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Combined Spectra Problems

The document contains NMR and IR spectral data for 10 different organic compounds. It provides the molecular formula, IR and NMR spectral data including 1H and 13C NMR spectra for each compound. The compounds include alcohols, ketones, aldehydes, esters, amines and halogenated hydrocarbons.

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Usama khan
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310 views11 pages

Combined Spectra Problems

The document contains NMR and IR spectral data for 10 different organic compounds. It provides the molecular formula, IR and NMR spectral data including 1H and 13C NMR spectra for each compound. The compounds include alcohols, ketones, aldehydes, esters, amines and halogenated hydrocarbons.

Uploaded by

Usama khan
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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molecular formula: C11H14O2

IR:

1
H NMR :

13
C NMR:
δ (ppm) = 147.0
145.5
130.8
130.0
122.6
117.2
113.1
112.0
64.0
18.2
14.9
molecular formula: C6H10O2

IR:

1
H NMR :
δ (ppm) = 6.97 (dq, J = 6.8 and 15.2 Hz, 1H),
5.83 (d, J = 15.2 Hz, 1H),
4.17 (q, J = 7.2 Hz, 2H),
1.87 (d, J = 6.8 Hz, 3H),
1.27 (t, J = 7.2 Hz, 3H).

13
C NMR
δ (ppm) = 170.0
144.6
123.0
60.3
18.1
14.5
molecular formula: C10H12O

13
C NMR: δ 207, 141, 128, 126, 124, 45, 29, 27
Formula: C11H14O

IR:

1H NMR:
6.75 4.30
(2H, d, J= 7.2) (2H, d, J=7.4)
1.25
7.17 6.45 (t, 3H, J=7.9)
(2H, d, J= 7.2) (1H, d, J=12.5)

4.30
6.25 (2H, d, J=7.4)
(1H, dt, J=12.5, 7.4)

2.60
(2H, q, J=7.9)

2.42
(1H, s)

13
C NMR: δ 140, 132, 128, 125, 122, 119, 65, 32, 14
Formula: C8H9OCl
IR: broad absorption from 3600-3400 cm-1
13C NMR: δ 138, 131, 129, 127, 65, 39
1H NMR: δ 7.50 d, J= 9.0, 2H
7.10 d, J= 9.0, 2H
3.70 t, J= 5.0, 2H
3.00 s, 1H
2.70 t, J= 5.0, 2H
Formula: C10H12O2
IR: 1690 cm-1
13C NMR: δ 200, 158, 130, 128, 114, 65, 32, 10
1H NMR: δ 7.80 d, J= 9.0, 2H
7.10 d, J= 9.0, 2H
3.90 s, 3H
2.50 q, J= 6.0, 2H
1.20 t, J= 6.0, 3H
Formula: C12H16O2

1H δ 1.62
NMR
(2H, tq, δ 0.90
δ 2.25 J = 7.2, 7.4) (3H, t,
(2H, t, J = 7.4)
δ 2.90 J = 7.2)
(2H, t,
δ 7.25 δ 4.30 J = 7.0)
(5H, m) (2H, t,
J = 7.0)

13
C NMR: δ 173.4, 137.9, 129.0, 128.4, 126.5, 64.6, 36.2, 35.2, 18.4, 13.6
Formula: C10H15NO

3.8 2.4 1.35


(3H, s) (3H, s) (3H, d, J= 6.6)

7.1
(2H, d, J= 7.3)
6.8 4.05 1.45
(2H, d, J= 7.3) (1H, q, J= 6.6) (1H, s)

13
C NMR: δ 159.0, 131.0, 129.0, 114.0, 60.5, 56.0, 33.3, 21.8
Formula: C13H15NO2

IR:

1
H NMR:

13
C NMR:
δ (ppm) = 177.0
143.5
131.8
129.0
119.0
115.8
64.7
35.2
40.0
64.0
18.9
Formula: C12H16O2

13
C NMR: δ 173.0, 137.2, 132.0, 129.7, 129.1, 61.7, 40.5, 25.5, 17.0, 14.1
Formula: C10H15N

IR:

1
H NMR:

13
C NMR: δ 142.1, 128.5, 127.3, 125.7, 54.2, 40.8, 35.4, 33.2

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