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Preparation 21

This document describes the preparation of a spirit. It defines a spirit as an alcoholic solution of volatile oils or aromatic substances with over 60% alcohol content. It provides details on the formulation, procedure, and storage requirements for making a Compound Orange Spirit, which is an alcoholic solution with the odor of orange containing between 25-30 mL of mixed essential oils in 100 mL of 65-70% alcohol. The active ingredients are mixed with alcohol, filtered, and filled into amber bottles for storage in a cool place.

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Khael
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100% found this document useful (1 vote)
2K views14 pages

Preparation 21

This document describes the preparation of a spirit. It defines a spirit as an alcoholic solution of volatile oils or aromatic substances with over 60% alcohol content. It provides details on the formulation, procedure, and storage requirements for making a Compound Orange Spirit, which is an alcoholic solution with the odor of orange containing between 25-30 mL of mixed essential oils in 100 mL of 65-70% alcohol. The active ingredients are mixed with alcohol, filtered, and filled into amber bottles for storage in a cool place.

Uploaded by

Khael
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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PREPARATION 21

SPIRIT

 Spirit
 A clear, saturated, alcoholic (over
60% alcoholic content) or
hydroalcoholic solution of volatile
oil or aromatic substances

By: Nelson T. Tubon


PREPARATION 21
SPIRIT

 Spirit
 The active ingredient in spirit like
aromatic water may be solid, liquid or gas
 Used internally for their medicinal value
 Flavoring agent
 Stored in tight light resistant container
and in a cool place, preventing
evaporation and volatilization of either the
alcohol or the active principles
By: Nelson T. Tubon
PREPARATION 21
SPIRIT

 PREPARATION
 Simple Solution
 65 mL volatile oil/1000 mL preparation
 Solution with Maceration
 macerates leaves in water to extract water
soluble components

By: Nelson T. Tubon


PREPARATION 21
SPIRIT

 PREPARATION
Distillation
 Brandy – fermented juice of ripe grapes
 Whisky – fermented mash of wholly germinated
malted cereal grain

NOTE:
Chemical Reaction
NaNO3 + C2H5OH + H2SO4  C2H5NO3 (Ethyl Nitrate Spirit)
+ Na2SO4 + H2O

By: Nelson T. Tubon


PREPARATION 21
COMPOUND ORANGE SPIRIT

 CATEGORY
Non-Medicated Spirit

By: Nelson T. Tubon


PREPARATION 21
COMPOUND ORANGE SPIRIT

 Synonym
 Spiritus Auranti Compositus

By: Nelson T. Tubon


PREPARATION 21
COMPOUND ORANGE SPIRIT

 Description of Final Product


 It is alcoholic solution with the odor of
orange
 between 65.0% - 70.0% of C2H5OH

By: Nelson T. Tubon


PREPARATION 21
COMPOUND ORANGE SPIRIT

 Use
 Flavoring agent

By: Nelson T. Tubon


PREPARATION 21
COMPOUND ORANGE SPIRIT

 Formulation
Ingredients OA CA

Orange Oil 200 mL


Lemon Oil 50 mL
Coriander Oil 20 mL
Anise Oil 5 mL
Alcohol, qs ad 1000 mL 30 mL

27.5 mL of mixed oils are present in the preparation. COS contains nlt
25 mL and nmt 30 mL of mixed oils in 100 mL of spirit. It contains 65%
to 70% alcohol

By: Nelson T. Tubon


PREPARATION 21
COMPOUND ORANGE SPIRIT

 Computations

By: Nelson T. Tubon


PREPARATION 21
COMPOUND ORANGE SPIRIT
21.75 mL
 Procedure
 Measure 21.75 mL alcohol
 Add orange oil, lemon oil, coriander
oil and anise oil, stirring after each
addition until the oil is mixed or
dissolved thoroughly

+ + + =

By: Nelson T. Tubon


PREPARATION 21
COMPOUND ORANGE SPIRIT

 Procedure
Filter until clear, add sufficient
amount of alcohol to make 30 mL

By: Nelson T. Tubon


PREPARATION 21
COMPOUND ORANGE SPIRIT

 Label
 White Label

 Container
 30 mL amber bottle

By: Nelson T. Tubon


PREPARATION 21
COMPOUND ORANGE SPIRIT

 Remarks
 Method of preparation  simple
solution method
 Container tight and light resistant
 Storage  cold place

By: Nelson T. Tubon

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