M04-Calibrating Measuring and Analysis System
M04-Calibrating Measuring and Analysis System
Technology
Level-IV
Based on October, 2023 Curriculum
Version 2
October, 2023
Addis Ababa, Ethiopia
Ministry of Labor and Skills wish to extend thanks and appreciation to the many
representatives of TVT instructors and respective industry experts who donated their time
and expertise to the development of this Teaching, Training and Learning Materials
(TTLM).
The nature of failure varies widely as do the causes of failure and the events
leading to failures. The failure of system could be due to:
em.
Attempts have been made to reduce failures of man- made systems with the
introduction of safety measures, quality control, reliability analysis, condition
monitoring and other approaches in design in order to reduce the probability of
failure. Use of measures such as factor of safety are usually resorted to in order to
improve the reliability of design and where health of the person is at great risk. Such
factor has to be very high reducing probabilities of accidents/ disaster to a very low
level.
3. Risk Control:
On Site Emergency Planning: he onsite emergency plan would be related to the final
assessment and it is the responsibility of the workers management to formulate it. The
plan must there fore, be specific to the site.
The plan sets out way in which designated people at the site of the incident initiate
supplementary action either inside or outside the workers at an appropriate time. An
essential of the plan is the provision for making the affected unit safe, for example,
by shutting it down. The plan also contains the full sequence of key personal to be
called in from other sections or from off site.
Off Site Emergency Plan:The offsite emergency plan is an integral part of any major
hazard control systems.It was based on those accidents identified by the works
management, which could affect people and the environment outside the works. Thus, the
offsite plan follows logically from the analysis that took place to provide the basis for the
onsite plan and the two plans was therefore complement each other. The key feature of a
good offsite emergency plan is flexibility in its application to emergencies other than
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those specifically included in the for mation of the plan The role of the various parties
that may be involved in the implementation of an offsite plan are described below. The
responsibility for the off site plan has been likely to rest either with the works
management or with the local authority.
Aspects to be included in an offsite emergency plan, some of the aspects to be
included in offsite emergency plan are as follows.
Emergency Control Centers :The emergency control center is the place from which the
operations to handle the emergency will be directed and coordinated. It has been attended
by the site work main controller, key personnel and the senior officers of the fire and
police services. Emergency control centers had therefore contained the following:
1. An adequate number of external telephones.
2. An adequate number of internal telephones
3. A plan of the workers to show
4. Areas where there are inventories of HSD and chlorine
5. Sources of safety equipment
6. Assembly point
7. Truck parking information
8. A nominal roll of employee
9. List of personnel with addresses telephone numbers
10. Specialized monitoring equipment will be available at all the sensitive points to
deal with small to medium spillages of the chemical.
11. The equipment operators must be trained in development of the equipment.
General Safety Rules:At the existing plant where fuels chemicals and other materials
are reactive in nature following general guidelines are made.
1. Fitting dress and use of personnel protective equipment recommended for
respective job has been adhered to by everyone.
2. All unsafe conditions or natural occurrences have been reported promptly to the
supervisor/ head of the department of safety.
Personal Protective Equipment: Personnel protective equipment play vital role in
reducing the losses in case of an accident. They provide protection to the workmen from
injuries during the execution of job. The various protective equipments are suggested as
below. Gloves and protective clothing: Since the chemicals are very corrosive and toxic,
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those called upon to handle has been provided with gloves and protective clothing.
Safety He lmets: Every one inside the plant and the visitors has to wear safety
shoes for protecting their toes and heels. The material of the shoes has required
being resistant to the type of chemicals available within the plant .Safety Belts: Safety
belts provide protection in case of fall while working at height .Safety goggles and face
shie lds : Suitable goggles protect the eyes from flying objects and harmful rays of
welding and furnace flames and also heat, dust and chemicals substances. Standard
welders goggles, face shield or hood has been used
1.2 Measuring Instruments for Calibration
Calibration is a comparison of two instruments against each other, one being the standard
(the calibrator). This process is essential to document the error of the instrument being
calibrated and to increase its accuracy All instruments have errors and decreasing
accuracies after a certain amount of time.
Reason of Calibrate your Instruments
The biggest reason behind performing periodic calibration of instruments is to test and
ensure that they make correct and accurate measurements .Regular calibration establishes
efficient instrument performance, safety during operations, long term sustainability, and
high instrument quality
All electric and electronic instruments drift over time with continuous usage.
Environmental conditions such as extreme temperature fluctuations, changing
weather, excess or lack of humidity can affect an instrument’s drift too. In most
instruments, greater usage means greater drift.In instruments requiring extreme
accuracy and precision, drift can be highly critical. Drift beyond the specified
tolerance also poses a safety hazard. To avoid these inaccuracies, it is important to
perform periodic instrument calibration.
Calibration helps identify the amount of drift, which helps analyze instrument stability
and measurement consistency.
Apart from drift, instruments are also prone to damage and defects due to loose
connections or faulty components. This damage can be detected at an earlier stage with
the help of calibration, and a total breakdown of the instrument can be safely
prevented.Once the defects are identified, the error propagation can be minimized,
reducing costs and resources of handling serious damages.
Proactive Safety
In industries such as oil and gas, petrochemical, chemical, energy, power, electric, and
electronic, there is a high risk of explosions, fires, and leakages. The measurement
equipment used in these industries must be calibrated regularly and properly to avoid
safety hazards and ensure employee safety and infrastructure safety.In other industries
such as pharmaceutical, food, and beverage, the calibration of instruments is necessary
for consumer/customer safety.
Reputation of Quality
Calibration is also important for social corporate responsibility, environmental and
financial reasons. Most companies and their customers have a quality system that needs to
be adhered to. Governments and regulatory bodies also lay down conditions that need to
be met to certify the company’s quality system, such as emission monitoring and
equipment testing. Measurement instruments used for these purposes should be highly
accurate which is why they need to be calibrated from time to time using calibration
techniques and equipment accredited to relevant ISO standards.
Labs and test equipment companies that adhere to updated standards like
ISO/IEC17025:2017 establish their competence in quality management, improved lab
testing environments, better customer satisfaction, an international reputation, &
systematic processes.
While calibration may seem like an additional cost, it must not be neglected. Calibration
has long-term benefits. Not calibrating your instruments regularly can lead to undesirable
results, including:
The manufacturing industry often faces the issue of false passes or false failures.
False passes may result in inferior and low-quality products being manufactured
and sold, reducing the credibility of the production factory.
False failures unnecessarily increase the manufacturing or reworking costs and
may end up discarding high quality and fully functioning products.
A lot of electric and electronic industries and laboratories require high precision
measurements with very small acceptable errors.
Not calibrating your measurement instruments can leave these errors unnoticed and
unattended, and can distort your final measurements and give highly inaccurate
results.
Errors in measurements can deviate the final output from the globally agreed
standards. This means the entire process of testing and measurement will need to be
repeated with new or repaired measurement instruments, making the process both
time-consuming and expensive.
Penalties
Benefits of Calibration
It is used for businesses that use thermal cameras, thermometers, humidity generators,
weather stations, and other instruments with their primary input as temperature and
humidity. This type of calibration is carried out in closed environments to eliminate
disturbances from the surroundings and atmosphere.
Pressure Calibration
It is used for instruments such as transmitters, test gauges, and barometers. In pressure
calibration, the spectrum of hydraulic and gas pressure is measured.
It is used for equipment such as torque wrenches, micrometers, scales, and balances.
Mechanical calibration calibrates for factors like force, mass, vibration, or torque to
ensure instrument accuracy.
Electrical Calibration
It is used for testing instruments such as clamp meters, data loggers, and insulation
testers. Equipment that measures frequency, voltage, or resistance should undergo
electrical calibration.
While there is no specific single to call attention to this need, there are some ways to
determine how often you should calibrate your instruments. The simplest thing to do is to
follow the equipment manufacturer’s recommendation. Manufacturers often provide
specifications about a device’s calibration and calibration period.
Another important factor to consider is the measurement location criticality and accuracy
requirements. Some measurements require greater accuracy compared to others. The
more critical locations should be calibrated frequently, while the less critical locations can
be calibrated in longer intervals.
If an instrument is used often and is subjected to high workload and extreme or harsh
operating conditions, it is good practice to calibrate often. The stability history of an
instrument should also be factored in. If the instrument has a demonstrated history of
being stable, it can be calibrated less frequently. On the other hand, if it has been shown
to drift quickly, it should be calibrated more often.
You should get your instruments professionally calibrated on a regular basis as inaccurate
readings may not fully represent the dangers of unsafe working environments. The
recommended frequency of calibration may vary, depending on manufacturer
recommendations, however generally for most items no longer than 12 months is
recommended. Some extremely stable items with limited parts and movement, no
dissimilar metals and other factors that reduce the likelihood of drift, and are continuously
stored in a controlled environment; calibration intervals over 12 months may be
considered.
Electrical calibration
Insulation testers
Clamp meters
Counter timers
Multimeters
Multifunction Testers
Oscilloscopes
Data loggers
Loop testers
Residual-current devices
Calibration professionals work with pneumatic and hydraulic pressure across a range of
sectors with various types of pressure gauges, transducers, balances and other devices.
Barometers
Analogue and digital pressure gauges
Test Gauges
Digital Indicators
Pressure Transmitters
Pressure Calibrators
Pressure Transducers
All processes where temperature readings play a critical role require temperature
calibration. The calibration tech performs this in a controlled environment with state-of-
the-art and highly precise equipment. Examples of equipment that requires periodic
calibration include:
Mechanical calibration
This process involves calibrating a number of elements such as force, mass, volumetric
dimension, angle, flatness, torque and vibration in a temperature-controlled facility. Some
of the most frequently tested instruments for mechanical calibration include:
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Torque tools (screwdrivers and wrenches)
Load cells and force gauges
Micrometers
Height gauges
Vernier calipers
Balances and scales
Weight and mass sets
Testing the instrument requires collecting sufficient data to calculate the instrument’s
operating errors. This is typically accomplished by performing a multiple point test
procedure that includes the following steps:
Using a process variable simulator that matches the input type of the instrument, set a
known input to the instrument Using an accurate calibrator, read the actual (or reference)
value of this input.
This process is repeated for a series of different input values and sufficient data is
collected to determine the instrument’s accuracy. Depending upon the intended
calibration goals and the desired error calculations, the test procedure may require from 5
to 21 input points.
The first test that is conducted on an instrument before any adjustments are made is called
the As-Found test. If the accuracy calculations from the As-Found data are not within the
specifications for the instrument, then it must be adjusted.
It is absolutely essential that the accuracy of the calibration equipment be matched to the
instrument being calibrated. Earlier on, a safe rule of thumb stated that the calibrator
should be an order of magnitude (10 times) more accurate than the instrument being
calibrated. As the accuracy of field instruments increased, the recommendation dropped
to a ratio of 4 to 1. Many commonly used calibrators today do not even meet this ratio
when compared to the rated accuracy of HART instruments.
The task of the calibration system is to estimate the static and slowly varying amplitude,
phase and delay differences among the feed elements (caused by propagation
impairments and changes induced by satellite and ground equipment) and to apply the
appropriate correction to reduce these errors.
The calibration methods may be categorized and compared with respect to the following
main characteristics .Operational representativeness of the calibration method (i.e.,
calibration under operational loading condition in terms of temperature, power supply
loading, leakages, etc.) need for a dedicated calibration mode and capability to detect
failures of payload modules
4. From the following which one is true Electrical equipment requiring calibration inclu:
D. Oscilloscopes E. All
List all instruments and indicate whether or not they are critical equipment. An instrument
is critical if the measurements of that instrument significantly affect the safety, quality or
proper operation of an installation.
Tip: If instruments are built into a specific installation or machine or belong to a specific
technician, it is good to record this as well. You can of course only calibrate these
instruments when they are not in use. If you record this properly, it will help you later
when planning the calibrations.
For each instrument, record the details that are important for the calibration. These
include: the measurement range, both the allowable deviation and the required accuracy
of the calibration, and the calibration interval.
The permissible deviation and the calibration interval are sometimes the subject of
discussion. Consider in advance what your choice is based on: will you follow the
manufacturer's advice, your own (risk) assessment or are there (legal) standards that must
be followed? In any case, make sure that you properly record what your choice is based
on. This will help you later on to determine how to deal with deviations.
Now that you've done this, you can establish a standard operating procedure (SOP) for the
calibrations. In it you lay down which steps you have to go through during the calibration,
which measuring points you use, what requirements the calibration equipment should
fulfill (for example, how much more accurate should the calibration standard be
compared to the measurement instrument) and how the results should be interpreted.
By doing this you ensure uniformity, and the calibration process becomes verifiable and
repeatable whether you perform it yourself or (partially) outsource it.
All blunders must be found and eliminated prior to submitting a survey for inclusion in
the project mapping. The surveyor must remain alert and constantly examine
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measurements to eliminate these mistakes. Blunders can be detected and eliminated by
reacting to “out-of- tolerance” messages by the data collector when they occur. They can
also be detected by carefully examining a plot of the collected survey points while in the
office.
2. Types of Errors
There are two types of errors, systematic and random. It is important for the surveyor to
understand the difference between the two errors in order to minimize them Systematic
Errors
Systematic errors are caused by the surveying equipment, observation methods, and
certain environmental factors. Under the same measurement conditions, these errors will
have the same magnitude and direction (positive or negative). Because systematic errors
are repetitive and tend to accumulate in a series of measurements, they are also referred
to as cumulative errors.
Although some systematic errors are difficult to detect, the surveyor must recognize the
conditions that cause such errors. The following list includes several examples of
systematic errors:
instrument.
The effect of these errors can be minimized by:
ing the correct instrument heights, targets heights, and prism offset in the data
collector.
If appropriate corrections are not made, these errors can accumulate and cause significant
discrepancies between measured values. By keeping equipment in proper working order
and following established surveying procedures, many of the systematic errors can be
eliminated.
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Random Errors
Random (or accidental) errors are not directly related to the conditions or circumstances
of the observation. For a single measurement or a series of measurements, it is the error
remaining after all possible systematic errors and blunders have been eliminated.
As the name implies, random errors are unpredictable and are often caused by factors
beyond the control of the surveyor. Their occurrence, magnitude, and direction (positive
or negative) cannot be predicted. Errors of this type are compensating and tend to at least
partially cancel themselves mathematically. Because the magnitude is also a matter of
chance they will remain, to some degree, in every measurement.
Misclosures (or residuals) are the difference in a measurement or a series of
measurements from an established value. Random errors account for the misclosure
when systematic errors have been corrected and blunders have been removed.
Misclosures are computed when adjusting level loops, traverses, and GPS networks.
Random errors conform to the laws of probability and are therefore equally distributed
throughout the survey. Because of their random nature, correction factors cannot be
computed and applied as they are with some systematic errors. However, they can be
estimated using a procedure based on the laws of probability known as the least-squares
method of adjustment. This method computes the most probable adjusted values and the
precision of the survey. The least-squares method may also reveal the presence of large
blunders.
3. Error Sources
There are a variety of factors that can lead to measurement errors. Errors typically arise
from three sources; natural errors, instrument errors, and human errors.
a. Natural Errors
Natural errors are caused by environmental conditions or significant changes in
environmental conditions. Wind speed, air temperature, atmospheric pressure, humidity,
gravity, earth curvature, and atmospheric refraction are examples of natural error sources.
Many of these environmental conditions can be compensated for by applying a correction
factor to each measurement. Commonly used correction factors are the parts per million
(ppm) and curvature and refraction constants.
The ppm correction factor is applied to slope distances to minimize the effects of
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atmospheric changes. The correction is determined using observed temperature and
pressure readings. With each instrument setup, new temperature and pressure readings
should be taken and the ppm constant revised, if necessary. The curvature and refraction
constant is applied to the vertical distance measurement. The constant corrects for the
Earth’s curvature and atmospheric refraction and should be applied to the survey by the
data collector.
There are other natural phenomena that can lead to measurement errors. Intense, direct
sunlight may cause differential expansion of the components of the instrument, resulting
in minor errors. This effect can be minimized by operating on cloudy days, times of low
Measurements and Errors
Heat waves can cause distortion in lines of sight near reflective surfaces. The effects of
heat waves can be minimized by surveying in cooler, cloudy periods, taking shorter
measurements, or avoiding measurements taken over asphalt or concrete in excessively
hot weather.
b. Instrument Errors
Instrument errors are caused by imperfectly constructed, adjusted, or calibrated surveying
equipment. Most of these errors can be reduced by properly leveling the instrument,
balancing backsight/foresight shots, reducing measurement distances, and observing
direct and reverse positions (double centering).
Prolonged storage, exposure to rapid changes in temperature, and jarring during
transportation may lead to instrument maladjustments. Collimation and other sighting
errors can be determined and compensated for by specific instrument adjustments.
Before making instrument adjustments or beginning surveying operations, allow the
instrument to adapt to the ambient temperature before proceeding.
Instrument errors can be further minimized by periodically calibrating surveying
instruments, prisms, rods, and tribrachs. Yearly maintenance agreements are purchased
to ensure that WYDOT surveying instruments are regularly cleaned, calibrated, and
adjusted by an authorized technician. Occasionally during these services visits, the data
collector’s operating system (firmware) will be replaced with a more current version.
It is equally important that equipment suspected of being out of tolerance is sent to the
appropriate service center. The Photogrammetry & Surveys Section should be notified
prior to sending equipment for unscheduled adjustment, calibration and/or repairs.
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C.. Human Errors
Human errors are caused by physical limitations and inconsistent setup and observation
habits of the surveyor. For example, minor errors result from misaligning the telescope
crosshairs on the target or not holding the target rod perfectly plumb. These errors will
always be present to some degree in every observation. However, by following
established setup and collection procedures, many potential errors can be minimized.
Because any survey is only as accurate as the instrument/target setup; a secure, level
tripod is paramount. A tripod should always be used to stabilize the backsight target
when placing it over a control point. When positioning the tripod, firmly press the tripod
feet into the ground. Place the tripod legs in a position that will reduce the amount of
walking near the instrument. Minimizing movement around the tripod will reduce the
chances of bumping it. In windy conditions, it may be necessary to place sandbags on the
feet of the tripod to ensure stability. When setting up on steep slopes, position two tripod
legs on the downhill side. Periodically check the optical plummet to verify that the
instrument is still centered over the point. Periodically check the level bubble to ensure
that the instrument is still on a horizontal plane. The level bubble should hold one
position when the instrument is smoothly rotated through a complete revolution.
When taking an observation with an optical instrument, the center of the target should
coincide with the center of the reticle (or crosshair). To obtain accurate results,
consistently sight the telescope to the same part of the target. Turn the ocular (or eye
piece) until the reticle is clearly focused. Then adjust the focusing knob until the target is
clearly defined within the field of view. When the observer’s eye moves behind the
ocular, the target and reticle should not be displaced with respect to one another
1. Identify the process variable and the desired operating range. What is the
variable that the instrument is monitoring? What are the desired minimum and
maximum values for this variable?
2. Consider the instrument's accuracy and repeatability. How accurate is the
instrument? How repeatable is its output?
3. Determine the desired set-point value. This value should be within the
instrument's accuracy and repeatability specifications and within the desired
operating range of the process variable.
4. Set the instrument's set-point value. This is typically done using the
instrument's programming interface.
5. Verify the set-point value. This can be done by simulating the process variable
and observing the instrument's output.
By following the steps and considerations above, you can ensure that your instrument set-
points are established correctly and that they will help to ensure the safe and efficient
operation of your process.
The specific steps involved in adjusting a measuring system will vary depending on the
type of system and the manufacturer's instructions. However, the general principles are
the same for all measuring systems.
1. A blunder (or gross error) is a significant, unpredictable mistake caused by human error
2. Keeping up-to-date records is an important aspect of the calibration process
3. In measurement Errors means by definition, are the difference between a measured
value and its true value
4. Measuring system adjustment is the process of correcting the output of a measuring
system to ensure that it accurately reflects the true value of the measurand
5. Wind speed, air temperature, atmospheric pressure, humidity,
gravity, earth curvature, and atmospheric refraction are examples of Instrument Error
Step1 :-Connect the hand pump calibrator to the pressure gauge to be calibrated using the
appropriate adapter or fitting.
Step 3:-Slowly pump the hand pump calibrator until the desired pressure is reached.
Step4:-Observe the pressure gauge and ensure that it reads the same pressure as the hand
pump calibrator.
Step5:-If the gauge does not read the correct pressure, adjust it according to the
manufacturer's instructions.
Step6:-Repeat the process at multiple pressure points to ensure the gauge is accurate
throughout its range.
Step7:-Record the results of the calibration and make any necessary adjustments.
Step8:-Once calibration is complete, disconnect the hand pump calibrator and store it
properly.
Lap Test 2
Instruction :-Given the necessary tools and materials you are expected to perform the
following tasks within 1:20 hour.
Task 1:- :- procedure to calibrate a pressure gauge
Eye PPE is designed to protect workers’ eyes from foreign objects, splashes, burns,
radiation and more. The type of eye protection equipment required varies based on the
hazards present in the environment. For example, workers involved with lawn care may
use safety glasses to prevent foreign objects from hitting them in the eye, while welders
need welding shields to protect their eyes from burns. Below is a list of the basic types of
PPE designed for eye protection
Ear protection equipment is designed to prevent hearing loss that could be caused by
exposure to workplace noise. There are several layers of noise protection equipment. For
example, some earplugs are designed for single use, while others are molded to the
individual’s ear and can be used for a designated time period. Earmuffs are also an
option. These form a physical barrier around the ear, offering increased protection from
workplace noise exposure.
Head PPE is designed to protect workers from the risk of impact, whether that is caused
by bumping into objects in confined spaces, or falling objects. As such, there are several
classifications of personal protection equipment designed to protect workers’ heads. For
example, “bump caps” are low profile, and can even include baseball style caps. These
are not ANSI rated, and will not provide adequate protection for industrial settings.
PPE designed to protect the body might include specialized clothing, shoes, and gloves.
The types of materials from which this gear is made determines the level of protection it
offers. For example, fire resistant clothing is designed specifically to be less flammable to
provide an extra layer of protection to employees working in the chemical industry. Steel
toe boots are designed to protect toes against falling objects and compression, and are
worn by workers in many industries. The level of protection required varies based on the
risks present in a work setting. Some applications may require a full HAZMAT suit to
protect workers from biological substances, chemicals, etc. While other applications may
only require employees to wear nitrile gloves to protect workers and end users from
pathogens.
Liquid analytical systems play a pivotal role in various industries, enabling precise and
comprehensive analysis of liquids in a range of applications. These systems integrate
cutting-edge technologies to measure and monitor crucial parameters, providing essential
insights for quality control, process optimization, and environmental monitoring. In this
article, we delve into the intricacies of liquid analytical systems, exploring their
components, working principles, and diverse applications.
Liquid analytical systems typically consist of sensors, transmitters, and control units.
Sensors, tailored for specific parameters such as pH, conductivity, dissolved oxygen, or
turbidity, employ various techniques including electrochemical, optical, and thermal
methods. These sensors measure target properties, converting them into electrical signals.
Transmitters amplify, process, and transmit these signals to the control unit, where
advanced algorithms and software algorithms facilitate data analysis and interpretation.
Applications:
The applications of liquid analytical systems are vast and varied. In the pharmaceutical
industry, they ensure the quality and safety of medications by monitoring critical
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parameters during production processes. In wastewater treatment plants, these systems aid
in maintaining optimal conditions for efficient purification. They also find applications in
food and beverage production, chemical processing, and environmental monitoring.
Here are some additional tips for diagnosing faults in systems and components:
Fig 3.9 Flow chart for the repair of a damaged structure made of composite