Scribd
Upload
11 views4 pages

Experiment No. 02: ID: Date

The document outlines an experiment for standardizing hydrochloric acid (HCl) solution using sodium hydroxide (NaOH) solution through a neutralization reaction. It details the theory behind the experiment, the apparatus and reagents needed, and the step-by-step procedure for conducting the titration. Experimental data tables are provided for recording observations and calculations to determine the strength of the HCl solution.

Uploaded by

10241019340
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
11 views4 pages

Experiment No. 02: ID: Date

The document outlines an experiment for standardizing hydrochloric acid (HCl) solution using sodium hydroxide (NaOH) solution through a neutralization reaction. It details the theory behind the experiment, the apparatus and reagents needed, and the step-by-step procedure for conducting the titration. Experimental data tables are provided for recording observations and calculations to determine the strength of the HCl solution.

Uploaded by

10241019340
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
You are on page 1/ 4

ID: DATE:

Experiment No. 02

NAME OF THE EXPERIMENT:


STANDARDIZATION OF HYDROCHLORIC (HCl) ACID SOLUTION WITH STANDARD SODIUM
HYDROXIDE (NaOH) SOLUTION.

Theory
The process of adding base to an acid (or vice versa) to produce a salt and water is called neutralization. In
the neutralization of hydrochloric acid with sodium hydroxide, the reaction that occurs is:

HCl (aq) + NaOH (aq) NaCl + H2O…….. (1)

When an acid and a base are present in stoichiometric amount, for example one mole of sodium hydroxide
is added to one mole of hydrochloric acid as in the above neutralization process, this means that the
equivalent point has been reached in the acid-base system. Suitable indicators can be used to monitor the
end-point (the point at which an indicator changes color) of the titration.

Here, by measuring the volume of the NaOH solution required to react completely with a solution of a
weighed sample of HCl the exact concentration of HCl solution is determined.

Apparatus Reagents and Chemicals Indicator

1. Conical flask 1. Sodium hydroxide 1. Phenolphthalein


2. Pipette 2. Oxalic acid 2. Methyl Orange
3. Burette 3. Hydrochloric Acid
4. Beaker
5. Funnel
6. Volumetric flask
7. Electric balance
Procedure:

Step-I Standardize the supplied NaOH solution.


i) Follow the procedure as mentioned in the Experiment 01.

ii) Fill in the Table 01.

Step-II Standardize the supplied HCl solution with the NaOH solution

1. Take 10 mL HCl solution in a conical flask.


2. Add 1-2 drops of Methyl Orange indicator to the solution. Then add
previously prepared NaOH solution drop wise from a burette. Shaking the
flask frequently during addition of NaOH. Stop addition of NaOH solution
as soon as the red color of the solution just changes to yellow.
3. Note the burette reading in the Table 02.
4. Repeat the process at least three times and take the mean reading.
Calculate the strength of the supplied HCl solution.
Experimental Data:

Table01: Standardization of supplied NaOH solution by the prepared Oxalic Acid solution

No. of
observation Burette reading (Volume of NaOH)
Volume of
Oxalic acid Mean
solution, Final Difference (mL) (Vbase)
Vacid Initial (mL) (mL) (mL)

COOH COONa
2NaOH (aq) + | .2H2O (aq) | .2H2O (aq) + H2O

COOH COONa

Table 02: Standardization of HCl by NaOH solution


No. of
observation Volume of Burette reading (Volume of NaOH)
HCl acid
solution Initial Final Difference
(mL) Mean
(mL) (mL) (mL)
(mL)
1

3
Calculation:

Using the equation (01) of the reaction of this experiment we get,

𝑉𝑎𝑐𝑖𝑑 𝑥 𝑆𝐴𝑐𝑖𝑑 1 Here,


=
𝑉𝑏𝑎𝑠𝑒 𝑥 𝑆𝑏𝑎𝑠𝑒 1
𝑉𝑎𝑐𝑖𝑑 = ……….... mL

𝑉𝑏𝑎𝑠𝑒 𝑥 𝑆𝑏𝑎𝑠𝑒 𝑉𝑏𝑎𝑠𝑒 = …………. mL


Then, 𝑆𝑎𝑐𝑖𝑑 = 1 𝑥
𝑉𝑎𝑐𝑖𝑑 𝑆𝑏𝑎𝑠𝑒 = ……….. M

𝑆𝐴𝑐𝑖𝑑 = ? M
𝑆𝑎𝑐𝑖𝑑 = ………. M

Result: The strength of the supplied HCl solution is calculated as ……….. M

You might also like

pFad - Phonifier reborn

Pfad - The Proxy pFad of © 2024 Garber Painting. All rights reserved.

Note: This service is not intended for secure transactions such as banking, social media, email, or purchasing. Use at your own risk. We assume no liability whatsoever for broken pages.


Alternative Proxies:

Alternative Proxy

pFad Proxy

pFad v3 Proxy

pFad v4 Proxy