Design of A Table Salt Processing Plant
Design of A Table Salt Processing Plant
A Design Proposal
Presented to
Iloilo City
In Partial Fulfillment
By
October 2019
Chapter I
Introduction
expensive and labor-intensive to harvest the mass quantities of salt necessary for food
preservation and seasoning. Salt was also used to clean food since bacteria and viruses cannot
live in a salt environment. This made salt an extremely valuable commodity. Entire economies
were based on salt production and trade. Though no longer presently a valuable commodity in
the monetary sense, salt is still valuable in the sense of being crucial to human health. Common
salt (sodium chloride) is 40% sodium and 60% chloride. An average adult consumes about 7 kg
Salt can be found deposited in Earth’s layers in rock salt deposits. These deposits formed
when the water in the oceans that covered Earth many millions of years ago evaporated. The salt
Salt plays a crucial role in maintaining human health. It is the main source of sodium and
chloride ions in the human diet. Sodium is essential for nerve and muscle function and is
involved in the regulation of fluids in the body. Sodium also plays a role in the body’s control of
blood pressure and volume. Although sodium is essential, people who consume too much
sodium may have hypertension or high blood pressure, a condition that can lead to serious
Electrolytes are compounds, often salts, which dissociate into their ionic components in solvents
like water. Chloride is also a crucial component in the production of stomach acid (HCl).
Humans excrete salt when sweating and must replenish these lost sodium and chloride ions
Salt production is one of the oldest chemical practices performed by man. Although salt
is produced naturally when seawater evaporates, the process can easily be reproduced to create a
higher yield. There are two main sources of salt. It is harvested directly either from sea water or
natural brine, or from rock salt deposits formed by the evaporation of earlier seas that left a layer
of rock salt, otherwise known as halite. There are three types of salt extraction: solar evaporation,
rock salt mining and vacuum evaporation. Each one involves specific technology and
manufacturers select the most appropriate technique depending upon the particular topographic
and socio-economic conditions in their area of operation. Some salt is still produced using
ancient methods, but new, faster, and less expensive methods have been developed. Depending
on the source of the salt and the technique used to create it, the end product will have different
The worldwide production of salt is more than 200 million tons. As per the available
statistics, the salt industry is dominated by five nations. These are China, the US, India, Canada
and Germany. The salt industry located in Germany, Australia, Mexico, Chile, Brazil and the
United Kingdom also produces a massive amount of salt annually. The top salt exporters are the
Netherlands, Canada and Germany while the top salt importers are the United States, China and
Japan (Sheth, 2017). The Philippines, being an archipelago is also abundant with the
geographical means to harvest salt and Occidental Mindoro accounts for 40% of the Philippines’
salt production.
This project aims to design an efficient and economical table salt manufacturing plant.
Chapter II
Concept Stage
Market Analysis
The industrial salt market was valued at USD 12.70 Billion in 2016 and is projected to
reach USD 14.93 Billion by 2022, at a CAGR of 2.8% from 2017 to 2022. The growth of the
chlor-alkali industry is driving the growth of the industrial salt market in the chemical processing
application. The growing use of industrial salt in de-icing and water treatment applications is
The rock salt segment of the industrial salt market is projected to witness a higher growth
during the forecast period. The growth of this segment of the market can be attributed to the
availability of large reserves of salt in salt mines. Rock salt is also commonly referred as halite.
Rock salt generally comprises of sodium chloride with impurities such as gypsum (CaSO4) and
sylvite (KCl). Rock salt deposits are found buried underground in arid regions, such as dry lake
beds, inland marginal seas, enclosed bays, and estuaries. These rock salts are mined either by
conventional mining, continuous mining equipment, or solution mining processes. Rock salt are
cheaper as compared to natural brine salt, due to the challenges in the evaporation process of
brine salt.
industrial salt market is projected to witness the highest growth during the forecast period. The
large availability of rock salt deposits and landscape of these mines favoring the mining process
is expected to drive the conventional mining process segment of the industrial salt market.
Figure 1. U.S. Industrial Salts Market Revenue
Global salt consumption is forecast to grow 1.9 percent annually through 2020 to 335
million metric tons, valued at $14.1 billion. Steady gains in the Asia/Pacific and Africa/Mideast
The average price for salt across the world is forecast to rise 2.0 percent per year to $42
per metric ton in 2020, rebounding from a low 2015 base. A strong dollar and a collapse in
commodity prices put downward pressure on dollar-denominated salt prices across the globe in
2014 and 2015. Through 2020, however, a more stable commodities market and increases in
Rock salt is another name for the mineral halite which is commonly known as sodium
chloride and has a chemical formula NaCl. It is formed by the evaporation of salty water from
large water bodies such as inland marginal seas, enclosed bays and estuaries in semi-arid regions
municipally for managing ice, because it has lower freezing point than pure water. It is also used
North America stood at the second largest market for rock salt in terms of revenue in
2016. The region’s market has been strengthened by robust sales of deicing salt in U.S. and
Canada.
Figure 3. Producer Price Index by Commodity for Chemicals and Allied Products: Rock Salt
Salt Brine Market
Brine fluid is a solution obtained when a salt usually sodium chloride is saturated in some
amount of water. Brine contains a very high salt content, which prevents the growth of bacteria
and thus help preserve the food items. The type of brine solution may vary with the variation in
the mixing proportions of salt with water. Brine fluids are typically formulated with inorganic
salts. These fluids are specifically manufactured to control formation pressure as well as reduce
The Global Brine Fluids market has witnessed rapid growth in recent years and this trend
is estimated to continue in coming years as well. Brine fluid is basically a solution of salt and
water. It is used as a preservative for food products through the process of brining. Brine
contains a very high salt content which prevents the growth of bacteria and thus help preserve the
food items. It also has industrial applications in medical and oil and gas industry.
The global brine fluids market is witnessing growth owing to the increasing consumption
in the regions of North America and Asia-Pacific. Manufacturers are investing heavily in
expansions and mergers & acquisitions in order to enhance their market share and revenue as
well as to fulfill the increasing demand for brine in various end-use applications. North America
leads the global brine fluids market with a market share of 50% in 2014.
Almost 85% of the total brine demand was from the oil and gas application in 2014. The
medical industry is seen as the fastest-growing end-use segment in coming years owing to the
increasing demand for medical services globally. The drivers of the global brine fluids industry
are extensive drilling activities, increasing demand for conventional and non-conventional
been discussed in detail in the report. It also covers the profiles of leading players of this industry
with their recent developments and other strategic industry activities. Currently, the global
market is served by Israel Chemicals Limited (Israel), Albemarle Corporation (U.S.), Chemtura
Corporation (U.S.), Jordan Bromine Company (Jordan), Dow Chemicals (U.S.), Halliburton
(U.S.), M-I SWACO (U.S.), Hindustan Salts Ltd. (India), Tata Chemicals Ltd. (India), and Tetra
Technologies (Texas).
The global salt market size will grow by 31 million metric ton during 2018-2022. This
report offers an analysis of the market based on the type (rock salt, brine, solar salt and others)
and application (chemical processing, road de-icing, food processing and others). The salt market
research report further presents an in-depth insight on the growth prospects of the market across
the Americas, APAC and EMEA. The report analyzes the market’s competitive landscape and
offers information on several companies including Akzo Nobel, Cargill, Compass Minerals,
2019, as consumers have become more health conscious and have reduced their sodium intake.
Over the five years to 2019, industry revenue decreased at an annualized rate of 0.1% to $497.8
million, including a 1.1% increase in 2019. Despite consumers steering away from sodium, table
salt remains a staple of the Western diet, which has helped support industry revenue during the
five-year period. The vast majority of table salt produced in the United States is used in the
production of processed foods sold in grocery stores and restaurants. The remainder is used by
Competitive Analysis
The table salt production industry operates with a high level of market share
concentration. This is due to expanded product line offerings and production capacity levels for
the industry's major players which served to expand the scale of production with which the
company operates.
In 2013, China accounted for over one-quarter of the global salt market, more than any
other single country, producing 68,517,465 tons of salt annually. In the following years, China
continued to represent the leading salt market, while India is projected to rank as the world's
fastest growing salt consumer and ranks third in the global salt production with an estimated
production of 27,006,626 tons. Huge chlor-alkali sectors in China and India primarily drive salt
consumption, supported by solid regional demand for PVC and other downstream products.
Massive population sizes in both countries, combined with ongoing advances in the nations' food
and beverage industries, boosted salt demand in their respective food processing markets. North
America stands as the second largest regional salt market, behind Asia/ Pacific, bolstered by
strong sales of deicing salt in the US and Canada with an estimated production 44,312,914 tons
annually. The US has plenty of salt reserves and deposits in underwater domes and other places,
while 28 companies have the mandate to operate the 67 salt plants in 16 states, including Kansas,
Utah, Louisiana, Ohio, Michigan, and New York. Large food and beverage industries in the
region further propel salt consumption. In Western Europe, Germany, the region's largest
producer of chlor-alkali chemicals, will continue to rank as the leading salt market through 2018.
As stated in the market analysis, there has been an increase in the possible applications of
salt. Aside from it being a staple in cuisines around the world, it is currently used by chemical
In this study, the vacuum evaporation method will be used. With this method, the product
obtained is of a higher purity and it can be used with rock salt or brine as raw material.
Therefore, constraints such as location and raw materials used are less likely to be encounter in
Design Alternatives
Rock Salt
Rock salt (also known as halite) is present in the rocky under layers of the Earth's surface
and can be extracted through deep-shaft mining. These large deposits of salt are the result of
Rock salt is extracted through dynamite, similar in fashion to the mining of any other
mineral. Once it is brought to the Earth's surface, it is crushed and used for industrial and other
non-food purposes. This type of salt contains many minerals and other impurities.
Salt Brines
While the ocean is a natural salt brine, hydraulic mining (or solution mining) of salt
involves pumping water below the earth's surface to dissolve salt deposits and create a salt brine.
This brine is then pumped to the surface and evaporated to create salt. The salty brine may be
treated prior to evaporation to reduce mineral content, yielding a nearly pure sodium chloride
crystal. This method is inexpensive, has a high yield, and produces a very clean salt. Most table
Another method of salt production is the evaporation of salt brine by steam heat in large
commercial evaporators, called vacuum pans. This method yields a very high purity salt, fine in
texture, and principally used in those applications requiring the highest quality salt.
The first part of the operation is known as solution mining. Wells are drilled from several
hundred to 1,000 feet apart into the salt deposit. These wells are connected via lateral drilling, a
recently developed technology. Once the wells are connected, the solution mining operation
begins: water is pumped down one well, the salt below is dissolved, and the resulting brine is
forced to the surface through the other well. It is then piped into large tanks for storage.
Next, the brine is pumped into vacuum pans. These are huge closed vessels under
vacuum about three stories high. They are normally arranged in a series of three, four or five,
with each one in the line under greater vacuum than the preceding one. This series of vacuum
pans operates on a very simple principle: Whenever pressure is lowered, the temperature at
which water will boil is also lowered. For instance, under normal air pressure at sea level, water
boils at 212°F. But at ten thousand feet above sea level, where air pressure is much less, water
In the vacuum pan process, steam is fed to the first pan. This causes the brine in the pan
to boil. The steam from the boiling brine is then used to heat the brine in the second pan. The
pressure in the second pan is lower, allowing the steam made by the boiling in the first pan to
boil the brine in the second pan. The pressure is reduced still further in each succeeding pan.
This allows the steam made by the boiling brine in the previous pan to boil the brine in the next
pan. While the boiling operation could be done with just one pan, several pans in a row produce
more salt per pound of steam, thus allowing greater energy efficiency.
The main impurities in natural brine are calcium, magnesium and sulphate. In open pans
these produce a thick scale on the pan bottom which, with fine pans, must be removed weekly
when the mother liquor from the week’s salt making is run to waste and replaced with fresh
brine. With a vacuum plant it is necessary to remove the scale forming impurities from the brine
some processes the sulphate can be reduced as barium sulphate but usually the evaporator is
operated in such a way that the sulphate level in the mother liquor is not allowed to build up to a
concentration that would permit the crystallization of hydrated sodium sulphate with the salt.
In the early days of the vacuum process it was necessary to discharge the mother liquor
and any build-up of solid impurities in the vessels by “boiling out” which was done every few
days. This reduced the time for salt making and, furthermore, led to a considerable discharge of
brine to the adjacent canal or river. With modern plants, improved methods of brine purification
and evaporator operation have enabled the plant to operate for as much as six months between
This is the oldest method of salt production. It has been used since salt crystals were first
noticed in trapped pools of sea water. Its use is practical only in warm climates where the
evaporation rate exceeds the precipitation rate, either annually or for extended periods, and
ideally, where there are steady prevailing winds. Solar salt production is, typically, the capturing
of salt water in shallow ponds where the sun evaporates most of the water. The concentrated
brine precipitates the salt which is then gathered by mechanical harvesting machines. Any
impurities that may be present in the brine are drained off and discarded prior to harvesting.
Usually two types of ponds are used. First is the concentrating pond, where the salty
water from the ocean or salt lake is concentrated. The second is called the crystallizing pond,
Crystallizing ponds range from to 40 to 200 acres with a foot-thick floor of salt resulting
from years of depositions. During the salt-making season of four to five months, brine flows
continuously through these ponds. This is a saturated brine solution, containing as much salt as it
can hold, so pure salt crystallizes out of the solution as the water evaporates. Natural chemical
There are three systems of evaporating the sea water and/ or brine.
Though production cost will be lower, quality of salt is very much reduced, and the
production rate is also limited. Impounding of sea water in all the ponds and after evaporation
scrapping of salt from all the ponds - a batch wise process – reduced the production cost.
However, complete evaporation in the same pond results in the crystallization of all the salts
The second system, in the process of salt recovery from sea water was made with the
division of the evaporation basin into two: the first basin, usually called nurse pond, was used for
the production of NaCl-saturated brine, which was fed into the second basin, usually called
crystallizer. Thus, it was made possible to achieve continuous salt production (crystallization)
and to eliminate those seawater salts, with less solubility than NaCl (i.e. CaCO3 and CaSO4),
The third and most decisive system concerned was the division of the nurse pond into
several interconnected basins. With this design, sea water enters the first basin and, as it flows
through successive ponds and evaporates in the sun, its concentration increases. This production
method ensures greater control over the concentrations and quantities of the brines fed through
the system, thus resulting in the unobstructed production of much better quality and quantity of
the salt. Nursing ponds cover around 90% (to concentrate brine 2.6 from 3.5 to 26°Be) of the
This production method is still used nowadays for the recovery of salt from sea water,
although there have been improvements and variations, allowing for the production of some
hundred to a few million tons of salt, depending on the size of the area in use (Korovessis and
Lekkas, 1994). These three stages (reservoirs, condensers and crystallizers) constitute the basic
The second oldest method of producing salt is the underground mining. This is probably
the most dramatic method of gathering salt. Large machines travel through vast cave-like
Salt mines are among the safest of mines. They are also the most comfortable to work in.
While mine temperature varies with depth, the average temperature remains about 70° F year-
round.
Salt may appear in veins, as does coal. Veins are the original bedded salt deposits. Salt
also may be found in domes, which were formed when Earth pressures forced salt up through
cracks in the bedrock from depths as great as 30,000 or 40,000 feet; they resemble plugs of
almost-circular shape a few hundred yards to a mile across. Some domes occur close to the
surface. Both domes and veins are mined in a similar way. Most domes in North America are
located in the south from Alabama to Texas with many out under water in the Gulf of Mexico.
To enter a salt mine, miners go down a shaft from the Earth’s surface to the salt bed.
There are two shafts in each Morton mine – one for personnel and one to lower materials and
equipment into the mine, as well as to hoist the mined rock salt to the surface. The shafts also are
used to deliver a constant supply of fresh air to the miners while they work hundreds to
thousands of feet below the surface. Most mine shafts are lined with a concrete wall called a
shaft liner.
Salt is mined by the room and pillar method. It is removed in a checkerboard pattern to
leave permanent, solid salt pillars for mine roof support. Usually 45 to 65 percent of the salt is
removed. The room height may average 18 feet in a bedded deposit to 100 feet in a dome mine.
Normally, the first operation is undercutting. Large machines cut a slot 10 or more feet in depth
across the bottom of a solid salt wall. This leaves a smooth floor for picking up the salt after
blasting.
Next, small holes are drilled into the salt wall to a depth of 10 or more feet and
explosives are loaded into the drilled holes. After the work shift, the explosives are set off
electrically. Several hundred to several thousand tons of rock salt are blasted and fall onto the
mine floor.
Equipment is used to load and haul the salt to machines that crush and feed the salt onto a
conveyor belt. The lumps are conveyed to a series of stations for crushing and additional sizing
of the lumps. The salt is then placed in a storage bin to await hoisting to the surface.
The above ground processing of the rock salt consists of screening the mined salt into
various marketable sizes by sorting through mechanically operated screens. When separated,
each size is conveyed to its individual storage bin to await packaging for shipment or to be
loaded as bulk salt into railroad cars, trucks, river barges or lake boats for shipment to customers.
In “cut and blast mining” a slot is cut at the base of the rock face using a machine called
an undercutter, with a jib carrying a series of tungsten-carbide picks. This is the “cut” part of the
process.
The face is then drilled with a series of carefully sited holes, using an electro-hydraulic
rotary drill. The holes are charged with explosives and detonated, yielding about 1,200 tons of
then carried on a conveyor belt to the main crusher. This breaks the rock down into smaller
pieces, passing through a sieve to ensure that it has reached the correct size for use in road de-
• Continuous Mining
Continuous mining produces smaller lumps of rock than the cut and blast technique. A
boring machine, similar to a pneumatic drill used in digging up roads, is used. It has a rotating
head, carrying tungsten-carbide tips, which bores into the salt. The lumps are then taken directly
to a crushing and screening plant, without the need to be crushed by a feeder-breaker first.
Salt Production
Advantages Disadvantages
Raw Materials
1. Rock Salt • Less energy expended for • Costly to obtain from salt
purification. domes.
• Large deposits of rock salt from • Causes environmental
around the world. problems from drilling and
mining.
• Possible conflicts with the
communities within the
vicinity.
2. Brine • Large deposits of brine since it can • Contains many impurities.
be found in oceans. • Uses more energy in the
• Impurities are commercially valuable purification process.
as the salt itself.
Chapter III
Mass and Energy Balance
Evaporator Balance
Vo, To, Po, Ho, V1, T1, P1, Hv1, V2, T2, P2, Hv2,
ho hv1 hv2 V3, T3
D1 D2 D3
The plant will use parallel feed triple effect evaporators to concentrate the brine. Since
the location of the plant is in the Philippines, the feed is assumed to have a temperature of 30℃
since the temperature of the brine source will be affected by the temperature of the environment
(average Philippine temperature is between 26-29℃ according to
https://www1.pagasa.dost.gov.ph). It is desired for the evaporating system to produce a total of
151 tons per day of wet solids (salt) with concentration of 60% solids.
SYMBOL MEANING VALUE REFERENCE
F1 Mass flowrate 1,200 Calculations
of feed (brine) T/day
entering the 1st
effect
evaporator
F2 Mass flowrate 1028.5714 Calculations
of feed (brine) T/day
entering the 2nd
effect
evaporator
F3 Mass flowrate 874.2857 Calculations
of feed (brine) T/day
entering the 3rd
effect
evaporator
xF Concentration 0.035 https://sensorex.com/blog/2016/05/04/brine-
of feed concentration-measurement/
TF Temperature of 30℃ https://www1.pagasa.dost.gov.ph
brine feed
L1 Mass flowrate 70 T/day Desired value
of product (wet
solids) exiting
the 1st effect
evaporator
L2 Mass flowrate 60 T/day Desired Value
of product (wet
solids) exiting
the 2nd effect
evaporator
L3 Mass flowrate 51 T/day Desired value
of product (wet
solids) exiting
the 3rd effect
evaporator
xL Concentration 0.6 Based on the process from
of wet solids http://www.beneteccn.com/epc-services/vacuum
-salt-plant-manufacturer-supplier/
Vo Mass flowrate 1,359.3869 Calculations
of steam T/day
entering the 1st
effect
evaporator
V1 Mass flowrate 1,130 Calculations
of steam exiting T/day
the 1st effect
evaporator and
entering the 2nd
effect
V2 Mass flowrate 968.5714 Calculations
of steam exiting T/day
the 2nd effect
evaporator and
entering the 3rd
effect
V3 Mass flowrate 823.2857 Calculations
of steam exiting T/day
the 3rd effect
evaporator and
entering the
condensers
Po Steam pressure 20 psi https://www.saltassociation.co.uk/education/salt-
entering 1st history/salt-the-chemical-revolution/vacuum-
effect process/
evaporator
P1 Steam pressure 15 psi Assumed based on
entering 2nd https://www.saltassociation.co.uk/education/salt-
effect history/salt-the-chemical-revolution/vacuum-
evaporator process/
P2 Steam pressure 27.3455 psi Table 2-305 at 118.1881℃ temperature, Perry’s
entering 3rd Chemical Engineers’ Handbook, 8th ed
effect
evaporator
To Temperature of 126℃ https://www.saltassociation.co.uk/education/salt-
steam entering history/salt-the-chemical-revolution/vacuum-
the 1st effect process/
evaporator
T1 Temperature of 121℃ Table 2-305 at 15 psi pressure, Perry’s Chemical
steam entering Engineers’ Handbook, 8th ed
the 2nd effect
evaporator
T2 Temperature of 118.1881 Calculations
steam entering ℃
the 3rd effect
evaporator
T3 Temperature of 109.9337 Calculations
steam exiting ℃
the 3rd effect
evaporator
Ho(vapor) Enthalpies of 2727.5171 Table 2-305 at 20 psi pressure and 126℃,
steam entering kJ/kg Perry’s Chemical Engineers’ Handbook, 8th ed
ho(liquid) the 1st effect 528.5942
kJ/kg
Ws Ws
XF Xprod
TF Tprod
The brine or wet solids from each evaporator containing approximately sixty percent
(60%) solids at 30oC will be subjected to drying under constant drying conditions. The process
will result to a product (dry solids) with minimal to no moisture, leaving the drier at 40oC.
The medium that will be used for drying is air, taken from the atmosphere at ambient
conditions based on the Philippine recorded data. The air will be preheated to 60oC in a heater
and then fed to the drier. There will be an increase in humidity in the medium from 75% to 80%
due to the transfer of moisture from the wet solids (brine). It will then be released to the
environment with a temperature of 40oC. These parameters are constant with all the heater and
drier assigned to each evaporator.
For first effect
SYMBOL MEANING VALUE REFERENCE
Y1 0.0383
Humidity Calculations
Y2 0.0149
Y3 0.0149
RH (final) 80% Average relative humidity in the
RH Relative Humidity 75% Philippines
(initial) (bagong.pagasa.dost.gov.ph)
Ws Wet Solids 70 T/day Calculations
XF Concentration of 0.6 solids/H2O
Calculations
feed 0.6667 H2O/kgDS
Xprod Concentration of 1 solids/H2O
Calculations
product 0 H2O/kgDS
V’ Mass flow rate of T d.a.
1196.6410 Calculations
dry air day
T1 Temperature of air 40 C
o
Desired value
(leaving the drier)
T2 Temperature of air 60oC
Optimal drying temperature for salt
(entering the drier)
T3 Temperature of air 25oC
Based on ambient conditions in the
(entering the
Philippines
heater)
TF Temperature of 30oC
https://www1.pagasa.dost.gov.ph
feed
Tprod Temperature of 40oC
Desired value
product
CpDS Specific Heat of 0.88 kJ/kg DS Relationship between salinity and
dry solids specific heat ( nexusstem.co.uk)
CpH2O Specific Heat of 4.1868 kJ/kg Table 2-305, Perry’s ChE Handbook,
dry solids 8th edition
q1 Heat required by 498.2749 kW
Calculations
heater
q2 Heat required by 513.3198 kW
Calculations
dryer
QT1
Tm1
F1 TS1
TF1
TTSS
QT2
Tm2
F2 TS2
TF2
QT3
Tm3
F3 TS3
TF3
Three condensers will be used to cool down, condense, and further cool the condensed
liquid from the exiting steam of each evaporator prior to discharge. The cooling medium will be
water at 25oC and cool the steam from 109.9337℃ to 80℃ .
For condenser 1:
For condenser 2:
, BHP
P2
u2
D2
P1 T2
u1
D1
T1
Three pumps will be used to supply the feed (brine) to each evaporator. Initial and final
temperatures will remain constant, only having a change in pressure and fluid velocity.
Pumps 1,2, and 3 used the same inlet and outlet parameters
, BHP
P2
u2
D2
P1 T2
u1
D1
T1
Three pumps will be used for each of the three condensers. Initial and final temperatures
will remain constant, only having a change in pressure and fluid velocity. All three pumps will
have the same mass and energy balance due to having the same feed flow rate.
SYMBOL MEANING VALUE REFERENCE
P1 Inlet pressure 1 atm Atmospheric pressure
u1 Inlet velocity 0 Velocity at bottom of
a pond
D1 Inlet diameter of pump 8 in Desired value
P2 Outlet pressure 0.5 atm Desired value
u2 Outlet velocity m Calculations
0.0462
s
D2 Outlet diameter of pump 6 in Desired value
ṁ Mass flow rate of water tons Calculations
274.4286
day
ρ Density of water kg Density of water at
1000
m3 4°C
∆P Change in pressure -0.5 atm Calculations
∆ (u2 ) Change in velocity m2 Calculations
3.1948
s2
∆ Ep Change in potential energy 0 Calculations
Ẇ Work produced by the pump -1547.6369 W Calculations
Q Heat 0 Assuming adiabatic
operation
BHP Break horse power 105 HP Calculations
Compressor Balance
ρ1
T1
P1
ṁ ρ@20◦C
Ẇ
V1
ρ2
T2
P2
ṁ
V2
Equipment Design
Long tube vertical or rising film evaporators are used due to its low residence
time compared to other evaporator designs. This is crucial because it allows the usage of the
evaporator in higher operating temperatures and gives assurance of high quality products.
Additional advantage is the availability of the option to operate the evaporator as a continuous
process which is overall more energy and time efficient than batch processing operations.
Stainless steel is used in the construction of the evaporator due to its resistance to corrosion and
tupe of dryer and has a low maintenance cost compared to other dryers. It also has the greatest
capacity of any type of dryer. Brass can withstand high temperatures and is highly resistant to
straight tube heat exchangers as their surface condensers. This makes construction much simpler.
Brass is recommended for the construction of heat exchangers for the service below 200°C and
The following equipment base prices were taken as the average selling prices from online
sources based on the specifications provided in Chapter IV. The total purchased equipment cost
The base prices of the direct cost were based on the total purchased equipment cost and
multiplied to the factor introduced in Plant Design and Economics for Chemical Engineers 5th
The base prices of the indirect cost were based on the total direct cost and total fixed
capital investment multiplied to the factor introduced in Plant Design and Economics for
Chemical Engineers 5th Ed. to compute for a total direct cost of ₱15,195,151.52.
The fixed capital investment was taken as the sum of direct and indirect costs incurred
The total capital investment was taken as the sum of fixed capital investment and
working capital. The working capital was approximated using the total capital investment as a
basis multiplied to a factor introduced in Plant Design and Economics for Chemical Engineers 5th
The base prices used to compute for total product cost were based on total product cost
and fixed capital investment multiplied to a factor introduced in Plant Design and Economics for
Chemical Engineers 5th Ed. to compute for direct production costs of ₱46,539,900.00.
The base prices used to compute for total product cost were based on total capital
investment and fixed capital investment multiplied to a factor introduced in Plant Design and
Economics for Chemical Engineers 5th Ed. to compute for total fixed charge of ₱8,128,735.69.
charges and plant overhead cost. The plant overhead cost was approximated using the total
product cost as a basis multiplied to a factor introduced in Plant Design and Economics for
Chemical Engineers 5th Ed. to compute for a total capital investment of ₱61,720,135.69
The base prices used to compute for general expenses were based on total product cost
multiplied to a factor introduced in Plant Design and Economics for Chemical Engineers 5th Ed.
The total product cost was taken as the sum of manufacturing cost and general expenses
181 tons per day and from this, the total income per day can be calculated by multiplying it to the
average selling price of ₱14,500.00 per ton of salt. Total income per day is estimated to be
₱2,624,500.00 and an annual income of ₱682,370,000.00 with 260 working days per year. Gross
earnings are calculated from the difference of total income and total product cost to yield
Based on the cost estimation of the proposed salt production plant, the plant is predicted
to provide enough profit to compensate the expenses incurred during start-up and operation.
Therefore, on account of cost analysis, the design of the proposed salt production plant can be
considered feasible.
Chapter VI
Majority of workers employed in the salt industry are unskilled and poorly educated and
employed through contractor on temporary basis. A major share of accidents is due to bad work
practice and human error and hence can be avoided. Apart from accidents, workers in the salt
industry suffer from health problems arising out of work environment/ work conditions
Sources of Exposure
Studies have established that a large number of salt workers are exposed to salt and
symptoms, headache, giddiness, breathlessness, muscular and joint pains. The ophthalmic
problems were most common, probably due to irritation by direct sunlight and its glare caused by
salt crystals to brine as well as irritation, traumatic ulcers, dermatitis, muscular and joint pains.
Headache and giddiness were other more common symptoms to salt workers (Durairaj &
Murugan, 2019).
This salt processing plant will also expose workers to heat from substances and
Although ingestion is not thought to produce harmful effects, Sodium chloride may still
be damaging to the health of the individual following ingestion, especially where pre-existing
is not thought to be cause for concern. There are also evidences to suggest that this material can
cause eye irritation and damage in some people and the material can produce health damage if it
enters through wounds, lesions, and abrasions. Persons with impaired respiratory function,
airway diseases and conditions such as emphysema or chronic bronchitis, may incur further
disability if excessive concentrations of particulate are inhaled. It is not normally a hazard when
inhaled but there is some evidence to suggest that this material can irritate the throat and lungs of
some persons.
The following precautions should be taken when working with the chemical to ensure
1. Work area should have sufficient exhaust ventilation. Regularly vacuum dust to minimize
2. Avoid eye contact and wear eye protection if/when eye contact is likely to occur.
1) Eye Contact
Remove contact lenses, if necessary. Rinse immediately with plenty of water for at least five
2) Skin Contact
Remove contaminated clothing and wash affected area with plenty of soap and water. Seek
3) Inhalation
Remove the person from exposure and bring into fresh air. Seek medical attention if the exposed
4) Ingestion
Do not induce vomiting. If person is conscious, rinse mouth with plenty of water and give
several glasses of water to drink. Seek medical attention if adverse symptoms occur.
In the event of a sodium chloride spill, the area should be vacuum or wet-swept. Dry
sweeping or other methods that will raise dust should be avoided and the area should be cleaned
In the industrial setting, there are many hazards – more importantly fires, explosions and
toxic releases. Fires occur most frequently in industries and are the first major hazard in chemical
or process industries. Industrial fires are highly hazardous and dangerous, and accidents lead to
the loss of lives and major damage to infrastructure. (Industrial Fire and Explosion Hazards,
2018)
Here are some of the major fires and explosions that can occur inside the plant:
1) Jet fires
Jet fires, or ejected flames, occur when there is an ejection of flammable liquid from a
vessel, pipe or pipe flange. Jet flames scenarios are highly dangerous and jet fires can go up to 50
meters or more. Jet fires dissipate thermal radiation away from the flame’s visible boundaries
and the energy transmitted could be hazardous to both life and property.
2) Pool fires
A pool fire, defined as “a pool of flammable liquid burning with a stationary diffusion
flame or the combustion of material evaporating from a layer of liquid at the base of fire”, occurs
when a flammable liquid spills and is ignited on the ground. A pool fire is dangerous because
wind can extend the base of the flame and cause flame drag.
Some incidents describe a pool fire taking place in a storage tank or bund. In both cases,
the boundary of the pool is clearly defined and the shape of the pool may be circular or
rectangular. Other types of pool fire occur after a liquid is discharged on the ground, the shape
3) Flash fires
Flash fires, or vapor cloud fires, are defined as “the combustion of a flammable vapor and
air mixture in which flame passes through the mixture, at less than sonic velocity (speed of
sound in the medium), such that negligible over pressure is generated”. A flash fire occurs when
a vapor cloud forms from a leak and is ignited. Release of flammable vapor from a process plant
followed by ignition is common. In a flash fire, the gas burns and may cause a sudden depletion
of oxygen.
The explosion resulting from the ignition of a cloud of flammable vapor, gas, or mist in
which flame speeds accelerate to sufficiently high velocities to produce significant overpressure.
BLEVE is a vapor explosion which may result from a catastrophic failure of a tank
structure, which was containing cargo liquid above the boiling point at nominal atmospheric
pressure.
The cargo in the tanks of gas carrier is partially liquid and partially vapors in normal
condition. However, when the tank structure collapses, the vapor tries to escape or leak through
the opening, resulting in a decrease in the pressure inside the tank. These drastic lowering of
pressure inside the cargo tank results in rapid boiling of liquid and increase in vapour formation.
Personnel Safety
In order for the plant to produce the desired product successfully, personnel/workers must
also work effectively and safely securing the equipment and the process as a whole. There are
some threats to the safety of the personnel working in the plant. One of the most common is the
eye problem in the salt industry which is caused by intense reflectance of the sun light from
water surface and salt. Contact with salt laden water causes different type of skin lesions
amongst the workers. According to medical practitioners and skin specialists, other skin ailments
c) Photo-dermatitis
d) Toxin metanosis
Other hazards that endanger worker’s health and well-being in the salt industry are:
b) Electricity
d) Air pollution
g) Heat
l) Shift work
In work situation where exposure to hazard cannot be avoid the worker needs to use
personal protection equipment for his safety. Equipment required to be used in the salt industry
include safety helmets, eye goggles, hand gloves, safety shoes disposal filter mask, breathing
Awareness amongst the workers of the salt industry should be increased regarding
different hazards of the work place and action required to be taken for safe working. Hazard
awareness education has to be given at the time of inducting the worker for job. Workers should
also be educated regarding the necessity of using personal protection equipment, its proper
Safety Regulations
The salt units have to comply with a number of statutes. Factories Act as amended by
Factories (Amendment) Act 1987 lays down aspects relating to licensing and registration of
factories, inspecting authorities under the Act, health, safety, welfare, working hours of the
workers, employment of adults and young children, annual leave and penalties. Workmen
compensation Act, 1923 provides for payment of compensation to the worker or his dependents
in the event of an accident taking place. Other laws covering the welfare of the workers include
ESIC Act, Employees Provident Fund and miscellaneous provisions Act, Maternity Benefit Act,
Payment of Gratuity Act, Contract labour (Regulation and abolition) Act, Industrial Dispute Act,
Payment of Bonus Act. The purpose of all such acts is to ensure safe work place for the
workmen, social justice and social security to the worker and his family.
Management of the salt units should organize awareness and orientation programs for all
new workers. It must ensure periodic testing of existing protective equipment and get the same
serviced for smooth functioning with the help of protective equipment manufacturers.
To avoid the problem of manual lifting of heavy loads, mechanical means of material
movement must be introduced wherever possible. In situation where it is not feasible to have
mechanization, action must be taken to explore the possibility of redesigning the workplace so as
to minimize worker fatigue and posture problem. For workers who are required to undertake
Management options like permit system tag out/ lockout system, planned maintenance
should be adopted to minimize human errors and unsafe work practices. Fixed guard or
interlocking guards or Trip Devices must be installed with various machines that are used in the
salt units to minimize incidents of accidents due to contact with moving machine parts.
Medical health surveillance must also be adopted. The medical check must be carried out
at the time of induction of worker and at regular intervals. The records of such medical checks
should be properly kept. Machine layout should be planned considering safety aspects, providing
access for maintenance, waste removal etc. Further, housekeeping should be good- allowing
sufficient space for material & worker movement without any obstruction.
Loss Prevention
HAZOP Study
Environmental Protection
Environmental Regulations
OF 2000
The law aims to adopt a systematic, comprehensive and ecological solid waste
management program that shall ensure the protection of public health and environment. The law
ensures proper segregation, collection, storage, treatment and disposal of solid waste through the
The law aims to protect the country's water bodies from pollution from land-based
activities). It provides for comprehensive and integrated strategy to prevent and minimize
pollution through a multi-sectoral and participatory approach involving all the stakeholders.
c) REPUBLIC ACT 8749 PHILIPPINE CLEAN AIR ACT OF 1999
The law aims to achieve and maintain clean air that meets the National Air Quality
guideline values for criteria pollutants, throughout the Philippines, while minimizing the possible
The law aims to regulate restrict or prohibit the importation, manufacture, processing,
sale, distribution, use and disposal of chemical substances and mixtures the present unreasonable
risk to human health. It likewise prohibits the entry, even in transit, of hazardous and nuclear
wastes and their disposal into the Philippine territorial limits for whatever purpose; and to
The Environment Impact Assessment System was formally established in 1978 with the
enactment of Presidential Decree no. 1586 to facilitate the attainment and maintenance of
protection. EIA is a planning and management tool that will help government, decision makers,
the proponents and the affected community address the negative consequences or risks on the
covers water pollution control, noise pollution control, soil pollution control, and thermal
pollution control. This system helps in reducing or preventing polluting particle of hazardous
Air pollution produce inside the plant will be eliminated using a technology that will
purify the air and also taking proper measures that will reduce it and its effects in the
environment. Air pollution abatement controls the quality of the air at surface level everywhere,
especially in the industrial sites. The main feature consists of monitoring and abating pollutants
like particulate matter (PM) emissions and the control of gaseous emissions. Processes that are
typically employed to reduce these particulate emissions are using settling chambers, cyclone
The air stream is directed through a settling chamber, which is relatively long and has a
large cross-section, causing the velocity of the air stream to be greatly decreased and allowing
sufficient time for the settling of solid particles. For wet scrubbers, they control particulate
emissions by wetting the particles in order to enhance their removal from air stream. In filtration,
the most commonly used device is a baghouse which consists of fabric bags through which the
air stream is directed. Particles become trapped in the fiber mesh on the fabric bags, as well as
concentration of salts such as sodium chloride. These streams of waste can be some of the most
challenging to treat or discharge because their composition and purification requirements can be
rather dynamic and complex. Brine waste was produced as a by-product such as the cooling
tower and boiler effluent. This waste can be either recycled for use in the facility’s process or
treated for disposal. It is known to reduce thermal conductivity so they are reused as a cooling
agent for steel heat exchangers. In treating brine waste for reuse, it can be pre-treated with
coagulants, polymers, additives, and pH adjustment to settle out many of the larger
contaminants. It can then be treated with specialty chelating resins that target specific metals for
removal without being exhausted by sodium. The technologies and methods of purification
and/or separation vary greatly depending on the quality of the brine waste and the brine
composition. (What is Brine Waste, and how it can be treated for Reuse or Disposal, 2018)
Solid waste produced by the process if non-toxic, could be used as an additive for soil
remediation. However, because of its salt content, it has no use and can be disposed to a licensed
Adequate and reliable technologies exist for the control of thermal pollution. Two of
water and a closed sink to which to return it after use. It must be sufficiently large that
evaporation and other heat transfer to the air from its surface can keep the average water
temperature low enough to provide a continuous source of cooling tower. The pond outlet is
usually located as far as possible from the hot water return to maximize the time allowed for
cooling.
A cooling tower allows for the efficient contact of ambient air with heated water,
resulting in the rapid cooling of the water without returning it to its source, or before it is
returned to its source. When a cooling tower is used, it is possible to use the same water for plant
cooling again and again, by adding small fractions of fresh water to make up for evaporation
losses.
Noise Control
treating it. A barrier could be placed between them and the receiver (which is much likely the
worker inside the plant), such that the sound waves cannot propagate to the receiver. Or, the
receiver can be treated by using ear plugs or headsets. Workers subjected to noise will have an
annual audiogram. If there is a shift in their hearing threshold relative to their baseline audiogram
of an average of 10 dB or more in the 2000, 3000, and 4000 Hz frequency levels, in either ear,
the worker must be retested within 30 days. OSHA has established permissible noise exposure
limits to help avoid the standard threshold shifts in working. (Industrial Noise Control-
Occupational Health and Safety, 2007) Substitution of the noisy equipment for quieter ones is
also a good alternative to protect the workers from exposure to noise. Other options can also be:
a) enclosing the noisy equipment with a sound-absorbing material b) avoiding metal to metal
The salt processing plant will be built in Occidental Mindoro in the Philippines.
Occidental Mindoro, along with the province of Cavite, were the biggest suppliers of salt in the
country in 1990 (Verdey & Abilay, 2017). Mindoro is surrounded by the sea which makes it
ideal for the salt processing plant since the raw material will be taken from the sea. Also, DOST
is presently planning to enhance the salt industry in Occidental Mindoro (Verdey & Abilay,
2017). It has many ports connecting to the various regions of the Philippines so there is greater
access and more opportunities for potential buyers since the location is easily accessible.
Occidental Mindoro is not highly urbanized, with only 83 inhabitants per square kilometer
according to the 2015 census so cost of labor is also low and since the place is not densely
populated, there will be less negative impact (less complaints from the community from noise,
odor, etc) compared to densely populated areas. Also, since the area is not as highly urbanized,
equipment and spaces for piping, instruments, and other possible additions, the area of the
process house having two floors was estimated to be 2000 square meters. Adding the warehouse,
other buildings and facilities, the wastewater pond, and other possible additions, the whole plant
was estimated to cover 4 hectares of area near the sea. Roads will be built between buildings
inside the plant for the people and for shipping vehicles to the main road. The main source of
waste in this plant is water from the different processes. The condensed steam will be recycled
back to the boiler. No chemicals are used in the process so the wastewater from other sources
The salt processing plant will be operated 260 whole days per year and 60 days per year
will be used for maintenance. Temperature and pressure sensors and level control devices will be
installed in the equipment to monitor and control the values. The product will be stored in the
warehouse before shipping and no storage for raw materials is required since the brine will be
collected immediately from the sea. Water for the boiler, the offices and other facilities will be
taken from underground and electricity for the plant will be provided by the boiler. Pipes will be
used to transport the materials during the process and conveyor belts will be used to transport the
REFERENCES
Azfryna. (2018, August 21). Industrial Fire and Explosion Hazards. Retrieved October 6, 2019
from https://www.opuskinetic.com/2018/08/industrial-fire-and-explosion-hazards/.
Brooks, P.J. (n.d.). Industrial Noise Control. Retrieved October 9, 2019 from
https://ohsonline.com/articles/2007/09/industrial-noise-control.aspx?m=1.
Chemical Engineering. (n.d.). Common Mistakes When Conducting a HAZOP and How to Avoid
https://www.chemengonline.com/common-mistakes-conducting-hazop-avoid/?
pagenum=2.
Chemistry LibreTexts (2019). Introduction to Salt. Retrieved July 12, 2019 from
https://chem.libretexts.org.
Durairaj, D. & Murugan, S. (2016). A Study on Health Hazard of Salt Workers in Tamilnadu
http://globalresearchonline.net/journalcontents/v40-2/29.pdf.
Eusalt (n. d.) Salt Production. Retrieved July 12, 2019 from https://eusalt.com/salt-
production.
https://www.businesswire.com/news/home/20160616005963/en/Global-Brine-Fluids-
Market-Report-2016-2021--
https://www.technavio.com/report/global-salt-market-analysis-share-2018
Hill, C. (1972). Thermal Pollution and its Control. Retrieved October 10, 2019 from
https://www.lawdigitalcommons.bc.edu/
Industrial Safety and Hazard Management in Salt Industry. (2019). Retrieved October 5, 2019
from https://tifac.org.in/index.php/8-publication/181-industrial-safety-and-hazard-
management-in-salt-industry.
Industrial Salts Market Size & Share | Global Industry Report, 2014-2025. (n.d.). Retrieved
from https://www.grandviewresearch.com/industry-analysis/industrial-salts-market
https://www.ibisworld.com/industry-trends/specialized-market-research-reports/
consumer-goods-services/food-production/table-salt-production.html
Major Environmental Laws. (n.d.). Retrieved October 7, 2019 from http://ecac.emb.gov.ph/?
page_id=43.
Marshall, K. (2018, November 28). What Is Brine Waste, and How Can It Be Treated for Reuse
brine-waste-how-treated-reuse-disposal/.
http://www.micromarketmonitor.com/market-report/brine-fluids-reports-
5317899398.html
Moncel, B. (2019, June 26). How Salt Gets to Your Dinner Table. Retrieved from
https://www.thespruceeats.com/how-is-salt-made-1328618
Monselt, B. (2019). How Salt Is Made. Retrieved July 12, 2019 from
https://www.thespruceeats.com/how-is-salt-made-1328618.
https://www.iosh.com/resources-and-research/our-resources/occupational-health-toolkit/noise/
control-measures/.
https://www.ilo.org/public/wcms_193193.pdf
https://www.envirotechasia.com/pollution-control-system/.
Producer Price Index by Commodity for Chemicals and Allied Products: Rock Salt. (2019,
https://www.aquasure.com.au/recycling-waste
Research and Markets. (2017, September 22). Industrial Salt (Rock Salt, Natural Brine)
salt--rock-salt-natural-brine-market-2017-2022---focus-on-conventional-mining-
vacuum-evaporation-solar-evaporation-300524330.html
Rock Salt Market Global Demand Analysis Opportunity Outlook 2024. (n.d.). Retrieved from
https://www.researchnester.com/reports/rock-salt-market-global-demand-analysis-
opportunity-outlook-2024/307
Rock Salt Production: How Do You Make Road Grit: Salt Association. (n.d.). Retrieved from
https://www.saltassociation.co.uk/education/make-salt/rock-salt-production/
production-and-processing/
Sheth, K. (2017). All About the Salt Industry. Retrieved July 12, 2019 from
https://www.worldatlas.com/articles/all-about-the-salt-industry.html.
https://www.saltassociation.co.uk/education/salt-history/salt-the-chemical-
revolution/vacuum-evaporator-design-and-operation/
Vapor Cloud Explosion (VCE). (2014, December 18). Retrieved October 6, 2019 from
https://www.aiche.org/ccps/resources/glossary/process-safety-glossary/vapor-cloud-
explosion-vce.
Verdey, A. C., & Abilay, M. J. (2017). DOST Eyes Salt Industry Enhancement in Occidental
http://region4b.dost.gov.ph.
Weird Science: Salt is Essential to Life. (n. d.). Retrieved July 12, 2019 from
https://manoa.hawaii.edu.
World Salt, Market Share, Market Size, Sales, Demand Forecast, Market Leaders, Company
https://www.freedoniagroup.com/World-Salt.html