations for column internals like trays and supports are also outlined.
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PPTX, PDF, TXT or read online on Scribd
You are on page 1/ 41
TYPES OF PACKINGS
Prof. Manoj B. Mandake
Department of Chemical Engineering,
BVCOE Navi Mumbai
PACKED DISTILLATION COIUMN • In a packed tower we have two types of packings , depending upon the way they are held in a tower.
• Random packings are packed randomly while
structured are arranged in a packing blocks, one over the other.
• This are the broad classes of packings. depending
upon the vendor there could be changes in shape. • Majority of the above packings are fabricated in metal, ceramic and plastics. some packings can also be fabricated in glass and graphite.
• Packed columns are not suitable for dealing with
liquid containing or producing large concentration of solids, as the packings will block up and or distribute unevenly.
• In order to overcome problems associated with ‘dirty’
fluids such as heavy residue, in refinery a new type of packings known as ‘grid trays’ has been introduced. • Packed columns are particularly useful in the field of vacuum distillation.
• A good packing material is the one that provides
a high surface area per volume.
• The material of construction must provide a high
liquid flow capacity as well as a good resistance to the pressure (high strength). Finally the pressure drop should be desirably low. • When the size increases, both mass transfer and pressure drop decrease.
• The optimal size and shape is the one which compromise
both factors.
• Nowadays metal and plastic packing have replaced the
ceramic
• However, ceramic elements are still used when corrosive
chemicals are involved and good wettability is required. • For random packing, the old rashig rings (d3) and berl saddles (d2, yellow pieces) are substituted by pall rings, intalox saddles, mini cascade ring, and a broad range of other different shaped elements (d1, d2).
• Concerning structured packing, it is considerably more expensive than the random one.
• However, it has the advantage of high mass
transfer efficiency with very low pressure drop. Pall rings Raschig Rings Structured Packings Grid Trays DESIGN AND CONSTRUCTION FEATURES OF COLUMN INTERNALS
• Several factors control the design and
construction of plates and trays.these factors are : • Load on the tray due to dead weight,liquid weight and impact due to downcoming liquid.
• Expansion due to a rise temperature.
• Ease of installation and fabrication.
• Ease of access and maintenance.
• Method of support.
• Material of construction.
• Safety. Plate design • Plates or trays can be either as one piece trays or as sectional trays.
• One piece tray may be made of cast iron.
• One of the main advantages is its ability
to cope with thermal expansion. Loading conditions for plates ands trays.
• The loads which cause deflection are:
• Weight of the trays with contacting devices and downcomers. • Weight of the liquid. • Impact load of the downcoming liquid, which is given by load= • Where w= wt. of the liquid per second. v=velocity per second g=gravitation constant. • Weight of maintenance personnel and tools. • The design based on certain guidelines for tray loadings are as follows: 1.Fractionating trays shall be designed for uniform live load of 60N/ 2.The weight of liquid at maximum height of weir setting whichever is greater. 3.Maximum deviation from horizontal at normal tray loading shall not exceed 1/900th of the span. 4.Areas under downcomers shall be design for a uniform load of 3200 N/ or weight of liquid for one half of the height of downcomer whichever is greater. 5.pans shall be designed for a uniform live load of 800 N/ or the wt. of liquid at the maximum operating level on the pan , whichever is greater. 6. baffels shall be designed for a live load of 800 N/ on the project horizontal area. Deflection and stresses • Defiection and stress determination for trays will depend on the methods used for the supporting structure.
1.the tray is supported on a peripheral ring. this
method is adopted only for small diameter columns.
2.the tray is supported on a truss made up of angel,
channel or trapezoidal section members rolled sheets. Trays supported on a peripheral ring
• 1.this may be considered as a circular plate,
fixed at the circumference and subjected to a uniform load over a surface. the deflection is given by • Where E=modulus of elasticity. t=thickness of the plate. R=radius of the plate. if possions ratio for metal is taken as1/3 i.e, m=3 then, • During the cleaning and assembly operations uniformly distributed load of tray and downcomers will produce a stress in the tray which is given by
where, p=uniformly distributed load
R= radius of tray t=thickness of tray. • While due to be concentrated load of maintenance personnel and tools the stress produced in the tray will be given by,
where,w=conc. Load at the centre of tray
t= thickness of tray R=radius of tray x= any intermediate radius. Trays supported on a truss • The size of each purlin or beam of the truss will be determined by the span and the load shared by the purlin. • The load on the tray will be shared by the purlins in proportion to the area of the tray supported by it. • The deflection of each purlin has to be limited. • The deflection is given by
Where W=total load carried by the purlin.
l=span or purlin. I=moment of Inertia. • The stress is the purlin is given by,
• For uniformly distributed load,
Where, Z=Modulus of section of the
purlin. Truss support for tray Purlins or beams • These may be fabricated in the form of angles , channels or trapezoidal sections from sheets. • The following conditions may be observed as far as possible,
1.Support beam axis should preferably be normal to the
direction of liquid flow on the tray.
2.Beam depth should not exceed 20% of the vertical
distance between trays. 3.tray areas blanked by supporting member should be in range of 5 to 10% of the total tray area.
4.holding down bolt should be of 10 mm
diameter.
5.bolt spacing around trays should not
exceed 100 mm and that on the downcomers should not exceed 75 mm. VERTICAL SUPPORTS • The load on the vertical supports is the total weight of all trays including the liquid and the total impact load. • The load is shared by a large no. of vertical bars. • By providing a sufficient no. of vertical supports it is possible to limit deflection of the tray to the desired range. • Support bars of carbon steel are either round or hexagonal. Support plates in the packed column • The load to be carried by the support plates at the bottom of the column are 1.weight of the packing 2.weight of the liquid 3.force due to the pressure surges. 4.weight of the intermediate supports. • If there are no intermediate supports, the entire load will be taken by the bottom support. Support for column • Column of 600 mm internal diameter and above are usually mounted on mild steel skirts. • Smaller columns are more often mounted on legs or from the steel structure. • The skirt height is decided by NPSH requirement of the bottom product pump. • Expect for the mild steel columns, the top 150 mm skirt should be made from same material as column to avoid the contamination of material in contact with process. Nozzles • The column is provided with several nozzles.
• All nozzles above 50 mm diameter have to
checked for reinforcement.
• Similarly, all nozzles above 50 mm diameter
are to be provided with standard pipe flanges. Trays • A column in this type used in industry, is made up of shell fabricated from sheets by welding.
• It has no flange joints.
• This naturally require a special design of
trays, which can be easily dismantled and removed. • Such trays are sectional trays.
• These trays are made from stainless
steel, with thickness of 2 mm and with holes of 5 mm diameter.
• The downcomers at even no.of trays are
located at the ends. • The shape of downcomers is segmental with size 300 mm * 1700 mm at the top and 225 mm *1700 mm at the lower end.
• The shape of the downcomer is rectangular
with a size 300 mm * 2620 mm at the top and 200 mm *2620 mm at the lower end. Support for trays • The supporting system consists of six purlins symmetrically placed underneath each tray. • The ends of purlins are attached to two sectors which are fixed to the column walls. • The load carried by each purlin is in proportion to the area of tray supported by purlin. • The width is taken as half the distance to the next purlin. THANK YOU
Strength Of Beams, Floor And Roofs - Including Directions For Designing And Detailing Roof Trusses, With Criticism Of Various Forms Of Timber Construction