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CHM 229 Updated Course Compact PDF

This document provides information about the Experimental Analytical Chemistry course offered at Covenant University's College of Science and Technology. The course is a 1 unit practical component of the CHM222 course. It will cover topics like sampling techniques, solvent extraction, separation methods, and chromatography. Students will learn quantitative chemical analysis principles and skills. They will be assessed based on practical lab scores. Safety regulations must be strictly followed during laboratory exercises. The course aims to build students' analytical skills for chemical analysis.

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Glory Usoro
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61 views2 pages

CHM 229 Updated Course Compact PDF

This document provides information about the Experimental Analytical Chemistry course offered at Covenant University's College of Science and Technology. The course is a 1 unit practical component of the CHM222 course. It will cover topics like sampling techniques, solvent extraction, separation methods, and chromatography. Students will learn quantitative chemical analysis principles and skills. They will be assessed based on practical lab scores. Safety regulations must be strictly followed during laboratory exercises. The course aims to build students' analytical skills for chemical analysis.

Uploaded by

Glory Usoro
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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COVENANT UNIVERSITY

College: College of Science and Technology

Department: Chemistry

Course lecturer: Dr. Anake W. U., Dr. Etchie A. T., Dr. Adedapo E. A., Mrs. Fred-
Ahmadu O.H., Mrs. Oloyede O. M.

Programme: Industrial Chemistry

Course Code: CHM 229

Course Title: Experimental Analytical Chemistry

Course Units: 1

Session: 2019/2020

Semester: Omega

Time: 10 am

Location: Hall 111

a) Brief Overview of Course: The course is the practical component of CHM222


course. Topics include sampling technique and statistical treatment of data,
solvent extraction, simple separation techniques and chromatography.

b) Course Objectives/Learning Goals: At the end of this course, students are


expected to:
i. Understand the concept of quantitative chemical analysis.
ii. Understand the theory and basic principles of separation techniques.
iii. Be able to carry out chemical analysis under sound analytical practices
and skills.

c) Methods of Instruction for laboratory Exercise:


i. Teaching
ii. Classroom interaction
iii. Practical demonstration
iv. Use of practical manual and reporting datasheet

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d) Course Outlines:
Module 1: Introduction to Experimental Analytical Chemistry
Week 1: Introduction to Experimental Analytical Chemistry Dr. Etchie A. T.

Module 2: Statistical Analysis of Data


Week 2: Application of chemometrics in Experimental Analytical Chemistry
Dr. Adedapo E. A.
Week 3: Calibration of volumetric glassware Dr. Etchie A. T.

Module 3: Solvent Extraction


Week 4: Separation of organic mixture by solvent extraction Mrs. Oloyede O. M.

Module 4: Chromatography
Week 5: Separation of acetaminophen, acetylsalicylic acid, ascorbic acid and an
unknown mixture Mrs. Fred-Ahmadu O.H.
Week 6: Thin layer chromatography: separation of amino acid Dr. Adedapo E. A.
Week 7: Column chromatography Dr. Anake W. U.

Module 5: Redox Titration


Week 8: Determination of ascorbic acid in food / drink sample
Mrs. Oloyede O. M.
Week 9: Determination of ascorbic acid in vitamin C tablet
Mrs. Fred-Ahmadu O.H.

e) Structure of the Programme/Method of Grading: Practical scores over 100 marks

f) Ground Rules & Regulations: Strict adherence to conventional safety rules


regarding ethics and conducts in the laboratory. These include but not limited to:
i. Use of lab coat
ii. Prohibition of dangerous practices such as eating or playing while working
in the laboratory
iii. Bench surface should be kept clean and all reagent bottles clearly labelled
iv. All glass wares or lab wares must be washed before and after use

g) Alignment with Covenant University Vision/Goals: Capacity building – students


will acquire skills necessary for conducting chemical analyses under sound
analytical practices.

h) Recommended Reading/Text: Manahan, Stanley E. Fundamentals of


environmental Chemistry. CRC Press LLC, 2001.

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