IS 9103 : 1999

(Reaffirmed 2004)
Edition 2.2
(2007-08)
B U R E A U O F I N D I A N S T A N D A R D S
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 110002
Price Group 7
BIS 2008
Indian Standard
CONCRETE ADMIXTURES SPECIFICATION
( First Revision )
(Incorporating Amendment Nos. 1 & 2)
ICS 91.100.30
Cement and Concrete Sectional Committee, CED 2
FOREWORD
This Indian Standard (First Revision) was adopted by the Bureau of Indian Standards, after the
draft finalized by the Cement and Concrete Sectional Committee had been approved by the Civil
Engineering Division Council.
Admixtures are materials added to the concrete before or during its mixing, with a view to
modifying one or more of the properties of concrete in the plastic or hardened state. An important
feature of the majority of admixtures for concrete is that it is difficult to quantitatively evaluate
the behaviour of the concrete under various possible circumstances. Therefore, performance of an
admixture is evaluated by comparing the properties of concrete with the admixture under test
with those of concrete without any admixture or with a reference admixture. This standard lays
down the procedure for such a relative evaluation of admixtures for concrete.
In recent time there has been a lot of development in the field of admixtures. Superplasticizers,
both normal and retarding type, constitute a major group of admixtures used by site engineers
now. Superplasticizers help in lowering the water/cement ratio so as to contribute to the
enhancement of durability. In this first revision of the standard, first published in 1979,
requirements of superplasticizers in detail and methods of determination of flow of concrete of
high workability have been added.
This standard also gives uniformity tests which demonstrate that a particular consignment is
similar to material that has previously been submitted to the acceptance test.
The admixtures covered in this standard are intended mainly for modifying a single property in
concrete, but some of the admixtures available in the market are often capable of modifying more
than one property of the concrete. In addition, an admixture may be used to improve the desirable
properties of concrete in more than one way. For example, water reducing admixtures ( see 3.4 )
may be used to improve the workability of concrete with the same water and cement contents, to
increase the compressive strength without changing the workability by reduction of the water
content in the concrete mix or to effect saving in cement content by reduction in both the cement
and water contents in the mix while maintaining the same workability and compressive strength
as in the reference concrete. In such cases, the procedure of evaluation of the admixture may have
to be appropriately chosen. This standard also provided for evaluation of admixtures for specific
use with the materials and mix proportions to be used on the work.
The performance of concrete admixtures including superplasticizers depend upon both the
admixtures and the cement and their compatibility, in addition to the concrete mix proportions and
the environmental conditions in the field. Among the characteristics of the cement, which affect the
performance of concrete admixtures including superplasticizers are the C
3
A, SO
3
and alkali contents,
nature of sulphates, and the fineness. The ambient temperature and humidity conditions influence
the performance of set-controlling admixtures and affect the retention of enhanced workability
(slump loss) when water-reducing admixtures and superplasticizers are used. While no
generalisation of these effects is possible, it is nevertheless necessary to evaluate concrete admixtures
for specific use with the concrete-making materials and mix proportions to be used on the work, under
field conditions. This standard also provides for such specific evaluation of an admixture, in addition
to the general evaluation for conformity to the requirements of this standard.
The requirements of integral waterproofing admixtures are covered in IS 2645 : 1975
Specification for integral cement waterproofing compounds ( first revision ).
This edition 2.2 incorporates Amendment No. 1 (January 2003) and Amendment No. 2 (August 2007).
Side bar indicates modification of the text as the result of incorporation of the amendments.
For the purpose of deciding whether a particular requirement of this standard is complied with,
the final value, observed or calculated, expressing the result of a test or analysis, shall be rounded
off in accordance with IS 2 : 1960 Rules for rounding off numerical values ( revised ). The number
of significant places retained in the rounded off value should be the same as that of the specified
value in this standard.
IS 9103 : 1999
1
Indian Standard
CONCRETE ADMIXTURES SPECIFICATION
( First Revision )
1 SCOPE
1.1 This standard covers the chemical
and air-entraining admixtures including
superplasticizers, solid or liquid or emulsion, to
be added to cement concrete at the time of
mixing so as to achieve the desired property in
concrete, in the plastic or hardened state.
1.2 The different types of admixtures covered
in this standard are as follows:
1.3 The chloride content in the admixture shall be
declared by the manufacturer. Superplasticizers
are expected to be chloride free.
1.3.1 Admixtures that contain relatively large
amounts of chloride may accelerate corrosion of
prestressing steel. Where corrosion of such
steel is of major concern, compliance with the
requirement of this specification does not
constitute assurance of acceptability of the
admixture for use in prestressed concrete. In
case of reinforced concrete, to minimize the
chances of deterioration of concrete, the total
chloride content in the concrete should be
limited as specified in IS 456.
2 NORMATIVE REFERENCES
The Indian Standards listed in Annex A
contain provisions which, through reference in
this text, constitute provision of this standard.
At the time of publication the editions indicated
were valid. All standards are subject to
revision, and parties to agreement based on
this standard are encouraged to investigate the
possibility of applying the most recent edition
of the standards indicated in Annex A.
3 TERMINOLOGY
3.0 For the purpose of this standard, the
following definitions shall apply.
3.1 Admixtures
A material other than water, aggregates, and
hydraulic cement and additives like pozzolana
or slag and fibre reinforcement used as an
ingredient of concrete or mortar and added to
the batch immediately before or during its
mixing to modify one or more of the properties
of concrete in the plastic or hardened state.
3.2 Accelerating Admixture or Accelerator
An admixture when added to concrete, mortar
or grout, increases the rate of hydration of a
hydraulic cement, shortens the time of set, or
increases the rate of hardening or strength
development.
3.3 Retarding Admixture or Retarder
An admixture which delays the setting of
cement paste, and hence of mixtures, such as
mortar or concrete containing cement.
3.4 Water Reducing Admixture or
Workability Aid
An admixture which either increases
workability of freshly mixed mortar or concrete
without increasing water content or maintains
workability with a reduced amount of water.
3.5 Air-Entraining Admixtures
An admixture for concrete or mortar which
causes air to be incorporated in the form of
minute bubbles in the concrete or mortar
during mixing, usually to increase workability
and resistance to freezing and thawing and
disruptive action of de-icing salts.
3.6 Superplasticizing Admixtures
An admixture for mortar or concrete which
imparts very high workability or allows a large
decrease in water content for a given workability.
3.7 Retarding Superplasticizing Admixture
Superplasticizing admixture that imparts
prolonged workability retention and retards
setting.
4 REQUIREMENTS FOR ADMIXTURES
Concrete made with admixtures when
compared with identical concrete made without
the admixture in accordance with 7 and 8 shall
conform to the requirements appropriate to the
type of admixture given in Table 1A and Table
1B, except in the case of air-entraining
admixture. In the case of air-entraining
admixtures, a reference admixture of approved
quality shall be used in the control concrete to
entrain identical amount of air.
NOTE If required by the purchaser, the concrete with
air-entraining admixture may be tested for resistance to
freezing and thawing in accordance with the procedure
given in Annex B, in such case the relative durability
factor of the concrete with admixture under test shall be
not less than 80.
a) Accelerating admixtures,
b) Retarding Admixtures,
c) Water-reducing admixtures,
d) Air-entraining admixtures, and
e) Superplasticizing admixtures.
IS 9103 : 1999
2
Table 1A Physical Requirements
( Clause 4 )
Sl
No.
Requirements Accele-
rating
Admixture
Retarding
Admixture
Water
Reducing
Admixture
Air-Entrain-
ing Admixture
Superplasticizing
Admixture (for Water-
Reduced Concrete Mix)
Test
Ref
Normal Retarding Type
(1) (2) (3) (4) (5) (6) (7) (8) (9)
i) Water content,
percent of control
sample, Max
95 80 80 7.2.5
ii) Slump Not more than 15 mm
below that of the
control mix concrete
7.2.1
iii) Time of setting,
allowable deviation
from control sample
hours:
7.2.3
Initial
Max
Min
3
1
+ 3
+ 1
1

+ 1.5

+ 4
+ 1
Final
Max
Min
2
1
+ 3
+ 1
1

1.5

+ 3

iv) Compressive strength

percent of control
sample, Min
, 8.2.1
1 day 140
3 days 125 90 110 90 125 125
7 days 100 90 110 90 125 125
28 days 100 90 110 90 115 115
6 months 90 90 100 90 100 100
1 year 90 90 100 90 100 100
v) Flexural strength,
percent of control
sample, Min
8.2.2
3 days 110 90 100 90 110 110
7 days 100 90 100 90 100 100
28 days 90 90 100 90 100 100
vi) Length change,
percent increase over
control sample, Max
8.2.3
28 days 0.010 0.010 0.010 0.010 0.010 0.010
6 months 0.010 0.010 0.010 0.010 0.010 0.010
1 year 0.010 0.010 0.010 0.010 0.010 0.010
vii) Bleeding, percent
increase over control
sample, Max
5 5 5 5 5 5 7.2.4
ix) Air content (%)
Max, over control
1.5 1.5

IS 9103 : 1999
3
5 METHOD OF SAMPLING OF
ADMIXTURE FOR TEST
5.1 Liquid Admixture
Liquid admixture shall be agitated thoroughly
immediately prior to sampling. Grab
(individual) samples taken for testing shall
represent not more than 9 000 litres of
admixture and shall have a volume of at least
one litre. A minimum of four grab samples shall
be taken. Composite samples shall be prepared
by thoroughly mixing the grab samples selected
and the resultant mixture sampled to provide
at least 4 litres for quality tests.
5.1.1 Admixture from bulk storage tanks shall
be sampled equally from the upper,
intermediate, and lower levels by means of
drain cocks in the sides of tanks or a weighed
sampling bottle fitted with a stopper that can
be removed after the bottle is lowered to the
desired depth.
5.2 Non-liquid Admixture
Grab samples taken for tests shall represent
not more than 2 tonnes of admixture and shall
weigh at least 1 kg. A minimum of 4 grab
samples shall be taken and composite sample
shall be prepared by thoroughly mixing the four
grab samples. The resultant mixture sampled
shall provide at least 2.5 kg from the composite
sample. Grab samples shall be taken from
different locations well distributed throughout
the quantity to be represented.
5.2.1 Samples of packed admixtures shall be
obtained in the same manner as described in
IS 3535.
5.2.2 Samples shall be packed in moisture-
proof, airtight containers.
6 PREPARATION OF TEST SAMPLES
6.1 Materials
6.1.1 Materials for Tests for Specific Use
When an admixture is required to be tested for
a specific work, test samples shall be prepared
using materials proposed to be used on the
work.
6.1.2 Materials for Tests for General Evaluation
of Admixture
When an admixture is required to be tested for
general evaluation, the requirements of
materials shall be as follows:
6.2 Preparation of Concrete
6.2.1 Except in the case of air-entraining
admixtures, the concrete mix shall be prepared
both with and without admixture, the latter
being treated as the reference or control
concrete mixture. In the case of air-entraining
admixtures, reference admixture shall be used
in control concrete ( see 4 ).
6.2.2 The admixture shall be used in
accordance with the recommendations of the
manufacturer. When an admixture is to be
tested specifically for air-entrainment, it shall
be used in such a quantity that it produces air
content in the range of 3.5 to 7 percent.
NOTE The manufacturer shall give detailed
instructions on the correct use of the admixture for the
purpose indicated.
Table 1B Requirements for High Workability Test Mix
( Clause 4 )
Sl No. Requirements Type of Superplasticizing Admixture Test Reference
Normal Retarding Type
(1) (2) (3) (4) (5)
i) Flow 510 mm - 620 mm 510 mm - 620 mm 7.2.1.1
ii) Loss of workability on standing At 45 min the slump shall be
not less than that of control
mix concrete at 15 min
At 2 h the slump shall be
not less than that of control
mix concrete at 15 min
7.2.1.2
iii) Minimum compressive strength,
percent of control mix concrete
8.2.1
7 days 90 90
28 days 90 90
6 months 90 90
1 year 90 90

a) Cement The cement shall be ordinary

Portland cement conforming to IS 269 or
IS 8112 or IS 12269.
b) Aggregate The coarse and fine aggre-
gates shall conform to the requirements
given in IS 383. While the fine aggregate
shall conform to the grading of Zone II,
the coarse aggregate shall be graded
aggregate of 20 mm nominal maximum
size, with the gradings conforming to
IS 383 in both the cases.
IS 9103 : 1999
4
6.2.3 Proportioning of Concrete
6.2.3.1 Proportioning concrete for tests for
specific use
The concrete mix shall be proportioned to have
the cement content specified for the work and
to meet the stipulated workability and strength
requirements. In case of air-entrained concrete,
the air content specified for the work shall be
used. If the maximum size of coarse aggregate
is greater than 20 mm, the concrete mix shall
be wet-screened over 20 mm IS Sieve before
test.
6.2.3.2 Proportioning concrete for tests for
general evaluation
The concrete mix may be designed according to
any accepted method of mix design, to meet the
following requirements:
6.2.3.3 Samples shall be thoroughly mixed as
recommended by the manufacturer to ensure
uniformity before testing.
6.2.4 The concrete shall be made in a
mechanical power driven mixer in accordance
with the procedure specified in IS 516.
7 SAMPLING AND TESTING OF FRESH
CONCRETE
7.1 Sampling
Sampling of fresh concrete shall be done
according to the requirements given in IS 1199.
7.2 Methods of Tests
Samples of freshly mixed concrete from at least
three separate batches for each condition of
concrete shall be analysed for the tests
described in 7.2.1 to 7.2.5.
7.2.1 Test for Workability
The workability of freshly mixed concrete in
terms of slump or compaction factor shall be
determined according to method given in
IS 1199.
NOTE In some cases, it may also be worthwhile to
determine the workability of fresh concrete not sooner
than 15 min and not later than 20 min after completion
of mixing, as the relative advantage of some water-
reducing admixtures may decrease with time after
mixing.
7.2.1.1 The flow of freshly mixed
superplasticized concrete of high workability
shall be determined according to the method
given in Annex C.
7.2.1.2 Loss of workability on standing
The slump of high workability concrete mixes
shall be determined at 45 min and at 2 h, using
normal type and retarding type
superplasticizers, respectively after the
following operations.
After mixing the concrete mixes shall be
covered to prevent loss of water by evaporation
and kept at a temperature of 27 2C and
relative humidity of 65 5 percent. At 45 min,
the concrete shall be remixed by hand using a
shovel just enough to counteract any bleeding
or segregation and slump of concrete shall be
determined. The tested concrete shall be
discarded and the remaining concrete shall be
covered and tested at 2 h, after mixing by hand
using a shovel.
7.2.2 Test for Air-content
Air-content of freshly mixed concrete shall be
determined by the pressure method given in
IS 1199.
7.2.3 Test for Time of Setting
Time of setting, initial and final, shall be
determined as given in IS 8142.
7.2.4 Test for Bleeding
Bleeding shall be computed at a percentage of
the net amount of mixing water in the concrete.
The net mixing water is the water in excess of
that present as absorbed water in the
aggregate. Absorbed water in the aggregate
shall be determined as given in IS 2386
(Part 3). The test shall be carried out in
accordance with the details given in Annex D.
7.2.5 Test for Water Content
7.2.5.1 The water-cement ratio of the concrete
shall be determined to the nearest 0.001, as
follows:
7.2.5.2 The relative water content for the
concrete containing admixture shall be
a) The cement content of the mix shall be
307 3 kg/m
3
,
b) The concrete mix shall have a slump of 50
10 mm or a compaction factor of 0.85 to
0.90 to facilitate compaction by
hand-rodding,
c) The concrete mix shall be compacted
according to the requirements given in
IS 516, and
d) In case of air-entrained concrete an air
content of 6 percent shall be used.
a) Net water content of the batch shall be
computed by determining the absorption
water of aggregate as given in IS 2386
(Part 3).
b) Mass of cement per unit volume of
concrete shall be computed as given in
IS 1199, and
c) Water-cement ratio shall be determined
by dividing the net mass of water by the
mass of cement in batch.
IS 9103 : 1999
5
expressed as a percentage of the water content
of the reference concrete mixture. This shall be
computed by dividing the average water
content of all batches of concrete by the average
water content of the reference concrete and
multiplying the quotient by 100.
8 TESTING OF HARDENED CONCRETE
8.1 Preparing Test Specimens
The test specimens shall be prepared as given
in IS 516.
8.2 Method of Testing
Specimens for tests on hardened concrete shall
be prepared from at least three separate
batches for concrete with and without the
admixture. The specimen shall be analysed for
the requirements described in 8.2.1 to 8.2.3.
8.2.1 Test for Compressive Strength
At least three specimens shall be tested for
each type of concrete and each age of testing.
Compressive strength shall be determined as
given in IS 516.
8.2.2 Test for Flexural Strength
At least three specimens shall be tested for
each type of concrete and each age of testing.
Flexural strength shall be computed as given in
IS 516.
8.2.3 Test for Length Change ( Drying
Shrinkage )
Changes in length on drying and wetting shall
be determined as given in IS 1199. The
moist-curing period, including the period in
moulds shall be 14 days.
9 UNIFORMITY TEST AND
REQUIREMENTS
Any batch of admixture shall have the same
physical state and composition, as that of the
admixture tested for acceptance. To check this
uniformity of composition, a representative
sample of the batch shall be tested and shall
satisfy the requirements given in Table 2.
10 MARKING
10.1 Each container of admixture shall be
legibly marked with the following information:
10.2 Additional Information
The following information shall be provided by
the manufacturer in a printed form
a) Identification of the source of
manufacture,
b) Year and date of manufacture,
c) Type of admixture, that is, whether
accelerating, retarding, water reducing,
air-entraining, normal superplasticizing
or retarding superplasticizing,
d) Batch Number, and
e) Chloride ion content.
a) Physical state (that is, liquid or solid) and
colour;
b) Composition;
i) Generic type of main active constituent(s),
for example, lignosulphonate, organic
hydroxycarboxylic acid or carbohydrate;
ii) Dry material content;
iii) Ash content;
iv) Relative density of liquid admixture;
v) Chloride ion content, expressed as a
percentage by mass of total admixture;
Table 2 Uniformity Tests and Requirements
( Clause 9 )
Sl No. Property Requirement Reference Test
(1) (2) (3) (4)
i) Dry material content Annex E
a) For liquid admixture 0.95T DMC < 1.05T,
b) For solid admixture where
T manufacturers stated valve, in percent by mass
DMC test results, in percent by mass
ii) Ash content 0.95T AC < 1.05T, do
where
T manufacturers stated valve, in percent by mass
AC test results in percent by mass
iii) Relative density Within 0.02 of the value stated by the manufacturer do
iv) Chloride ion content Within 10 percent of the value or within 0.2 percent
whichever is greater as stated by the manufacturer
do
v) pH 6, Min do
NOTE Uniformity requirements for ash content is not applicable to accelerating admixture which may contain more
than 1 percent chloride content.
IS 9103 : 1999
6
10.3 Information Concerning the
Admixture Acceptance Test
The following information shall be provided by
the manufacturer in a printed form, if
requested:
a) The source of cement (works of
11 BIS Certification Marking
The product may also be marked with Standard
Mark.
11.1 The use of Standard Mark is governed by
the provisions of Bureau of Indian Standards
Act, 1986 and the Rules and Regulations made
thereunder. The details of conditions under
which the licence for the use of Standard Mark
may be granted to manufacturers or producers
may be obtained from the Bureau of Indian
Standards.
ANNEX A
( Clause 2 )
LIST OF REFERRED INDIAN STANDARDS
c) The chloride ion content relative to the
cement mass contributed by the
recommended dosage or dosages expressed
as percentage by mass of chloride ion;
d) Recommended storage conditions,
maximum storage time before use and
necessary safety precautions, for
example, toxic or corrosive;
e) Any known incompatibility with other
admixture or with certain types of cement
etc;
f) The recommended dosage or dosages;
g) The effect of underdosage and
overdosages; and
h) Expiry date.
manufacture) and aggregates (quarry or
pit or for material dredged from seas,
estuaries or river the locality);
b) The quantity of admixture used in the
test mix concretes;
c) The values of slump, w/c ratio and cement
content for each batch of the control and
test mix concretes; and
d) The air content of each batch of the
control and test mix concrete.
IS No. Title
269 : 1989 Specification for 33 grade
ordinary Portland cement
( fourth revision )
383 : 1970 Specification for coarse and fine
aggregates from natural sources
for concrete ( second revision )
456 : 1978 Code of practice for plain and
reinforced concrete ( third
revision )
516 : 1959 Method of test for strength of
concrete
1199 : 1959 Methods of sampling and
analysis of concrete
2386
(Part 3) : 1963
Methods of test of aggregates
for concrete : Part 3 Specific
gravity, density, voids,
absorption and bulking
IS No. Title
3535 : 1966 Methods of sampling hydraulic
cement ( first revision )
6925 : 1973 Methods of test for
determination of water soluble
chlorides in concrete
admixtures
8112 : 1989 Specification for 43 grade
ordinary Portland cement
( first revision )
8142 : 1976 Methods of test for determining
setting time of concrete
penetration resistance
12269 : 1987 Specification for 53 grade
ordinary Portland cement
IS 9103 : 1999
7
ANNEX B
( Note under Clause 4 )
TEST FOR RESISTANCE OF CONCRETE AGAINST FREEZING AND THAWING
B-0 TEST FOR RESISTANCE OF
CONCRETE AGAINST FREEZING AND
THAWING
B-1 The freezing and thawing cycle shall
consist of alternately lowering the temperature
of the specimens from 4 1C to 18 2C and
raising it from 18 2C to 4 1C in not less
than 2 h nor more than 5 h. The freezing and
thawing can take place either in (i) water, or (ii)
freezing in air and thawing in water.
B-2 The test for fundamental transverse
frequency shall be conducted on concrete prism
specimens (100 mm 100 mm 400 mm or
150 mm 150 mm 600 mm) or on concrete
cylinder specimens (150 mm in dia 300 mm
length). The test shall commence at the age of
14 days (water-curing till then) by electro-
dynamic method in accordance with IS 516.
The relative dynamic modulus of elasticity
shall be calculated as follows:
where
The relative durability factor shall be
calculated as follows:
DF (or DF
1
) = PN/300
RDF = DF/DF
1
100
where
ANNEX C
( Clause 7.2.1.1 )
METHOD OF DETERMINATION OF FLOW OF CONCRETE OF HIGH WORKABILITY
C-0 This method covers determination of the
flow of fresh mixed superplasticized concrete of
high workability.
C-1 APPARATUS
C-1.1 The Slump Cone
The slump cone for receiving the freshly mixed
concrete shall consist of a frustrum of cone of
minimum thickness of 1.5 mm metal, with the
following internal dimensions:
The slump cone shall be provided with two
metal foot pieces at the bottom and two handles
at the top.
C-1.2 Tamping Bar
The tamping bar shall be made of hardwood
and having a 40 mm 40 mm section of length
200 mm, with a circular section to form a
handle to the bar.
P
c
=
P
c
= relative dynamic modulus of
elasticity (percent), after C cycles
of freezing and thawing;
n
2
2
/n
1
2
100
n
1
= fundamental transverse frequency
at zero cycle of freezing and
thawing; and
n
2
= fundamental transverse frequency
after C cycle of freezing and
thawing.
DF = durability factor of the concrete
containing the admixture under
test,
DF
1
= durability factor of the concrete
containing the reference
admixture,
P = relative dynamic modulus of
elasticity in percentage of the
dynamic modulus of elasticity at
zero cycle (values of P will be 60 or
greater), and
N = number of cycles at which P
reaches 60 percent, or 300 if P
does not reach 60 percent prior to
the end of the test (300 cycles).
Diameter of the base : 200 2 mm
Diameter of top : 130 2 mm
Height : 200 2 mm
IS 9103 : 1999
8
C-1.3 Flow Table Apparatus
The flow table apparatus shall be constructed
in accordance with Fig. 1A and 1B. Flow table
top shall be constructed from a flat metal plate
of minimum thickness 1.5 mm. The top shall
have a plan area of 700 mm 700 mm and a
flatness of within 1.5 mm. The centre of the
table shall be scribed with a cross, the lines of
which run parallel to and out to the edges of the
plate, and with a central circle 200 mm in
diameter. The under surface of the plate shall
be reinforced in order to prevent distortion of
the flat surface. The front of the flow table top
shall be provided with a lifting handle as shown
in Fig. 1. The total mass of the flow table top
shall be 16 1 kg.
The flow table top shall be hinged to a base
frame using externally mounted hinges in such
a way that no aggregate can become trapped
easily between the hinges or hinged surfaces.
The front of the base frame shall extend a
minimum 120 mm beyond the flow table top in
order to provide a top board. An upper stop
similar to that shown in Fig. 1A shall be
provided on each side of the table so that the
lower front edge of the table can only be lifted
40 1 mm.
The lower front edge of the flow table top shall
be provided with two hard rigid stops which
transfer the load to the base frame. The base
frame shall be so constructed that this load is
then transferred directly to the surface on
which the flow table is placed so that there is
minimal tendance for the flow table top to
bounce when allowed to fall.
C-1.4 Accessory Apparatus
C-1.4.1 Mould
The mould shall be made of a metal readily not
attacked by cement paste or liable to rust and of
minimum thickness 1.5 mm. The interior of the
mould shall be smooth and free from projections,
such as protruding rivets, and shall be free from
dents. The mould shall be in the form of a hollow
frustrum of a cone having the internal
dimensions as shown in Fig. 2. The base
All dimensions in millimetres.
FIG. 1 FLOW TABLE
IS 9103 : 1999
9
and the top shall be open and parallel to each
other and at right angles to the axis of the cone.
The mould shall be provided with two metal foot
pieces at the bottom and two handles above them.
C-1.4.2 Tamping Bar
The tamping bar shall be made of a suitable
hardwood and having dimensions as shown in
Fig. 3.
C-2 SAMPLING
C-2.1 The sample of freshly mixed concrete
shall be obtained in accordance with the
provisions given in IS 1199.
C-3 PROCEDURE
The flow table shall be level and properly
supported. Before commencing the test, the
table-top and inner surface of the mould shall
be wiped with a damp cloth. The slump cone is
placed centrally on the table and to be held in
position by standing on the two foot pieces. The
slump cone is to be filled with concrete in two
equal layers, each layer tamped lightly 10
times with the wooden tamping bar. After
filling the mould, the concrete is to be struck off
flush with the upper edge of the slump cone and
the free area of the table-top cleaned off.
Half a minute after striking off the concrete,
the cone shall be slowly raised vertically by the
handles. After this, the table-top raised by the
handle and allowed to fall 15 times in 15 s. The
concrete spreads itself out. The diameter of the
concrete spread shall then be measured in two
directions, parallel to the table edges. The
arithmetic mean of the two diameters shall be
the measurement of flow in millimetres.
ANNEX D
( Clause 7.2.4 )
METHOD OF TEST FOR BLEEDING OF CONCRETE
D-0 This method covers determination of the
relative quantity of mixing water that will
bleed from a sample of freshly mixed concrete.
D-1 APPARATUS
D-1.1 Measure
A cylindrical container of approximately 0.01 m
3
capacity, having an inside diameter of 250 mm
and inside height of 280 mm. The container shall
be made of metal of minimum thickness of 4 mm
and shall be externally reinforced around the top
with metal band 38 mm wide and 4 mm thick.
The inside shall be smooth and free from
corrosion, coating, or lubricants. Suitable
handles should be provided, properly welded on
the outer surface of the container, on the
opposite sides in centre, so as to enable
lifting/handling of the container with concrete.
D-1.2 Tamping Bar
The tamping bar shall be a round-ended steel
bar of 16 mm diameter and 600 mm length.
D-1.3 Pipette
A pipette for drawing off free water from the
surface of the test specimens.
D-1.4 Graduated Jar
A graduated jar of 100 cm
3
capacity.
D-2 SAMPLING
The sample of freshly mixed concrete shall be
obtained in accordance with the provisions
given in IS 1199 except when small batches are
made under laboratory conditions.
All dimensions in millimetres.
FIG. 2 CONCRETE MOULD
All dimensions in millimetres.
FIG. 3 TAMPING BAR
IS 9103 : 1999
10
D-3 PROCEDURE
D-3.1 Compacting
The container shall be filled with concrete as
soon as practicable after mixing to a height of
250 3 mm. The concrete shall be filled into the
measure in layers approximately 50 mm deep
and each layer shall be compacted by hand.
D-3.1.1 Compacting by Hand
When compacting by hand, tamping with the
tamping bar shall be distributed in a uniform
manner over the cross-section of the measure.
The number of strokes per layer required to
produce the specified condition will vary
according to the type of concrete, but in no case
shall the concrete be subjected to less than 60
strokes per layer for the 0.01 m
3
measure.
Then, the top surface of the concrete shall be
levelled to a reasonably smooth surface by a
minimum amount of trowelling.
D-3.2 The test specimen shall be kept at a
temperature of 27 2C. Immediately after
trowelling the surface of test specimens the
time as well as the mass, of the cylinder and its
contents shall be recorded. The container shall
be kept on a level surface free from vibration
and covered with a lid. Water accumulated at
the top shall be drawn off by means of a pipette,
at 10 min intervals during the first 40 min and
at 30 min intervals subsequently till bleeding
ceases. To facilitate collection of bleeding
water, the specimen may be tilted by placing a
50-mm block under one side of the measure
during collection of water. The water shall be
transferred to graduated jar and accumulated
quantity of water shall be recorded after each
transfer.
D-4 CALCULATION
Accumulated bleeding water expressed as a
percentage of the net mixing water shall be
calculated as follows:
where
ANNEX E
( Clause 10.1 )
CHARACTERISTIC PROPERTIES OF ADMIXTURE
E-1 DRY MATERIAL CONTENT
The dry material content in the liquid or
non-liquid samples shall be determined
according to the following procedures.
E-1.1 Liquid Admixture
Place 25 to 30 g of preheated, completely dry
sand in a wide mouth glass weighing bottle (60
mm dia, 30 mm height) provided with ground
glass stopper. Place the bottle with sand and
stopper in the electric oven and dry for 17 1/4
h at 105 2C. (The period of drying may be
shortened if sand is already dry.) Transfer the
bottle with stopper to a desiccator and allow to
cool to room temperature and weigh nearest to
0.001 g. Remove the stopper and with the help
of a pipette evenly distribute 4 ml of the liquid
over the sand. Insert the stopper and place the
bottle and stopper in the oven. Dry for 17 + 1/4
h at 105 2C. At the end of the drying period
transfer to a desiccator, cool to room
temperature. Stopper the weighing bottle and
weigh to nearest 0.001 g. Again place the bottle
and stopper in the oven for one hour and repeat
the drying and the weighing etc. The weight
should become constant.
Calculation:
Find the weight of sample and the dried
residue.
Bleeding water percentage =
V
w
= total mass of the bleeding water, kg;
w = net mass of water in the batch, kg;
W = total mass of the batch, kg; and
s = the mass of sample, kg.
V
w
w
W
----- s
--------100
Weight of bottle and sand = W
1
Weight of bottle, sand and
sample
= W
2
Weight of sample = W
2
W
1
Weight of bottle, sand and
dried residue
= W
3
Weight of dried residue = W
3
W
1
Percent residue on drying =
W
3
W
1
W
2
W
1
------------------------ - 100
IS 9103 : 1999
11
E-1.2 Non-Liquid Admixture
Place about 3 g of the non-liquid sample into an
already weighed dried tared glass stoppered
weighing bottle to the nearest 0.001 g. Remove
the stopper and immediately place both stopper
and bottle in the drying oven. Dry for 17 + 1/4 h
at 105 2C. At the end of the drying period
transfer the bottle and stopper to a desiccator,
cool to room temperature, stopper the bottle
and weigh to nearest 0.001 g. Calculate as
above in E-1.1.
E-2 ASH CONTENT
The ash content which gives an indication of
inorganic constituents, is determined by
igniting the admixture at 600C to remove any
organic material. Place, accurately weighed to
the nearest 0.001 g, about 1 g of the sample to a
clean pre-ignited and accurately weighed silica
or porcelain crucible. Then place the crucible
over a steam water bath or an air oven, at 90C
to remove the liquid portion by evaporation.
Finally transfer the crucible with its solid
contents to a muffle furnace at room
temperature and heat gradually so that the
temperature reaches 300C in 1 h and 600C in
a further 2 to 3 h period. Maintain the
temperature of the furnace at 600 25C for 16
to 24 h. Remove the crucible from the furnace,
cool, covered with its lid in the desiccator. After
cooling for 30 min, weigh the crucible plus lid
and contents to the nearest 0.001 g.
Calculate the ash content in the original mass
of the superplasticizer:
E.3 RELATIVE DENSITY OF LIQUID
ADMIXTURE
E-3.1 Apparatus
Following apparatus shall be used:
Place about 400 ml of admixture in a 500-ml
graduated cylinder avoiding the formation of
air bubbles in the liquid. Allow the temperature
of the liquid to be 20 5C. Hold the
temperature of the stem and insert it into the
liquid in the cylinder. Insert the hydrometer
into the cylinder in such a way that it floats
free and does not touch the side of the cylinder.
Release the hydrometer when approximately in
the equilibrium position. When it has reached
the equilibrium read the scale at the bottom of
the meniscus for transparent liquids or where
the meniscus merges with the stem of the
hydrometer for opaque liquids to report the
relative density.
E-4 CHLORIDE ION CONCENTRATION
The chloride ion content in an admixture shall
be determined as given in IS 6925.
E-5 pH
The hydrogen ion concentration represented by
pH value of the liquid superplasticizer shall be
determined with the help of a suitable pH
meter.
Weight of crucible and lid = W
1
Weight of crucible, lid and
sample
= W
2
Weight of crucible, lid and ash = W
3
Ash content =
a) Constant temperature bath,
b) Hydrometer, and
c) Measuring cylinder.
W
3
W
1
W
2
W
1
------------------------ -100
IS 9103 : 1999
12
ANNEX F
( Foreword )
COMMITTEE COMPOSITION
Cement and Concrete Sectional Committee, CED 2
Chairman
DR H. C. VISVESVARYA
Chandrika, 63-64 East Park Road, Malleswaram, Bangalore 560003
Members Representing
SHRI H. BHATTACHARYA Orissa Cement Limited, New Delhi
SHRI G. R. BHARTIKAR B. G. Shirke & Co, Pune
DR A. K. CHATTERJEE The Associated Cement Companies Ltd, Mumbai
SHRI S. H. SUBRAMANIAN ( Alternate )
CHIEF ENGINEER (DESIGN) Central Public Works Department, New Delhi
SUPERINTENDING ENGINEER (S&S) ( Alternate )
CHIEF ENGINEER, NAVAGAM DAM Sardar Sarovar Nirman Nigam Ltd, Gandhinagar
SUPERINTENDING ENGINEER, QCC ( Alternate )
CHIEF ENGINEER (RESEARCH-CUM-DIRECTOR) Irrigation and Power Research Institute, Amritsar
RESEARCH OFFICER CONCRETE TECHNOLOGY ( Alternate )
DIRECTOR A. P. Engineering Research Laboratories, Hyderabad
JOINT DIRECTOR ( Alternate )
DIRECTOR (CMDD) (N&W) Central Water Commission, New Delhi
DEPUTY DIRECTOR (CMDD) (NW&S) ( Alternate )
SHRI K. H. GANGWAL Hyderabad Industries Ltd, Hyderabad
SHRI V. PATTABHI ( Alternate )
SHRI V. K. GHANEKAR Structural Engineering Research Centre (CSIR), Ghaziabad
SHRI S. GOPINATH The India Cements Ltd, Chennai
SHRI R. TAMILAKARAN ( Alternate )
SHRI S. K. GUHA THAKURTA Gannon Dunkerley & Co Ltd, Mumbai
SHRI S. P. SANKARANARAYANAN ( Alternate )
SHRI N. S. BHAL Central Building Research Institute (CSIR), Roorkee
DR IRSHAD MASOOD ( Alternate )
DR IRSHAD MASOOD Cement Corporation of India, New Delhi
SHRI N. C. JAIN ( Alternate )
JOINT DIRECTOR STANDARDS (B&S) (CB-I) Research, Designs and Standards Organization (Ministry of
Railways), Lucknow
JOINT DIRECTOR STANDARDS (B&S) (CB-II) ( Alternate )
SHRI N. G. JOSHI Indian Hume Pipes Co Ltd, Mumbai
SHRI P. D. KELKAR ( Alternate )
SHRI D. K. KANUNGO National Test House, Calcutta
SHRI B. R. MEENA ( Alternate )
SHRI P. KRISHNAMURTHY Larsen and Toubro Limited, Mumbai
SHRI S. CHAKRAVARTHY ( Alternate )
DR A. G. MADHAVA RAO Structural Engineering Research Centre (CSIR), Chennai
SHRI K. MANI ( Alternate )
CHAIRMAN-CUM-MANAGING DIRECTOR Hospital Services Consultancy Corporation (India) Ltd, New Delhi
SHRI J. SARUP ( Alternate )
( Continued on page 13 )
IS 9103 : 1999
13
( Continued from page 12 )
Members Representing
SHRI PRAFULLA KUMAR Ministry of Transport, Department of Surface Transport, Roads
Wing, New Delhi
SHRI P. P. NAIR ( Alternate )
MEMBER SECRETARY Central Board of Irrigation and Power, New Delhi
DIRECTOR (CIVIL) ( Alternate )
SHRI SUDESH DHIMAN, CE Engineer-in-Chiefs Branch, Army Headquarters, New Delhi
SHRI DINESH SIKAND, ADDITIONAL CE ( Alternate )
SHRI Y. R. PHULL Central Road Research Institute (CSIR), New Delhi
SHRI S. S. SEEHRA ( Alternate )
SHRI Y. R. PHULL Indian Roads Congress, New Delhi
SHRI A. K. SHARMA ( Alternate )
DR C. RAJKUMAR National Council for Cement and Building Materials, New Delhi
DR K. MOHAN ( Alternate )
SHRI G. RAMDAS Directorate General of Supplies and Disposals, New Delhi
SHRI R. C. SHARMA ( Alternate )
SHRI S. A. REDDI Gammon India Ltd, Mumbai
REPRESENTATIVE Builders Association of India, Mumbai
SHRI J. S. SANGANERIA Geological Survey of India, Calcutta
SHRI L. N. AGARWAL ( Alternate )
SHRI S. B. SURI Central Soil and Materials Research Station, New Delhi
SHRI N. CHANDRASEKARAN ( Alternate )
SUPERINTENDING ENGINEER (DESIGN) Public Works Department, Government of Tamil Nadu, Chennai
EXECUTIVE ENGINEER (S. M. R. DIVISION) ( Alternate )
SHRI A. K. CHADHA Hindustan Prefab Ltd, New Delhi
SHRI J. R. SIL( Alternate )
DR H. C. VISVESVARAYA The Institution of Engineers (India), Calcutta
SHRI D. C. CHATURVEDI ( Alternate )
SHRI VINOD KUMAR,
Director (Civ Engg)
Director General, BIS ( Ex-officio Member )
Member-Secretary
SHRI J. K. PRASAD
Additional Director (Civ Engg), BIS
Concrete Subcommittee, CED 2 : 2
Convener
DR A. K. MULLICK National Council for Cement and Building Materials, New Delhi
Members
SHRI C. R. ALIMCHANDANI Stup Consultants Ltd, Mumbai
SHRI S. RANGARAJAN ( Alternate )
DR P. C. CHOWDHARY Torsteel Research Foundation in India, Calcutta
DR C. S. VISHWANATH ( Alternate )
SHRI J. P. DESAI Gujarat Ambuja Cement Ltd, Ahmedabad
SHRI B. K. JAGETIA ( Alternate )
DIRECTOR Central Soil Materials Research Station, New Delhi
SHRI N. CHANDRASEKARAN ( Alternate )
JOINT DIRECTOR STANDARDS (B&S)/CB-II Research, Designs and Standards Organization, Lucknow
JOINT DIRECTOR STANDARDS (B&S)/CB-I ( Alternate )
( Continued on page 14 )
IS 9103 : 1999
14
( Continued from page 13 )
Members Representing
SUPERINTENDING ENGINEER (DESIGNS) Central Public Works Department, New Delhi
EXECUTIVE ENGINEER (DESIGNS) ( Alternate )
SHRI V. K. GHANEKAR Structural Engineering Research Centre, Ghaziabad
SHRI D. S. PRAKASH RAO ( Alternate )
SHRI S. K. GUHA THAKURTA Gannon Dunkerley and Co Ltd, Mumbai
SHRI S. P. SANKARANARAYANAN ( Alternate )
SHRI J. S. HINGORANI Associated Consulting Services, Mumbai
SHRI A. P. REMEDIOS ( Alternate )
SHRI LALIT KUMAR JAIN In personal capacity ( Consulting Structural Engineer 36, Old
Sneh Nagar, Wardha Road, Nagpur 440015 )
SHRI M. P. JAISINGH Central Building Research Institute (CSIR), Roorkee
SHRI B. KAMESWARA RAO ( Alternate )
CHIEF ENGINEER & JOINT SECRETARY Public Works Department, Mumbai
SUPERINTENDING ENGINEER ( Alternate )
PROF S. KRISHNAMOORTHY Indian Institute of Technology, New Delhi
SHRI K. K. NAYAR ( Alternate )
DR S. C. MAITI National Council for Cement and Building Materials, New Delhi
MANAGING DIRECTOR Hindustan Prefab Ltd, New Delhi
SHRI M. KUNDU ( Alternate )
SHRI M. K. MUKHERJEE Ministry of Transport (Roads Wing), New Delhi
SHRI N. K. SINHA ( Alternate )
SHRI B. V. B. PAL The Associated Cement Co Ltd, Mumbai
SHRI M. G. DANDAVATE ( Alternate )
SHRI A. B. PHADKE The Hindustan Construction Co Ltd, Mumbai
SHRI D. M. SAVUR ( Alternate )
SHRI Y. R. PHULL Central Road Research Institute, New Delhi
SHRI S. S. SEEHRA ( Alternate I )
SHRI SATENDER KUMAR ( Alternate II )
SHRI A. S. PRASAD RAO Structural Engineering Research Centre (CSIR), Chennai
SHRI K. MANI ( Alternate )
SHRI K. L. PRUTHI National Building and Construction Corporation Ltd, New Delhi
SHRI J. R. GABRIEL ( Alternate )
SHRI B. D. RAHALKER Nuclear Power Corporation, Mumbai
SHRI U. S. P. VERMA ( Alternate )
SHRI HANUMENTHA RAO A. P. Engineering Research Laboratories, Hyderabad
SHRI G. RAMAKRISHNEN ( Alternate )
SHRI S. A. REDDI Gammon India Ltd, Mumbai
DR N. V. NAYAK ( Alternate )
SHRI S. C. SAWHNEY Engineers India Ltd, New Delhi
SHRI R. P. MEHROTRA ( Alternate )
SHRI J. R. SHARMA Army Headquarters, Engineer-in-Chiefs Branch, New Delhi
SHRI SURINDER MOHAN ( Alternate )
PROF M. S. SHETTY Indian Concrete Institute, Chennai
SHRI B. T. UNWALLA In personal capacity ( 15/9, Rustam Baug, Victoria Road,
Mumbai 400027 )
DIRECTOR (C&MDD) Central Water Commission, New Delhi
DEPUTY DIRECTOR (C&MDD) ( Alternate )
Bureau of Indian Standards
BIS is a statutory institution established under the Bureau of Indian Standards Act, 1986 to promote
harmonious development of the activities of standardization, marking and quality certification of goods and
attending to connected matters in the country.
Copyright
BIS has the copyright of all its publications. No part of these publications may be reproduced in any form
without the prior permission in writing of BIS. This does not preclude the free use, in the course of
implementing the standard, of necessary details, such as symbols and sizes, type or grade designations.
Enquiries relating to copyright be addressed to the Director (Publications), BIS.
Review of Indian Standards
Amendments are issued to standards as the need arises on the basis of comments. Standards are also
reviewed periodically; a standard along with amendments is reaffirmed when such review indicates that no
changes are needed; if the review indicates that changes are needed, it is taken up for revision. Users of
Indian Standards should ascertain that they are in possession of the latest amendments or edition by
referring to the latest issue of BIS Catalogue and Standards : Monthly Additions.
This Indian Standard has been developed from Doc : No. CED 2 (5421)
Amendments Issued Since Publication
Amend No. Date of Issue
Amd. No. 1 January 2003
Amd. No. 1 August 2007
BUREAU OF INDIAN STANDARDS
Headquarters:
Manak Bhavan, 9 Bahadur Shah Zafar Marg, New Delhi 110002.
Telephones: 323 01 31, 323 33 75, 323 94 02
Telegrams: Manaksanstha
(Common to all offices)
Regional Offices: Telephone
Central : Manak Bhavan, 9 Bahadur Shah Zafar Marg
NEW DELHI 110002
323 76 17
323 38 41
Eastern : 1/14 C. I. T. Scheme VII M, V. I. P. Road, Kankurgachi
KOLKATA 700054
337 84 99, 337 85 61
337 86 26, 337 91 20
Northern : SCO 335-336, Sector 34-A, CHANDIGARH 160022 60 38 43
60 20 25
Southern : C. I. T. Campus, IV Cross Road, CHENNAI 600113 235 02 16, 235 04 42
235 15 19, 235 23 15
Western : Manakalaya, E9 MIDC, Marol, Andheri (East)
MUMBAI 400093
832 92 95, 832 78 58
832 78 91, 832 78 92
Branches : AHMEDABAD. BANGALORE. BHOPAL. BHUBANESHWAR. COI MBATORE.
FARI DABAD. GHAZI ABAD. GUWAHATI . HYDERABAD. JAI PUR. KANPUR.
LUCKNOW. NAGPUR. NALAGARH. PATNA. PUNE. RAJKOT. THIRUVANANTHAPURAM.
VISHAKHAPATNAM.