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Presentado Por: Valentina Camargo Velandia Camilo Ramirez Javier Quiroga Valdez

This document contains 27 heuristics for process synthesis: 1. It recommends dryer types for different particle sizes, including continuous tray and belt dryers, rotary cylindrical dryers, and fluidized-bed dryers. 2. It suggests drum dryers for pastes and slurries, and spray dryers for liquid or pumpable slurries. 3. It provides strategies for handling exothermic and endothermic reactions, such as using excess reactant, inert diluents, or intercoolers/interheaters.

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Camilo Ramirez
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54 views20 pages

Presentado Por: Valentina Camargo Velandia Camilo Ramirez Javier Quiroga Valdez

This document contains 27 heuristics for process synthesis: 1. It recommends dryer types for different particle sizes, including continuous tray and belt dryers, rotary cylindrical dryers, and fluidized-bed dryers. 2. It suggests drum dryers for pastes and slurries, and spray dryers for liquid or pumpable slurries. 3. It provides strategies for handling exothermic and endothermic reactions, such as using excess reactant, inert diluents, or intercoolers/interheaters.

Uploaded by

Camilo Ramirez
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as PPTX, PDF, TXT or read online on Scribd
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Heurísticas

para la
Síntesis de
Procesos 19-
Presentado Por: 27
Valentina Camargo Velandia
Camilo Ramirez
Javier Quiroga Valdez
HEURISTIC 19

● For granular material, free flowing or not, of particle


sizes from 3 to 15 mm, use continuous tray and belt
dryers with direct heat.

● For free flowing granular solids that are not heat


sensitive, use an inclined rotary cylindrical dryer,
where the heat may be supplied directly from a hot gas
or indirectly from tubes, carrying steam, that run the
length of the dryer and are located in one or two rings
concentric to and located just inside the dryer rotating
shell. For small, free-flowing particles of 1 to 3 mm in
diameter, when rapid drying is possible, use a
pneumatic conveying dryer with direct heat.

● For very small free-flowing particles of less than 1


mm in diameter, use a fluidized-bed dryer with direct
HEURISTIC 20

For pastes and slurries of fine solids,


use a drum dryer with indirect heat. For
a liquid or pumpable slurry, use a spray
dryer with direct heat.
HEURISTIC 21

To remove a highly exothermic heat of


reaction, consider the use of excess
reactant, an inert diluent, or cold shots.
These affect the distribution of
chemicals and should be inserted early
in process synthesis.
Ejemplo
HEURISTIC 22

Heat removal and addition

For less exothermic heats of


reaction, circulate reactor fluid to
an external cooler, or use a jacketed
vessel or cooling coils.

Also, consider the use of


intercoolers between adiabatic
reaction stages.
Ejemplo
Ejemplo
HEURISTIC 23

Heat removal and addition

To control temperature for a highly


endothermic heat of reaction:

Consider the use of excess reactant, an


inert diluent, or hot shots. These affect
the distribution of chemicals and
should be inserted early in process
synthesis
Ejemplo
HEURISTIC 24

Heat removal and addition

For less endothermic heats of reaction,


circulate reactor fluid to an external
heater, or use a jacketed vessel or
heating coils. Also, consider the use of
inter heaters between adiabatic reaction
stages.
Ejemplo
The usual methods of heat exchange are:
1. Heat exchange between two process fluids using a double-pipe, shell-and-tube, or
compact heat exchanger.
2. Heat exchange between a process fluid and a utility, such as cooling water or steam,
using a double-pipe, shell-and-tube, air-cooled, or compact heat exchanger.
3. High-temperature heating of a process fluid using heat from the products of
combustion in a furnace.
4. Heat exchange within a reactor or separator, rather than in an external heat-exchange
device.
5. Direct heat exchange by mixing the two streams that are exchanging heat.
6. Heat exchange involving solid particles
Ejemplo
HEURISTIC 25:

Unless required as part of the design of the


separator or reactor, provide necessary heat
exchange for heating or cooling process fluid
streams, with or without utilities, in an external
shell-and-tube heat exchanger using
countercurrent flow. However, if a process stream
requires heating above 7508F, use a furnace unless
the process fluid is subject to chemical
decomposition.
HEURISTIC 26:

Near-optimal minimum temperature


approaches in heat exchangers depend on the
temperature level as follows:
10°F or less for temperatures below ambient.

20°F for temperatures at or above ambient up


to 300°F.

50°F for high temperatures.

250 to 350°F in a furnace for flue gas


temperature above inlet process fluid
temperature.
HEURISTIC 27:

When using cooling water to cool or condense


a process stream, assume a water inlet
temperature of 90°F (from a cooling tower)
and a maximum water outlet temperature of
120°F.
Ejemplo
1. Su presión se incrementa a 26
atm.
2. Su temperatura se eleva al
punto de ebullición, que es 242°C
a 26 atm.
3. El dicloroetano líquido se
vaporiza a 242°C.
4. Su temperatura se eleva a la
temperatura de pirolisis, 500°C.

Diagrama de flujo que muestra la integración de tareas para el proceso de dicloroetano


Ejemplo

Formas diferentes de ebullición en transferencia de calor. Flujo concurrente

Flujo concurrente

Flujo cruzado

Patrones de flujo estándar en intercambiadores de calor.


REFERNCIAS
BIBLIOGRAFICAS
 Seader, S. L. (2004). PRODUCT AND PROCESS DESING PRINCIPLES SYNTHESIS, ANALYSIS AND
EVALUATION. John Wiley & Sons, Inc
GRACIAS

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