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The document appears to be a test containing multiple choice questions about materials characterization techniques like thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), thermomechanical analysis (TMA), and dynamic mechanical analysis (DMA). It tests understanding of concepts like glass transition temperature (Tg), melting point (Tm), crystallization temperature (Tc), and how material properties are reflected in the outputs of these analytical techniques.

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72 views6 pages

User Course Test Started Submitted Due Date Status Attempt Score Time Elapsed

The document appears to be a test containing multiple choice questions about materials characterization techniques like thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), thermomechanical analysis (TMA), and dynamic mechanical analysis (DMA). It tests understanding of concepts like glass transition temperature (Tg), melting point (Tm), crystallization temperature (Tc), and how material properties are reflected in the outputs of these analytical techniques.

Uploaded by

Aranas Trisha
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd
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User EDDIE ROM EXEQUIEL ORDOÑEZ REGUINDIN

Course THERMODYNAMICS AND PHASE EQUILIBRA OF MATERIALS


LABORATORY
Test MSE 102L Finals
Started 4/16/19 9:01 PM
Submitted 4/16/19 10:18 PM
Due Date 4/16/19 11:00 PM
Status Completed
Attempt 21 out of 0 points  
Score
Time 1 hour, 17 minutes out of 2 hours
Elapsed
Tuesday, April 16, 2019 10:18:52 PM PHT

The longer the chains are, the higher the melt index.
 True
 False

1. The bigger the pendant groups are, and the bigger the components of the backbone, the
lower is the melt index of a polymer.
 True
 False

2. Covalent bond in polymers is a weaker bond than ionic bond because polymers are more
stretchable than ceramics.
 True
 False

Question 4
Recrystallization happens as observed in a TMA curve of a
thermoplastic polymer in order to
a
. gain more energy
b increase the degradation of the
. polymer
c
. increase the Tg of the polymer
d refine even more the crystallized
. region

Question 5
In DMA, the G’ and G” of a material can be compared during glass
transition, crystallization, recrystallization and melting.
 True
 False

Question 6
The addition of a more amorphous polymer to a more crystalline one
gives us lower Td.
 True
 False

Question 7
In the TMA curve of a thermoplastic polymer, the smaller the slope of
stage 3, the ________ is the CTE.
lower

Question 8
In DMA, the modulus G’’ gives information on the _________ of the
members (atoms or molecules) in the material as it is continuously
subjected to a cyclic load while the temperature increases. Note:
Answer is in two words.
viscous flow

Question 9
In TGA, H 2O and CO 2 gases form at a higher rate
a
. after melting of the polymer
b before gas atmosphere
. exchange
c after the gas atmosphere
. exchange
d during polymer
. decomposition

Question 11
Crystallization occurs after Tg because
a
. it has to release heat to become stable
b
. none of the above
c crystalline regions break bonds and then form
. again after Tg
d amorphous regions becomes mobile enough to
. crystallize

Question 12
Theoretically, ‘pure’ amorphous polymers will only have Tg and no
melting point.
 True
 False

Question 13
During the solidifcation of polymerized monomers, fewer crystalline
regions are formed because
a of slow
. cooling
b of fast
. cooling
c of longer
. chains
d of heat
. losses

Question 14
Melting point occurs at higher temperatures since
a
. none of the above
b amorphous regions have high
. energy bonds
c crystalline regions have high energy
. bonds
d crystalline regions have low energy
. bonds

Question 15
In a DMA curve, the loss modulus (G”) is highest 
a
. at Tg
b at higher
.
temperatures
c
. at Tm
d
. at Tc

Question 16
In DMA, the modulus G’ gives information on the _________ between or
among members (atoms or molecules) of the material as it is
continuously subjected to a cyclic load while the temperature
increases. Note: Answer is in two words.
Elastic Modulus

Question 17
In the DMA curve of a thermoplastic polymer, G’’ increases again after
an increase during glass transition because of ________.

Question 18
The smaller the difference between loss modulus and shear (elastic)
modulus of a thermoplastic polymer, the ________ is the _________
coefficient. Note: Use ‘and’ to separate your answers.
lower and damping

Question 19
Peaks in a DSC curve represent the latent heat of the process.
 True
 False

Question 20
Stage 6 in a DSC Curve shows an exothermic peak because
a the heat is continuously abosrbed by the
. material
b
. of sample’s reaction to oxygen
c
. the sample disappear
d
. the sample degrades

Question 21
Carbon black is formed when _______ reacts with ________.
a
. Hydrocarbons ; water
b
. Hydrocarbons ; CO2
c Comprex Hydrocarbons ;
. oxygen
d Complex Hydrocarbons ;
. CO2

Question 22
In the DMA curve of a thermoplastic polymer, G’ increases again after
a decrease during glass transition because of ________.
crystallization

Question 23
The purpose of changing the gas atmosphere from N 2 to Air is
a
. to achieve stability of the polymer
b to increase decomposition of the
. polymer
c
. N2   is toxic
d to increase heat absorption of the
. polym

Question 24
The higher the damping coefficient, the more resistant is the material
to high-temperature cyclic loads.
 True
 False

Question 25
In stage 2 of the TGA curve, the polymer is already melted.
 True
 False

Question 26
In TMA, the highest expansion occurs
a
. at Tg
b
. at Tc
c right after
. Tm
d right before
. Tm

Question 27
In a DSC apparatus, the reference pan absorbs less heat than the
sample pan.
 True
 False

Question 30
The addition of a more amorphous polymer to a more crystalline
polymer will give higher percent mass decrease during the final
decomposition process.
 True
 False

Question 28
In DMA, the modulus G’ is inversely proportional to the bond length of
the members (atoms or molecules) of a polymer.
 True
 False

Question 29
Thermosets do not melt because
a
. of low Td
b they’re bound by primary
. bonds
c
. their Tm is very high
d melting happens instead of
. Tg

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