900 Series

Ultra Low Temperature

Upright Freezers

Operating and Maintenance Manual

Manual No: 7000902 Rev. 1

 Model 900 Series _______________________________________________________________________________

Models Capacity in Voltage

Read This Instruction Manual. Cubic Feet
902 13 230
Failure to read, understand and follow the instructions in 903 13 120
this manual may result in damage to the unit, injury to operat-
904 17 120
ing personnel, and poor equipment performance.
905 17 230
906 23 230
CAUTION! All internal adjustments and maintenance must 907 28 230
be performed by qualified service personnel. Double Door Units
991 13 230
992 13 120
Refer to the serial tag on the back of this manual.
993 17 120
994 17 230
995 23 230

The material in this manual is for information purposes only.

The contents and the product it describes are subject to change
without notice. Thermo Forma makes no representations or war-
ranties with respect to this manual. In no event shall Thermo
Forma be held liable for any damages, direct or incidental, aris-
ing out of or related to the use of this manual.

MANUAL NUMBER 7000902

1 21404 3/26/03 Additional electrical schematic revisions aks
21404 3/17/03 Revised electrical schematics and relay enclosure drawings aks
21039 3/11/03 Line cord bracket installation aks
0 -- 1/14/03 Original Manual aks
REV ECR/ECN DATE DESCRIPTION By

i
Model 900 Series _________________________________________________________________________Warnings

Important operating and/or maintenance instructions. Read the accompanying text carefully.

Potential electrical hazards. Only qualified persons should perform procedures associated with this symbol.

Hot surface(s) present which may cause burns to unprotected skin or to materials which may be damaged by elevated
temperatures

Extreme temperature hazards, hot or cold. Use special handling equipment or wear special, protective clothing.

√ Always use the proper protective equipment (clothing, gloves, goggles, etc.)
√ Always dissipate extreme cold or heat and wear protective clothing.
√ Always follow good hygiene practices.
√ Each individual is responsible for his or her own safety.

ii
Model 900 Series ___________________________________________________________________________Service

iii
 Model 900 Series __________________________________________________________________Table of Contents

Table of Contents

Section 1 - Installation and Start-up . . . . . . . . . . . . . . .1 - 1 Section 5 - Factory Options . . . . . . . . . . . . . . . . . . . . . .5 - 1

1.1 Freezer Components . . . . . . . . . . . . . . . . . . . . . . . . .1 - 1 5.1 BUS (Back Up System) . . . . . . . . . . . . . . . . . . . . . . .5 - 1
1.2 Control Panel Keys, Displays and Indicators . . . . . .1 - 2 a. Installing the vent stack, solenoid and injection
1.3 Operation of the Keypad . . . . . . . . . . . . . . . . . . . . . .1 - 3 assembly . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 - 1
1.4 Installing the Freezer . . . . . . . . . . . . . . . . . . . . . . . . .1 - 3 b. Installing the Temperature Probe . . . . . . . . . . . . . .5 - 2
a. Choosing the Location . . . . . . . . . . . . . . . . . . . . .1 - 3 c. Connecting the probe/solenoid harness . . . . . . . . .5 - 2
b. Installing the Wall Bumpers . . . . . . . . . . . . . . . . .1 - 3 d. BUS Control Panel . . . . . . . . . . . . . . . . . . . . . . . .5 - 3
c. Installing the Shelves . . . . . . . . . . . . . . . . . . . . . .1 - 3 e. Configuring the Optional BUS . . . . . . . . . . . . . . .5 - 3
d. Remote Alarm Contacts . . . . . . . . . . . . . . . . . . . . .1 - 3 f. Setting the Optional BUS Set Point . . . . . . . . . . . .5 - 3
e. Attaching the Power Cord . . . . . . . . . . . . . . . . . . .1 - 4 g. System Operation Check . . . . . . . . . . . . . . . . . . . .5 - 3
f. Connecting the Unit to Electrical Power . . . . . . . .1 - 4 h. Cleaning the Vent Stack . . . . . . . . . . . . . . . . . . . . .5 - 3
1.5 Freezer Start-Up . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 - 4 i. Disconnecting the fitting assembly and
a. Setting the Operating Temperature . . . . . . . . . . . .1 - 4 transfer hose . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 - 3
b. Setting the High Temperature Alarm . . . . . . . . . . .1 - 4 5.2 Chart Recorder . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 - 4
c. Setting the Low Temperature Alarm . . . . . . . . . . .1 - 5 a. Installing the chart paper . . . . . . . . . . . . . . . . . . .5 - 4
1.6 Run Mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 - 5 b. Recorder Calibration . . . . . . . . . . . . . . . . . . . . . . .5 - 4
5.3 Datalogger . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 - 5
Section 2 - Calibrate . . . . . . . . . . . . . . . . . . . . . . . . . . . .2 - 1 5.4 Water-Cooled condenser . . . . . . . . . . . . . . . . . . . . . . .5 - 5
2.1 Calibrate Mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2 - 1 5.5 Five Inner Door Option . . . . . . . . . . . . . . . . . . . . . . .5 - 5
a. Calibrating the Control Probe . . . . . . . . . . . . . . . .2 - 1
Section 6 - Specifications . . . . . . . . . . . . . . . . . . . . . . . .6 - 1
Section 3 - Alarms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 - 1
3.1 Alarms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 - 1 Section 7 - Spare Parts . . . . . . . . . . . . . . . . . . . . . . . . . .7 - 1
3.2 Probe Failure Alarm . . . . . . . . . . . . . . . . . . . . . . . . . .3 - 1
Section 8 - Refrigeration Schematics . . . . . . . . . . . . . .8 - 1
Section 4 - Maintenance . . . . . . . . . . . . . . . . . . . . . . . . .4 - 1
4.1 Cleaning the Cabinet Exterior . . . . . . . . . . . . . . . . . .4 - 1 Section 9 - Electrical Schematics . . . . . . . . . . . . . . . . .9 - 1
4.2 Cleaning the Air Filter . . . . . . . . . . . . . . . . . . . . . . . .4 - 1
4.3 Cleaning the Condenser . . . . . . . . . . . . . . . . . . . . . . .4 - 1 Section 10 - Warranty . . . . . . . . . . . . . . . . . . . . . . . . .10 - 1
a. Cleaning the Water-cooled Condenser . . . . . . . . . .4 - 1
4.4 Defrosting the Chamber . . . . . . . . . . . . . . . . . . . . . . .4 - 1 Appendix A - Handling Liquid Nitrogen . . . . . . . . . . . .A - 1
4.5 Cleaning the Door Gasket . . . . . . . . . . . . . . . . . . . . .4 - 2
4.6 Cleaning the Vacuum Relief Port . . . . . . . . . . . . . . . .4 - 2 Appendix B - Handling Liquid CO2 . . . . . . . . . . . . . . .B - 1
4.7 Replacing the Battery(s) . . . . . . . . . . . . . . . . . . . . . .4 - 2
4.8 Preparing the Unit for Storage . . . . . . . . . . . . . . . . . .4 - 2 First Aid . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .C - 1
Preventive Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . .4 - 3

iv
Model 900 Series ___________________________________________________________________Installation and Start-Up

Section 1 - Installation and Start-up

Figure 1-4
Figure 1-1 Vacuum Relief and Probe Cover Location
Model 900 Series Front
1.1 Freezer Components

Figure 1-1
• Control Panel - keypad, displays and indicators.
• BUS (Optional Back Up System) panel.
• Optional temperature recorder - 7 day, one pen or
Datalogger.
Figure 1-2
• Remote alarm contacts.
• Power Inlet for power cord connection.
• Optional BUS connections for probe and solenoid.
• Power Switch (mains disconnect).
Figure 1-2
Model 900 Series Rear Figures 1-3 and 1-4
• Vacuum relief port - pressure equalization port.
• Probe cover - houses control, optional recorder or
Datalogger and 1535 alarm (optional) probes.

Figure 1-3
Vacuum Relief Port and Probe Cover

1-1
 Model 900 Series ____________________________________________________________Installation and Start-Up

Figure 1-5

• Battery mounting bracket wing nuts

(three).
• Battery power switch (freezer and BUS).
• Freezer battery.
• Optional BUS battery.
• Freezer filter location.

Figure 1-5
Battery(s) location and Switch

Figure 1-6, Control Panel

1.2 Control Panel Keys, Displays and Indicators

(See Figure 1-6)

4. Silence - Silences the audible alarm.

1. Temperature Display - Displays temperature in degrees 5. Alarm Panel - indicates the current alarm condition.
Celsius. 6. Up and Down Arrows - Increases or decreases values,
2. Mode Select Switch - Used to select Run, Set toggles between choices.
Temperature, Set High Alarm, Set Low Alarm, Calibrate, 7. Enter - Stores the value into memory.
Backup.
3. Alarm Indicator - Light pulses on/off during an alarm
condition of the cabinet.

1-2
 Model 900 Series ___________________________________________________________________Installation and Start-Up

1.3 Operation of the Keypad

Figure 1-7
The 900 Series freezer has five basic modes
which allow freezer setup and operation. Press the
Mode key to scroll through the mode selections. a. Choosing the Location

Locate the freezer on a firm, level surface in an area with

Up Arrow: Increases or toggles the parameter an ambient temperature between 18°C and 32°C. Provide ample
value. room to reach the mains disconnect switch (power switch)
located on the rear of the freezer.
Enter: Must press Enter key to save to memo-
ry all changed values.
b. Installing the Wall Bumpers
Down Arrow: Decreases or toggles the param-
eter value. The parts bag, located inside the cabinet, contains the fol-
lowing parts.
Silence Key: Press to silence the audible
alarm. See Section 4 for alarm ringback times. Quantity Stock # Description Purpose
2 510016 1/4-20 x 5-1/2” Bolt Wall Bumper
1.4 Installing the Freezer 2 380520 Neoprene Cap Cap Protector

Install the bolts into the pre-tapped holes on the back of the
If tipped more than 45°, allow the unit to set compressor section. Install a neoprene cap on each bolt. Refer
upright for 24 hours before start up. to Figure 1-2 for the locations of the pre-tapped holes.

To remove the freezer from the pallet, use the 7/16" c. Installing the Shelves
wrench to remove all the bolts securing the shipping bracket to
the pallet. Install the shelf clips into the shelf pilasters (front and
Remove the shipping bracket. Remove the ramp back) at the desired shelf level. Install the shelves in the cabinet
boards from the pallet and place the slotted end over the ramp onto the clips.
brackets on the pallet. The support blocks on the ramps will be
facing down. Before moving the freezer, make sure the casters NOTE: On units having the optional 5 inner door option, refer
are unlocked and moving freely. Align the caster with the ramp to the instructions accompanying the inner door kit.
boards. Use adequate personnel to roll the freezer off the pallet.
The freezer can be easily pushed to the desired
approved location, described in Section 1.4.a. If necessary, the
doors and lower front panel may be opened to move the unit
through tight openings. When the freezer is in position, set the
front caster brakes.

The freezer must not be moved with the product

load inside.

For proper ventilation and airflow, a minimum

clearance of 5” at the rear and top and a clear-
ance of 8” on the side of the freezer is required.
Allow adequate space in the front of the freezer
for door opening.

1-3
 Model 900 Series ___________________________________________________________________Installation and Start-Up

d. Remote Alarm Contacts First, turn on the freezer power switch. Then open the
lower front door by grasping the bottom left corner. Locate the
The remote alarm provides a NO (normally open) output, battery switch and turn it on. See Figure 1-5. During initial
a NC (normally closed) output and COM (common). The con- freezer start-up, the system battery may require charging and
tacts will trip on a power outage, high temperature alarm or low the Low Battery indicator may illuminate.
temperature alarm.
The pin configuration for the remote contacts is shown Assure the battery switch is turned on. The
below (in alarm state). rechargeable batteries require 36 hours to charge
at initial start-up. A “Low Battery” alarm may
occur until the batteries are fully charged. Should
a power failure occur during the initial start-up
period, the electronics will have limited operation.

1.5 Freezer Start-Up

With the freezer properly installed and connected to power,

system set points can be entered. The following set points can
be entered in Settings mode: Control temperature, high temper-
Figure 1-8 ature alarm set point, low temperature alarm set point, and
(optional) BUS set point. Default settings are shown in the table
below.
Control Set Point -80°C
High Temperature Alarm -70°C
Low temperature alarm -90°C
Optional BUS Set Point -60°C

a. Setting the Operating Temperature

e. Attaching the Power Cord
If the set point is changed and the low temperature and high
Insert the power cord into the power inlet module. Place temperature alarms are set 10° from the set point, the alarm
the retaining bracket (p/n 195763) over the connector. Tighten set points will be adjusted automatically to maintain a dis-
retaining screws to secure. tance of at least 10° from set point.

All 900 Series freezers have an operating temperature

range of -50°C to -86°C, depending on ambient temperature.
The freezer is shipped from the factory with a temperature set
point of -80°C. To change the operating temperature set point:
1. Press the Mode key until the Set Temperature indicator
Figure 1-9 lights.
2. Press the up/down arrow key until the desired tempera-
ture set point is displayed.
f. Connecting the Unit to Electrical Power
3. Press Enter to save the set point.
4. Press the Mode key until the Run indicator lights for
See the serial tag on the side of the unit for electrical specifi- Run mode
cations or refer to the electrical schematics in this manual. If no keys are pressed, the freezer will automatically
return to RUN mode after 5 minutes.
The freezer should be operated on a dedicated grounded
service. Check the voltage rating on the serial tag of the unit
and compare it with the outlet voltage. Then, with the power
switch turned off, plug the line cord into the wall outlet.
1-4
 Model 900 Series ____________________________________________________________Installation and Start-Up

b. Setting the High Temperature Alarm 1.6 Run Mode

The high temperature alarm will activate an audible/visual The Run mode is the default mode for the freezer. The run
warning when the freezer chamber temperature has reached or mode will display the cabinet temperature on the temperature
exceeded the high temperature alarm set point. display under normal operating conditions. In addition, the
To set the high temperature alarm set point: Run mode allows display of the high stage heat exchange tem-
perature.
1. Press the Mode key until the Set High Alarm indicator
lights. This information is scrolled by pressing the up or down
arrow keys. The display will return to the operating temperature
2. Press the up or down arrow key until the desired high in 10 seconds if no keys are pressed.
temperature alarm set point is displayed.
3. Press Enter to save the setting.
4. Press the Mode key until the Run indicator lights for
Run mode
If no control keys are pressed, the freezer will automatical-
ly return to RUN mode after 5 minutes.

Note: The high alarm set point must be set at least 10°C from
the control set point.

c. Setting the Low Temperature Alarm

The low temperature alarm will activate an audible/visual

warning when the freezer chamber temperature has reached or
decrease below the low temperature alarm set point.
To set the low temperature alarm set point:
1. Press the Mode key until the Set Low Alarm indicator
lights.
2. Press the up or down arrow key until the desired low
temperature alarm set point is displayed.
3. Press Enter to save the setting.
4. Press the Mode key until the Run indicator lights for
Run mode
If no control keys are pressed, the freezer will automatical-
ly return to RUN mode after 5 minutes.

Note: The low alarm set point must be set at least 10°C from
the control set point..

1-5
 Model 900 Series _________________________________________________________________________Calibration

Section 2 - Calibrate

2.1 Calibrate Mode

Once the freezer has stabilized, the control probe may need
to be calibrated. Calibration frequency is dependent on use,
ambient conditions and accuracy required. A good laboratory
practice would require at least an annual calibration check. On
new installations, all parameters should be checked after the
stabilization period.

Before making any calibration or adjustments to

the unit, it is imperative that all reference instru-
ments be properly calibrated.

a. Calibrating the Control Probe

Plug a type T thermocouple reader into the receptacle

located inside the lower door (see Figure 1-5). Compare the
control temperature set point to the temperature of the measur-
ing device.
1. Press the Mode key until the Calibrate indicator lights.
2. Press up/down arrow to match the display to calibrated
instrument.
3. Press Enter to store calibration.
4. Press the Mode key to return to Run mode.

Temperature Stabilization Periods

Startup - Allow 12 hours for the temperature in the cabinet to

stabilize before proceeding.
Already Operating - Allow at least 2 hours after the display
reaches set point for temperature to stabilize before proceeding.

During calibration, the temperature display will not be avail-

able.

If no keys are pressed for approximately five minutes while

in calibration mode, the system will reset to Run mode.

2-1
 Model 900 Series ___________________________________________________________________________Alarms

Section 3 - Alarms

3.1 Alarms

The Model 900 Series freezer alarms are displayed on the freezer control panel. When an alarm is active, the indicator next to
the alarm description will light and there will be an audible alarm. Press the Silence key to disable the audible alarm for the ringback
period. The visual alarm will continue until the freezer returns to a normal condition. The alarms are momentary alarms only. When
an alarm condition occurs and then returns to normal, the freezer automatically clears the alarm condition.

Description Delay Ringback Relay

Power Failure 1 min. 15 min. Yes
High Temperature Alarm 1 min. 15 min. Yes
Low Temperature Alarm 1 min. 15 min. Yes
Probe Failure see 3.2 1 min. 15 min. No
Door Open 1 min. 15 min. No
Clean Gasket 0 min. 3 months No
Low Battery 1 min. 12 hours No
Hot Condenser 1 min. none No
Clean Filter 0 min. 3 months No
All alarm delays and ringback times are ±30 seconds.

In addition to the alarms listed above, two other conditions 3.2 Probe Failure Alarm
are detected by the controls that will result in an audible and The microprocessor in 900 series freezers continually scans
visual alarm. These alarm conditions are unlikely to occur, and all probes including the control probe, heat exchanger probe and
as such, there are no LED's on the control panel to indicate these condenser probe to ensure that they are operating properly.
conditions exist. Should an error be detected, the "Probe Failure" alarm will occur
The first condition is when incorrect voltage is applied to as described in 3.1 above. If an error is detected with the control
the freezer. If a 230 V freezer is connected to a 120 V power probe, the high and low stage compressors will run continuously.
source or a 120 V freezer is connected to a 230 V power source, As a result, the cabinet temperature will decrease until it reaches
the electronics will detect that the "Wrong Power" has been the lowest temperature that the refrigeration system can main-
applied. Under this condition, the fans and compressors will not tain. If an error is detected with the heat exchanger probe, the
turn on and an audible and visual alarm will occur. The audible freezer will cycle properly at its temperature set point using a 5
and visual alarms will remain until the freezer is connected to minute step start between the high and low stage compressors.
the correct power source. The audible alarm cannot be silenced If an error is detected with the condenser probe, there is no
under this condition. impact on the performance of the freezer; however, the hot con-
denser alarm may also occur. Contact the Thermo Forma
The second condition is when a "high stage system fail-
Service Department (1-888-213-1790) or your local distributor.
ure" occurs. This condition is created when the high stage com-
pressor and fans run for 30 minutes and are not capable of cool-
ing the interstage heat exchanger to the proper temperature.
Under this condition, the high stage compressor and fans will
turn off after 30 minutes and an audible and visual alarm will
occur. The audible alarm can be silenced and will ring back
every 15 minutes.

3-1
 Model 900 Series ______________________________________________________________________Maintenance

Section 4 - Maintenance a. Cleaning the Water-cooled Condenser

4.1 Cleaning the Cabinet Exterior The water-cooled condenser can be cleaned-in-place
by using the CIP procedure. Cleaning solutions can be used,
depending on type of deposits or build-up to be removed.
Avoid the excessive use of water
around the control area due to the risk Do not use liquids that are corrosive to stainless
of electrical shock. Damage to the con- steel or the brazing material (copper or nickel).
trols may also result.

Wipe down the freezer exterior using soap and water and CIP (Clean-In-Place) Procedure
a general use laboratory disinfectant. Rinse thoroughly with
clean water and dry with a soft cloth. 1. Disconnect the unit from the water supply.
2. Drain the unit.
4.2 Cleaning the Air Filter (minimum of four times a 3 . Rinse with fresh water and drain the unit again.
year*)
4. Fill with fresh water.
1. Open the front lower door by grasping the bottom left 5. Add cleaning agent (solution and concentration depend-
corner. ent on deposits or build-up).
2. Locate the grille on the door. See Figure 1-5. Grasp the 6. Circulate cleaning solution (if feasible).
middle of the grille material and gently pull out to 7. Drain the cleaning solution.
remove.
8. Add and circulate a passivating liquid for corrosion inhi-
3. Wash the filter material using water and a mild deter- bition of plate surfaces.
gent.
9. Drain this liquid.
4. Dry by pressing between two towels.
10. Rinse with fresh water and drain.
5. Install the filter back into the grille and attach the grille.
11. Reconnect the water supply and fill the unit.
12 . Return to service.
* The Clean Filter alarm occurs every three months as a
reminder to clean the air filter. Depending upon environmental
conditions, the filter may need to be cleaned or replaced more
frequently. If the filter becomes torn or excessively dirty, a 4.4 Defrosting the Chamber
replacement can be purchased from Thermo Forma. See the
exploded parts list, Section 7, for filter part number. A filter kit 1. Remove all product and place it in another freezer.
(set of 5) is also available. 2. Turn the unit off and disconnect it from the power
source.
3. Turn off the power switch (see figure 5-1) to the bat-
4.3 Cleaning the Condenser (minimum of twice a tery(s).
year*)
4. Open all of the doors and place towels on the chamber
1. Open the front lower door by grasping the bottom left floor.
corner. See Figure 1-5. 5. Allow the frost to melt and become loose.
2. Using a vacuum cleaner, exercising care to not damage 6. Remove the frost with a soft cloth.
the condenser fins, clean the condenser. 7. After defrosting is complete, clean the interior with a
non-chloride detergent. Rinse thoroughly with clean
* Depending upon environmental conditions, the condenser water and dry with a soft cloth.
may need to be cleaned more frequently. 8. Plug unit in and turn power switch on.
9. Turn the battery power switch to the on position.
10. Allow the freezer to operate empty overnight before
reloading the product.

4-1
 Model 900 Series ______________________________________________________________________Maintenance

4.5 Cleaning the Door Gasket (minimum monthly*)

Using a soft cloth, remove any frost build-up from the gas-
ket and door(s). The Clean Gasket alarm occurs every three
months as a reminder to remove frost build-up from the gasket
and door(s). Press the Silence key to disable the audible alarm.

*The door gasket may need to be cleaned more frequently

if dirt or excessive frost build-up prevents the door from clos-
ing properly.

4.6 Cleaning the Vacuum Relief Port (minimum

monthly*)

Using a soft cloth, remove any frost build-up from the vac-
uum relief, located in the front left corner of the chamber. See
figures 1-3 and 1-4.
Figure 4-1

The vacuum relief port contains a small heating The % of charge can vary depending on the age,
element. If the freezer is not disconnected from usage and condition of the battery. For a consistent
the electrical supply or turned off at the power and dependable charge, replace the battery every 2
switch, the heating element will continue to years. Replacement batteries must be rechargeable
operate and may cause injury to personnel and are available from Thermo Forma. Refer to
cleaning the freezer chamber. the parts list for stock number and description of
the replacement batteries. Dispose of the used bat-
teries in a safe manner and in accordance with
good environmental practices.
4.7 Replacing the Battery(s)

1. To gain access to the battery, open the lower door by grasp-

ing the bottom left corner. The battery is rectangular in
4.8 Preparing the Unit for Storage
shape, located on the front left corner of the compressor
compartment and is secured in place by a mounting bracket
Defrost the unit as described in Section 4.4. This will pre-
with three bolts.
pare the unit for storage. Turn off the battery power switch.
2. Directly above the battery(s) is the battery power switch. Turn off the freezer power switch. Disconnect power to the bat-
Turn the battery power switch to the off position. tery(s) and to the freezer.
3. Disconnect the battery connections
4. Remove the three nuts securing the battery bracket.
5. Remove the bracket and old battery, install the new battery If the unit has been in service, turn it off and disconnect the
and secure. power cord connector before proceeding with any mainte-
6. Reconnect the battery (red to positive and black to nega- nance.
tive).
7. Turn on the battery power switch.
8. Close lower panel door.

4-2
Model 900 Series ________________________________________________________________________________________________________________Maintenance

PREVENTIVE MAINTENANCE
Freezers
Your Thermo Forma equipment has been thoroughly tested and calibrated before shipment. Regular preventive maintenance is important to keep
your unit functioning properly. The operator should perform routine cleaning and maintenance on a regular basis. For maximum performance and
efficiency, it is recommended that the unit be checked and calibrated periodically by a qualified service technician.

The following is a condensed list of preventive maintenance requirements. See the specified section of the instruction manual for further details.

Thermo Forma has qualified service technicians, using NIST traceable instruments, available in many areas. For more information on Preventive
Maintenance or Extended Warranties, please contact us at the number below.

Cleaning and calibration adjustment intervals are dependent upon use, environmental conditions and accuracy required.

Tips:
• Fill an upright by starting at the bottom near the probe and add racks to one shelf at a time. Allow freezer to recover to set point between shelves.
• Fill a chest by starting at the left side near the probe. Filling with room temperature racks will result in a long pull-down time.
• Fill unit with frozen product to help overall performance; frozen water jugs, for example.
• Always make certain the vacuum relief port is free of frost and ice, to allow for timely re-entry into the freezer after a door opening.

•Millcreek Road, Box 649 •Marietta, Ohio 45750 USA •740-373-4763

•USA and Canada 888-213-1790 •Telefax: 740-373-4189 •email: service@thermoforma.com

4-3
 Model 900 Series ________________________________________________________________________________________________________________Maintenance

Preventive Maintenance for 900 Series Freezers

Refer to Manual Section Action Monthly Yearly Every
2 Years
-- Verify ambient temperature, <90°F ;
-- * Adjust door handle for firm latching, as needed ;
Figure 1-4 for probe location Check and clean probe cover, gaskets, hinges, and vacuum relief port ;
4.5, 4.6 of ice and snow. More frequent cleaning may be
required, depending on use and
environmental conditions.
4.2 Check air filter. Clean or replace as needed ;
4.7 Check alarm back-up battery. ; ** Replace
-- Check condenser fan motor for unusual motor noise or vibration. ;
2 * Verify and document calibration, at the minimum, annually. ;
4.3 * Clean condenser compartment and wipe off condenser ;
* Qualified service technicians only
** Dispose of properly, according to all state and federal regulations.

4-4
 Model 900 Series ________________________________________________________________________Factory Options

Section 5 - Factory Installed Options The BUS operates on an internal 12-volt, rechargeable bat-
tery which is kept charged during normal operation by the inte-
5.1 BUS - Back Up System (195875, 195877) gral battery charger.

a. Installing the vent stack, solenoid and injection

assembly
Before installation of BUS components, make sure the power
to the freezer is disconnected, the battery switch is turned off 1. Install the injection assembly through the 1/2” pre-
and the freezer has warmed to ambient temperature. punched hole, directly behind the 2” vent stack hole in
the center of the chamber ceiling. Using a long blade
The built-in BUS (back up system) will keep the freezer screwdriver or similar instrument, punch a guide hole up
chamber temperature below the critical level in the event of a through the foam insulation to the top exterior ceiling
power or equipment failure. If power to the freezer fails, or tem- opening.
perature increases to the back up alarm set point, the BUS
injects liquefied gas into the chamber to keep the chamber tem-
perature within the specified range. CAUTION! Do not use the injection assembly to bore the hole.
The injection assembly could become clogged with insulation
and not function correctly.

Note: Cover the open end of injection assembly with tape to

keep insulation from entering the nipple.
2. Slide 3/8” flatwasher over open end of nipple.
3. Insert the covered end of the injection assembly through
the exterior hole.
4. Remove the tape covering from the end of the nipple and
install the 1/8” NPT brass tee on the open end of the nip-
ple. Place Permagum sealant between the brass tee and
the interior top.
5. Use the 1-3/8” x 20” copper tubing. Remove the plastic
cap from the beveled end (Caution - it is sharp!) and
place the cap on the non-beveled end. Position the
beveled end of the tubing against the foam opening and
use a back and forth twisting motion to cut a hole through
the insulation to the top external opening.

Figure 5-1

Figure 5-2

5-1
 Model 900 Series ________________________________________________________________________Factory Options

6. Remove the two Phillips head screws securing the metal 16. Connect power to the freezer. Leave the back-up battery
bracket on the vent stack assembly. switch at the OFF position. Turn the freezer on. The
7. Install the vent stack through the opening and secure it to Inject light on the BUS control panel will illuminate but
the top of the freezer, using screws. no injection will occur. The Low Battery indicator may
also illuminate. Once the freezer has stabilized at the
8. Go to the interior and seal around the end of the vent operating temperature, turn the battery switch on.
stack with permagum.
9. Install the transfer hose connecting one end to the injec-
tion assembly, the other end to the solenoid valve. Install
the solenoid valve to the supply source.

When selecting a CO2 supply cylinder, it must be equipped with

a siphon tube.

b. Installing the Temperature Probe

10. Locate the 0.500” pre-punched hole in the upper left hand
back corner of the chamber ceiling. Remove the tie wrap
securing the coiled probe/solenoid harness. Uncoil the
probe lead and run the probe tip (approximately 12”) Figure 5-4
down through 0.500” porthole (Figure 5-4).
11. As shown in
Figure 5-3, thread
the small tie wrap
through the open-
ings in the front of
the bracket.
Secure the probe
on the back of the
bracket with the
tie wrap.
12. Tap #8-32 the two
pre-punched holes
located on the
interior left wall
of the freezer. Figure 5-3
Mount the brack-
et. Figure 5-4 shows the Back-Up probe mounted on the
interior left side wall of the freezer.

c. Connecting the probe/solenoid harness

13. Remove the four screws on the freezer back panel and
use them to mount the tie wrap anchors as shown in
Figure 5-5. Secure the probe wire with tie wraps.
14. Plug the solenoid/probe connector into the BUS connec-
tion and secure with a screw on the right and left side.
The connector is keyed.
15. Loosen the terminal screws on the solenoid. Slide the
spade lug connectors under the screws and tighten to
secure.

Figure 5-5
5-2
 Model 900 Series ____________________________________________________________________Factory Options

Figure 5-6

BUS Operation and Maintenance 3. Press Enter to save the setting.

d. BUS Control Panel (see figure 5-6) 4. Press the Mode key until the Run indicator lights for Run
mode
If no control keys are pressed, the freezer will automatically
WARNING! When activated, this unit injects liq- return to to RUN mode after 5 minutes.
uid nitrogen or carbon dioxide. Liquid Nitrogen
can cause serious freezing (frostbite) if it comes in
contact with unprotected skin or eyes. Nitrogen The BUS set point must not be any colder than
suppresses oxygen levels and may cause suffoca- the high temperature alarm set point. (See section
tion if area is not well ventilated. Refer to 1.6.b). If the back-up system is installed with CO2,
Appendix A for the proper handling of liquid LN2. then -65°C is the coldest BUS set point that can
be used.

g. System Operation Check

Carbon Dioxide gas suppresses oxygen levels and
may cause suffocation if area is not well ventilat- It is advisable to periodically check the operation of the
ed. Refer to “Handling Liquid CO2 in Appendix B entire system. To check the system:
of this manual.
1. Close the valve at the gas source.
Power - indicates the unit has AC power and is operational. 2. Set the freezer temperature 12 - 15°C higher than the nor-
Low Battery - battery charge is low. The battery needs replaced. mal operating temperature.
Solenoid Engaged - BUS is actively injecting gas into the freezer 3. Listen for the gas valve to open as the freezer temperature
chamber. rises to the Back-Up unit set point.
Press-To-Test - Activates the solenoid and injects LN2 or CO2 4. Check the gas flow by momentarily opening the valve at
into the freezer chamber as long as the button is depressed. The the gas source.
solenoid engaged indicator should light. If the Low Battery indi- 5. Turn off the flow of gas.
cator lights during the test, replace the BUS battery.
6. Reset the freezer temperature to the normal operating tem-
e. Configuring the Optional BUS (Back Up System) perature, and allow the temperature to stabilize.
7. When the freezer has stabilized at the operating tempera-
The optional BUS can be configured for LN2 or CO2 supply. ture, open the valve at the gas source.
To select the supply type: h. Cleaning the Vent Stack
1. Press the Mode key until the Backup indicator lights.
2. Press the up or down arrow key. The display will show Routinely check the vent stack for frost or ice build-up. The
OP1 for CO2 selection and OP2 for LN2 selection. type of frost that forms in the vent stack is generally very soft
3. Press Enter to save the setting. and may be easily removed with a bristle brush or soft cloth. if
ice build-up has occurred, a complete defrost may occasionally
4. Press the Mode key until the Run indicator lights for Run be required. See section 4.4 for freezer defrost instructions.
mode
i. Disconnecting the Fitting Assembly and
If no control keys are pressed, the freezer will automatically Transfer Hose
return to to RUN mode after 5 minutes.
f. Setting the Optional BUS Set Point To disconnect the freezer back-up from the gas supply:
1. Close the supply valve.
The optional back up system is designed to inject CO2 or 2. Depress the test button on the BUS control box to remove
LN2 into the freezer compartment if the temperature rises above the gas from the line.
back up system set point. To set the BUS set point:
3. Slowly disconnect the fitting assembly from the supply (in
1. Press the Mode key until the Set Temperature and Backup the event that any gas remains in the line).
indicators light.
2. Press the up or down arrow key until the desired
BUS set point is displayed. 5-3
 Model 900 Series ____________________________________________________________________Factory Options

Figure 5-7
Recorder Details

5.2 Chart Recorder Program From To

a. Installing the chart paper 1 -40 30°C

2 0 60°C
1. Open the glass door of the recorder and press button #3 until
the pen begins to move outward. 3 -100 38°C
2. Unscrew the knob at the center of the chart and remove the 4 -5 50°C
paper. 5 0 100°C
3. Install the new chart paper, position the paper to the correct 6 -100 200°C
time line and replace the knob.
7 -115 50°C
4. Remove the cap from the felt pen and press button #3.
8 -10 70°C
Figure 5-8
Recorder Buttons
Calibrating the chart recorder:

The recorder must be in service for 24 hours before per-

forming the following calibration procedure.

1. Place an accurate thermometer in the chamber next to the

recorder probe.
2. Temperature probes for the recorder are located in the left
b. Recorder Calibration front corner of the freezer chamber (Figure 1-4).
3. After about three minutes, compare the thermometer reading
Changing the recorder range: with the chart recorder reading.
4. If an adjustment is necessary, press the #1 button to move the
The chart recorder contains eight temperature ranges and is pen to the left or the #2 to move the pen to the right. The but-
factory-programmed for the freezer. ton must be held about five seconds before the pen begins to
move. Release the button when the pen position matches the
1. Press and hold button #3 until the pen moves off the chart thermometer.
paper.
2. Press and hold for eight seconds button #1. NOTE: The felt-tip pen on the recorder requires periodic
3. Release the button and the pen will move to the current range replacement. Usually the ink will appear to fade before
on the range sticker. replacement becomes necessary. Additional pen tips
4. To change the program setting, press the left or right arrows to may be purchased from Thermo Forma. Refer to Parts
move the pen within the program ranges. List, Section 8.
5. When the pen is located on the desired range, press button #3
to bring the pen arm back onto the chart. Recording will
begin in the new program.

5-4
 Model 900 Series ____________________________________________________________________Factory Options

5.3 Datalogger

Thermo Forma dataloggers and ELPRO evaluation software

provide monitoring and documentation of temperature and alarm
conditions. The dataloggers have a memory capacity of 64,000
measured values or data points. Temperature is measured, stored
and displayed. Alarm conditions are recorded. Optional evalua-
tion software permits data to be downloaded to a PC. A variety
of statistical information is provided through calculations, analy-
sis, graphs and printed reports. Refer to the ELPRO documenta-
tion for operating instructions for the datalogger.

5.4 Water-cooled Condenser (195145, 195611)

The water-cooled condenser is a factory installed option and

requires a qualified technician at freezer installation. The instal-
lation should include proper adjustment of the regulating valve,
which controls the discharge pressure. Specifications for this
option are displayed in figure 5-9.
Water Source Tower City
Water Pressure Not to exceed 150 psig
Water Temperature Range Not to exceed 29.4C (85F)
Inlet Connection 0.5” compression
Outlet Connection 0.5” compression
Flow Rate Required 3.0 gallons (11.4 liters) per minute 1.0 gallon (3.8 liters) per minute
Drain Required No (return line is required) Yes

Figure 5-9

5.5 Five Inner Door Option (189405, 189406, 189407,

195642)

The five inner door option is factory installed. The freezer

is converted to accommodate four adjustable specimen shelves
with the fifth “shelf” as the bottom of the freezer chamber.

5-5
 Specifications - Single Door Units

Model 902 903 904 905 906 907

Model 900 Series _____________________________________________________________________Specifications

Temperature -50°C (-58°F) to -86°C (-123°F) in an 18C to 32C* (64.4F to 89.6F) ambient
Range
Exterior 33.3”W x 77.8”Hx31.0” 33.3”W x 77.8”Hx31.0” 33.3”W x 77.8”Hx37.0” 33.3”W x 77.8”Hx37.0” 40.8”W x 77.8”Hx37.0” 46.8”W x 77.8”Hx37.0”
Dimensions 84.6x197.6x78.7cm 84.6x197.6x78.7cm 84.6x197.6x94.0cm 84.6x197.6x94.0cm 103.6x197.6x94.0cm 118.9x197.6x94.0cm

Interior 23.0”Wx51.5”Hx19.3” 23.0”Wx51.5”Hx19.3” 23.0”Wx51.5”Hx25.3” 23.0”Wx51.5”Hx25.3” 30.6”Wx51.5”Hx25.3” 36.6”Wx51.5”Hx27.0”

Dimensions 58.4x130.8x49.0cm 58.4x130.8x49.0cm 58.4x130.8x64.3cm 58.4x130.8x64.3cm 77.7x130.8x64.3cm 93.0x130.8x68.6cm
Capacity 13.0 cu. ft. 13.0 cu. ft. 17.3 cu. ft. 17.3 cu. ft. 23.0 cu. ft. 28.0 cu. ft.
(368.1 liters) (368.1 liters) (489.9 liters) (489.9 liters) (651.3 liters) (792.8 liters)

Two 1 HP (2545 BTUH each)

Non-CFC, foamed-in-place urethane: 5.0”(12.7cm) cabinet; 4.5” (11.4 cm) door

Electrical 230V,50/60Hz, 12.0FLA 120V, 60 Hz, 16.0 FLA 120V, 60 Hz, 16.0 FLA 230V,50/60Hz, 12.0FLA 230V,50/60Hz, 12.0FLA 230V,50/60Hz, 12.0FLA
Operating Range: Operating Range: Operating Range: Operating Range: Operating Range: Operating Range:
208VAC-240VAC 108-130V 108-130V 208VAC-240VAC 208VAC-240VAC 208VAC-240VAC

Breaker 15 amp, 230V, 20 amp, 120V, 20 amp, 120V, 15 amp, 230V, 15 amp, 230V, 15 amp, 230V,
Requirements Dedicated Circuit, Dedicated Circuit, Dedicated Circuit, Dedicated Circuit, Dedicated Circuit, Dedicated Circuit,
15 Amp 20 amp 20 amp 15 Amp 15 Amp 15 Amp
Time Delay Breaker Time Delay Breaker Time Delay Breaker Time Delay Breaker Time Delay Breaker Time Delay Breaker
Shipping Weight: 690 lbs. (313.0 kg) 690 lbs. (313.0 kg) 790 lbs. (358.3 kg) 790 lbs. (358.3 kg) 880 lbs. (399.2 kg) 965 lbs. (437.7 kg)
Motor
Specifications - Double Door Units
6 -1

Model 991 992 993 994 995

Temperature -50°C (-58°F) to -86°C (-123°F) in an 18C to 32C* (64.4F to 89.6F) ambient
Range
Exterior 33.3”W x 77.8”Hx31.0” 33.3”W x 77.8”Hx31.0” 33.3”W x 77.8”Hx37.0” 33.3”W x 77.8”Hx37.0” 40.8”W x 77.8”Hx37.0”
Dimensions 84.6x197.6x78.7cm 84.6x197.6x78.7cm 84.6x197.6x94.0cm 84.6x197.6x94.0cm 103.6x197.6x94.0cm

Interior 23.0”Wx51.5”Hx19.3” 23.0”Wx51.5”Hx19.3” 23.0”Wx51.5”Hx25.3” 23.0”Wx51.5”Hx25.3” 30.6”Wx51.5”Hx25.3”

Dimensions 58.4x130.8x49.0cm 58.4x130.8x49.0cm 84.6x130.8x64.3cm 84.6x130.8x64.3cm 103.6x130.8x64.3cm
Capacity 13.0 cu. ft. 13.0 cu. ft. 17.3 cu. ft. 17.3 cu. ft. 23.0 cu. ft.
(368.1 liters) (368.1 liters) (489.9 liters) (489.9 liters) (651.3 liters)

Refrigeration Two 1 HP (2545 BTUH each)

Insulation Non-CFC, foamed-in-place urethane: 5.0” (12.7 cm) cabinet; 4.5” (11.4 cm) door

Electrical 230V,50/60Hz, 12.0FLA 120V, 60 Hz, 16.0 FLA 120V, 60 Hz, 16.0 FLA 230V,50/60Hz, 12.0FLA 230V,50/60Hz, 12.0FLA
Operating Range: Operating Range: Operating Range: Operating Range: Operating Range:
208VAC-240VAC 108-130V 108-130V 208VAC-240VAC 208VAC-240VAC
Breaker 15 amp, 230V, 20 amp, 120V, 20 amp, 120V, 15 amp, 230V, 15 amp, 230V,
Requirements Dedicated Circuit, Dedicated Circuit, Dedicated Circuit, Dedicated Circuit, Dedicated Circuit,
15 Amp 20 amp 20 amp 15 Amp 15 Amp
Time Delay Breaker Time Delay Breaker Time Delay Breaker Time Delay Breaker Time Delay Breaker

Shipping Weight: 710 lbs. (322.1 kg) 710 lbs. (322.1 kg) 810 lbs. (367.4 kg) 810 lbs. (367.4 kg) 880 lbs. (399.2 kg)
Motor

*Compressors may not cycle off with cabinet running at -86C in a 32C ambient.
 Model 900 Series _____________________________________________________________________Specifications

Certifications
Refer to the Declaration of Conformity at the back of this manual

Safety Specifications
Indoor Use Only
Altitude - 2,000 meters
Temperature - 5°C to 40°C
Humidity - 80% RH at or below 31°C, decreasing linearly to 50% RH at 40°C
Mains Supply Fluctuations - Mains supply voltage fluctuations not to exceed ±10% of the nominal voltage
Installation Category II 1
Pollution Degree 2 2
Class of Equipment I

____________________________________________________________________________________________________
1 Installation category (overvoltage category) defines the level of transient overvoltage which the instrument is designed to withstand safely. It
depends on the nature of the electricity supply and its overvoltage protection means. For example, in CAT II which is the category used for instru-
ments in installations supplied from a supply comparable to public mains such as hospital and research laboratories and most industrial laboratories,
the expected transient overvoltage is 2500V for a 230V supply and 1500V for a 120V supply.

2 Pollution degree describes the amount of conductive pollution present in the operating environment. Pollution degree 2 assumes that normally
only non-conductive pollution such as dust occurs with the exception of occasional conductivity caused by condensation.

6 -2
Model 900 Series ________________________________________________________________________________Parts

7-1
Model 900 Series ________________________________________________________________________________Parts

7-2
Model 900 Series ________________________________________________________________________________Parts

7-3
Model 900 Series ________________________________________________________________________________Parts

7-4
Model 900 Series ________________________________________________________________________________Parts

7-5
Model 900 Series ________________________________________________________________________________Parts

7-6
Model 900 Series ________________________________________________________________________________Parts

7-7
Model 900 Series ________________________________________________________________________________Parts

7-8
Model 900 Series ________________________________________________________________________________Parts

7-9
Model 900 Series ________________________________________________________________________________Parts
7 - 10
Model 900 Series ________________________________________________________________________________Parts
7 - 11
Model 900 Series ________________________________________________________________________________Parts

7 - 12
Model 900 Series ________________________________________________________________________________Parts

7 - 13
Model 900 Series ________________________________________________________________________________Parts

7 - 14
Model 900 Series ________________________________________________________________________________Parts

7 - 15
Model 900 Series ________________________________________________________________________________Parts

7 - 16
Model 900 Series __________________________________________________________________Refrigeration Schematics
8-1
Model 900 Series __________________________________________________________________Refrigeration Schematics
8-2
Model 900 Series __________________________________________________________________Refrigeration Schematics
8-3
Model 900 Series __________________________________________________________________Refrigeration Schematics
8-4
Model 900 Series __________________________________________________________________Refrigeration Schematics
8-5
Model 900 Series __________________________________________________________________Refrigeration Schematics
8-6
Model 900 Series __________________________________________________________________Refrigeration Schematics
8-7
Model 900 Series ______________________________________________________________________Electrical Schematics

9-1
Model 900 Series ______________________________________________________________________Electrical Schematics

9-2
Model 900 Series ______________________________________________________________________Electrical Schematics

9-3
Model 900 Series ______________________________________________________________________Electrical Schematics

9-4
Model 900 Series ______________________________________________________________________Electrical Schematics

9-5
Model 900 Series ______________________________________________________________________Electrical Schematics

9-6
 Model 900 Series _____________________________________________________________________________Appendix A

Appendix A

Handling Liquid Nitrogen

Contact of liquid nitrogen or cold gas with the skin or eyes may cause serious freezing (frostbite) injury.

Handle liquid nitrogen carefully.

The extremely low temperature can freeze human flesh very rapidly. When spilled on a surface the liquid tends to cover it com-
pletely and intimately, cooling a large area. The gas issuing from the liquid is also extremely cold. Delicate tissue, such as that of
the eyes, can be damaged by an exposure to the cold gas which would be too brief to affect the skin of the hands or face.

Never allow any unprotected part of your body to touch objects cooled by liquid nitrogen.
Such objects may stick fast to the skin and tear the flesh when you attempt to free yourself. Use tongs to withdraw objects
immersed in the liquid, and handle the object carefully.

Wear protective clothing.

Protect your eyes with a face shield or safety goggles (safety glasses without side shields do not give adequate protection).
Always wear gloves when handling anything that is, or may have been, in immediate contact with liquid nitrogen. Insulated gloves
are recommended, but heavy leather gloves may also be used. The gloves should fit loosely, so that they can be thrown off quickly
if liquid should splash into them. When handling liquid in open containers, it is advisable to wear high-top shoes. Trousers (which
should be cuffless if possible) should be worn outside the shoes.

A-1
 Model 900 Series _____________________________________________________________________________Appendix A

Introduction

The safe handling and use of liquid nitrogen in cryogenic refrigerators and dewar flasks is largely a matter of knowing the
potential hazards and using common-sense procedures based on that knowledge. There are two important properties of liquid nitro-
gen that present potential hazards:
1. It is extremely cold. At atmospheric pressure, liquid nitrogen boils at -320°F (-196°C).
2. Very small amounts of liquid vaporize into large amounts of gas. One liter of liquid nitrogen becomes 24.6cu. ft. (0.7ml) of
gas.
The safety precautions in this booklet must be followed to avoid potential injury or damage which could result from these two
characteristics. Do not attempt to handle liquid nitrogen until you read and fully understand the potential hazards, their conse-
quences, and the related safety precautions. Keep this booklet handy for ready reference and review.
Note: Because argon is an inert gas whose physical properties are very similar to those of nitrogen, the precautions and safe prac-
tices for the handling and use of liquid argon are the same as those for liquid nitrogen.
Use only containers designed for low temperature liquids.
Cryogenic containers are specifically designed and made of materials that can withstand the rapid changes and extreme tempera-
ture differences encountered in working with liquid nitrogen. Even these special containers should be filled SLOWLY to minimize
the internal stresses that occur when any material is cooled. Excessive internal stresses can damage the container.
Do not cover or plug the entrance opening of any liquid nitrogen refrigerator or dewar. Do not use any stopper or other
device that would interfere with venting of gas.
These cryogenic liquid containers are generally designed to operate with little or no internal pressure. Inadequate venting can
result in excessive gas pressure which could damage or burst the container. Use only the loose-fitting necktube core supplied or one
of the approved accessories for closing the necktube. Check the unit periodically to be sure that venting is not restricted by accumu-
lated ice or frost.
Use proper transfer equipment.
Use a phase separator or special filling funnel to prevent splashing and spilling when transferring liquid nitrogen into or from a
dewar or refrigerator. The top of the funnel should be partly covered to reduce splashing. Use only small, easily-handled dewars for
pouring liquid. For the larger, heavier containers, use a cryogenic liquid withdrawal device to transfer liquid from one container to
another. Be sure to follow instructions supplied with the withdrawal device. When liquid cylinders or other large storage containers
are used for filling, follow the instructions supplied with those units and their accessories.
Do not overfill containers.
Filling above the bottom of the necktube (or specified maximum level) can result in overflow and spillage of liquid when the
necktube core or cover is placed in the opening.
Never use hollow rods or tubes as dipsticks.
When a warm tube is inserted into liquid nitrogen, liquid will spout from the top of the tube due to gasification and
rapid expansion of liquid inside the tube.

Nitrogen Gas Can Cause Suffocation Without Warning!

Store and use liquid nitrogen only in a well-ventilated place.

As the liquid evaporates, the resulting gas tends to displace the normal air from the area. In closed areas, excessive amounts of
nitrogen gas reduce the concentration of oxygen and can result in asphyxiation. Because nitrogen gas is colorless, odorless and
tasteless, it cannot be detected by the human senses and will be breathed as if it were air. Breathing an atmosphere that contains less
than 18% oxygen can cause dizziness and quickly result in unconsciousness and death.
Note: The cloudy vapor that appears when liquid nitrogen is exposed to the air is condensed moisture; not the gas itself. The issu-
ing gas is invisible.
Never dispose of liquid nitrogen in confined areas or places where others may enter.
Disposal of liquid nitrogen should be done outdoors in a safe place. Pour the liquid slowly on gravel or bare earth where it can
evaporate without causing damage. Do not pour the liquid on pavement.

A-2
 Model 900 Series _____________________________________________________________________________Appendix B

Appendix B

Handling Liquid Co2

High concentrations of CO2 gas can cause asphyxiation! OSHA Standards specify that employee exposure to carbon
dioxide in any eight-hour shift of a 40-hour work week shall not exceed the eight-hour time weighted average of
5000 PPM (0.5% CO2). The short term exposure limit for 15 minutes or less is 30,000 PPM (3% CO2). Carbon diox-
ide monitors are recommended for confined areas where concentrations of carbon dioxide gas can accumulate.

Store and use liquid CO2 only in a well-ventilated place.

As the liquid evaporates, the resulting gas tends to displace the normal air from the area. In closed areas, excessive amounts of
CO2 gas reduce the concentration of oxygen and can result in asphyxiation. Because CO2 gas is colorless, odorless and tasteless, it
cannot be detected by the human senses and will be breathed as if it were air. Breathing an atmosphere that contains less than 18%
oxygen can cause dizziness and quickly result in unconsciousness and death.
Note: The cloudy vapor that appears when liquid CO2 is exposed to the air is condensed moisture; not the gas itself. The issu-
ing gas is invisible.
Never dispose of liquid CO2 in confined areas or places where others may enter.
Disposal of liquid CO2 should be done outdoors in a safe place. Pour the liquid slowly on gravel or bare earth where it can
evaporate without causing damage. Do not pour the liquid on pavement.

B-1
 Model 900 Series _____________________________________________________________________________Appendix C

First Aid

If a person seems to become dizzy or loses consciousness while working with liquid nitrogen or carbon dioxide, move to a well-
ventilated area immediately. If breathing has stopped, apply artificial respiration. If breathing is difficult, give oxygen. Call a
physician. Keep warm and at rest.
If exposed to liquid or cold gas, restore tissue to normal body temperature (98.6° F) as rapidly as possible, followed by protec-
tion of the injured tissue from further damage and infection. Remove or loosen clothing that may constrict blood circulation to the
frozen area. Call a physician. Rapid warming of the affected part is best achieved by using water at 108° F. Under no circumstance
should the water be over 112° F, nor should the frozen part be rubbed either before or after rewarming. The patient should neither
smoke nor drink alcohol.

C-1
 Thermo Forma
Millcreek Road, P.O. Box 649
Marietta, Ohio 45750
U.S.A.

Telephone (740) 373-4763

Telefax (740) 373-4189