~ wry eww wrerwe ww wewnevuevvuvw ve Basic Science(Chemisty) (22102) 0 mw VI vil ‘Maharashtra State Board of Technical Education Experiment No. 1@: Effect of temperature on viscosity Practical Significance Redwood viscometer -1 is equipment used by the manufacturing companies to determine the property like viscosity of their products. Oils are used in many industries as lubricant for different machines working on different temperature levels. Determination of effect of temperature on viscosity of various lubricating oil will help in selecting the relevant lubricating oil for different machines on different temperatures. Since the viscosity of lubricating oils changes with temperature the selection of lubricating oil for any machine become critical. Determination of effect of temperature on viscosity of various lubricating oil will helps us in use of relevant _ engineering materials in industry. Relevant Program Outcomes (POs). PO3 Experiments and practices PO10 Life-long learning Relevant Course Outcomes ) Use paints, varnishes and relevant engineering materials in industry. Practical Learning Outcome Determine the effect of temperature on viscosity for given lubricating oil using Redwood viscometer-I Practical Skills ‘Measurement skills 1. 2: Measurement of the temperature Measurement of flow rate Relevant Affective domain related Outcomes a ei ‘Minimum Theoretical Background a). Viscosity is the property of a homogeneous fli b) °) Demonstrate working as a leader/a team member Practice good housekeeping , which causes it to offer frictional resistance to motion. Viscosity is the property of a fluid that determines its resistance to flow. It is an indicator of flow ability of a lubricating oil; the lowest the viscosity, greater the flow ability. Viscosity generally decreases with increase in temperature, The rate of change of viscosity over the range of temperature is called as the viscosity Index. A relatively small change/no change in viscosity with temperature is indicated by high viscosity index whereas low viscosity index shows relatively large change in viscosity with temperature. 5‘Basic Sclence(Chemistry) (22102) 4) Viscosity is resistance to flow. Viscosity and flow rate are inversely Proportional to each other . This resistance in turn is directly proportional to the viscosity. VIE Experimental set-up ‘tirerbinde Pointer . Sines siels Vale rod steal 122mm cia : Eimenan Leveng Redwood Viscometer IX Resources required ‘Sr. [Name of resources Specifications Quantity | Remark No. . T_| Red Wood viscometer no. I a 2_| Stop watch 2 ° 3_| Kohirausch flask 02 4 | Thermometer 04 5_| Filter Paper 6 | Oil sample z X Procedure 1. Clean the viscometer with the help of water. 2. Level the viscometer with the help of leveling screws. 3. Fill the outer cup with water for determining the viscosity at different temperatures. 4, Place the ball valve on the jet to close it and pour the test oil into the cup up to the tip of indicator. 5. Place a clean dry Kohlrausch flask immediately below and in the line with discharging jet. 6. Insert a clean thermometer and a stirrer in the cup and cover it ith a lid. “Maharashtra State Board of Technical Education 764660 ¢860 Ce CE ee euvesvsse ve CEU CEKECUHSEHTHUHUUHOWToWwuves Basic Science(Chemisty) (22102) 7. Heat the water bath slowly with constant stirring. When the oil in the cup attains a desired temperature, stop the heating, 8. Lift the ball valve and start the stop watch. Oil from the jet flows into the flask. 9. Stop the stop watch when lower meniscus of the oil res neck of receiving flask. 10. Perform the experiment at three elevated temperatures to get readings of flow time. XI Precautions ‘aches the 50 ml mark on the 1. An oil should be filtered thoroughly using muslin cloth to remove solid particles that may clog the jet. 2. The receiving flask should be placed in such a manner that the oil stream from Jet strikes the neck of receiving flask and do not cause any foaming 3. After each reading the oil should be completely drained out from receiving flask XI Actual procedure followed. AG Peer Sted Rothe. XIII Resources used (with major specification 9001...... WISI EN. XIV Precautions followed “TAS Pex. Sven. in mannual. XV Observations moannual Flow time ‘tin seconds Sr.No | Temperature of | Temy ire of oil fer 40% Soc 5-22 Secondg 2 60°C 30 | 9. nds _| 3 80°C 90°. 1:52. Seconds. XVI Results Viscosity of oil sample at 40°C is H.fgheat, . (Highest/Moderate/Lowest) Viscosity of oil sample at 60°C is MEd... (Highest/Moderate/Lowest) Viscosity of oil sample at 80°C is ..\OUI€Sb....... (Highest/Moderate/Lowest) XVII Interpretation ote eo ods Viscosity of oil .. AECAEOSRG...(increases/decreases) with {ACBLAGES (increase/ decrease) in temperature and thus its flow rate 10 {crease/Decreases) ‘Maharashira State Board of Technical Education+ Basic Science(Chemisty) 22102) XVIII Conclusions and Recommendations As the viscosity XIX Practical Related Questions 1. Describe the process for cleaning of Redwood viscometer. Name various types of viscometer. Explain the importance of water bath in the Redwood viscometer. Write precautions to be taken while performing the practical Explain proper way to place the receiving flask. XX_ References / Suggestions for further Reading Sr. Title of Book Author Publication No. 1 | Engineering Chemistry | Jain andJain | Dhanpat Rai and sons; New Delhi, 2015, ot ISBN : 9352160002, 2 | Engineering Chemistry | Dara, S.S. S.Chand. Publication, New Delhi, 2013, ISBN; 8121997658 3 | Experiments and DrS.S.Dara S.Chand, Publication, New Delhi, 2011, calculations in ISBN: 8121908647 engineering chemistry 4 | Practical Chemistry Dr.N.K.Verma | Laxmi publication New Delhi 2012 ISBN bl 81-7008-594-2 5 | Engineering Chemistry | Shashi Chawla | $.Chand. Publication, New Delhi, 2013, ISBN; 1234567155036 XXI_ Assessment Scheme Process related assessment scheme Sr. Process related Weightage(60%) No. 1_ | Process for cleaning of Redwood viscometer. 15% 2__| Process for maintaining temperature, 15% 3_| Reading of temperature. 15% 4 | Operation of stopwatch, 15% Product related assessment scheme Sr. | Product related Weightage(40%) No. 1._| Determination of the viscosity index 40% List of Student Team Members ‘Maharashira State Board of Technical Education \ 78SSR UU HUUH CHOKE KOKOKCKOKCKCGEEKCKEHHOHK CES Basic Science(Chemistry) (22102) Marks Obtained “| Dated Process] Product | Total | Signature of Related (15) | Related (10) Teacher @5) [Space to Write Answers] fa Reda ead. Uiscomeles..1.. clean...by. using... aie conten “both._1S.uged.....eo...oaderr..km..beab. Hoe. wothh..cangtand eee es 319.27..An...0ll.. I Should. he... _-thasougth ust ng. i ati = ae Sol fd... podizcles : ear should be...placed. ta. aa Herbed Hoat....01.| eee From. Jet Statkes. the. oie es Hasls.cnd..clo. col OF. COURSE... LOY, Mog. “Co. PPlezs. foe. Se tee, ot. Sido paid 14. -~tredussond ‘Maharashtra State Board of Technical Education