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Lab Report - Raman Spectos

1. The document discusses a laboratory demonstration report submitted by 6 students on material characterization of propane under various pressures and temperatures using Raman spectroscopy. 2. The experiment showed that propane can transform into different saturated and unsaturated hydrocarbons under high pressures and temperatures relevant to depths within the Earth. 3. The report is assessed based on its introduction, results, discussion, conclusion, format, and writing skills. The students are found to have clearly explained the various sections and demonstrated good communication skills in their written report.

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315 views5 pages

Lab Report - Raman Spectos

1. The document discusses a laboratory demonstration report submitted by 6 students on material characterization of propane under various pressures and temperatures using Raman spectroscopy. 2. The experiment showed that propane can transform into different saturated and unsaturated hydrocarbons under high pressures and temperatures relevant to depths within the Earth. 3. The report is assessed based on its introduction, results, discussion, conclusion, format, and writing skills. The students are found to have clearly explained the various sections and demonstrated good communication skills in their written report.

Uploaded by

tira
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd
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FACULTY OF MANUFACTURING ENGINEERING

BMFB 3723 MATERIAL CHARACTERIZATION

SEM II 2019/2020

3 BMFG 1

REPORT TITLE: A deep-learning technique for phase identification in


multiphase inorganic compounds using synthetic XRD powder patterns

LECTURER’S NAME: PM IR. DR. ASYADI AZAM BIN MOHD


ABID

NO NAME MATRICS NO
1. MUHAMMAD KHAIRANY AFFAN BIN B051710134
SAIMIN
2. MUHAMMAD SYAZWAN BIN SULAIMAN B051710127
3. NORMA SYAKILA BINTI ASOHA B051710156

4. NUR ATIRAH ASNA BINTI MOHAMAD RAUS B051710149


5. SHAHRIN HAKIMI BIN AHMAD B051710205

6. NOOR FATIN NABILAH BINTI ROSLEY B051710143

SUBMISSION DATE: 18 MARCH 2020

Introduction
Raman Spectroscopy is a non-destructive chemical analysis technique which
provides detailed information about chemical structure, phase and polymorphy,
crystallinity and molecular interactions. This study focusing on how the reactions of
propane, C₃H₈ in various of pressure and temperature by using Raman spectroscopy
to provide information on molecular vibrations and also crystal structures itself. The
range of pressures from 3 to 22 GPa and temperatures from 900 to 3000 K. We want
to know propane could react, leading to these three formations of hydrocarbons which
are in both saturated and unsaturated as well as soot.

Result
The experiment demonstrate that various pressures and temperatures conditions
are relevant for wide range of depth within the Earth pure propane can transform into
different hydrocarbons, both saturated and unsaturated. Under these circumstances,
propane is reacting using two simultaneous and competing pathways. The first
pathway is the growing of the hydrocarbon chain via the condensation or
polymerization mechanisms and the second one is the destruction via the cleavage of
C-C and C-H bonds. The observations suggest that propane, if subducted into mantle,
undergoes complex transformations.

Figures 1 : Chemical transformations of propane at 17 GPa and 22 GPa respectively

Discussion
The discussion will cover only the chemical transformations of pure propane at
the two highest pressures subjected which are at 17 GPa and 22 GPa. At 17 and 22
GPa, the Raman bands of hydrocarbons become less distinguished with the overlap of
the C-C bending area by graphite frequencies with the presence of unidentified C-H
vibrations of saturated hydrocarbons in the region of 3000 cm-1.

Conclusion
In summary, this study observed the transformations of the propane chemical
under the certain range of high pressures and temperatures by using Raman
Spectroscopy. Moreover, we have know that at the greater than 900 K temperatures,
propane looks to transform into the formation of complex hydrocarbon systems and
soot over the full range of pressures. Lastly, at the temperature of 1000 to 2000 K and
under pressures from 6 to 22 GPa, the results shown that the formation of heavier
alkanes from propane is possible without any presence of catalyst.
UNIVERSITI TEKNIKAL MALAYSIA MELAKA
FACULTY OF MANUFACTURING ENGINEERING
Hang Tuah Jaya, 76100 Durian Tunggal, Melaka.

Tel: +606-3316419 Fax: +606 331 6411

LABORATORY DEMONSTRATION
ASSESSMENT FORM

Subject Code BMFB 3723


Subject Name MATERIALS CHARACTERIZATION
Session/Semester 2 – 2019/2020
Name of Student (1)
Learning Outcomes Program Outcomes
Able to communicate effectively on complex
engineering activities with the engineering community
Display good communication skill on matters and with society at large, such as being able to
related to materials characterization in a written comprehend and write effective reports and design
report and presentation documentation, make effective presentation, and give
LO3 PO9
and receive clear instructions.

STUDENTS’ NAME LIST: MATRIX NO.

1. MUHAMMAD KHAIRANY AFFAN BIN SAIMIN B051710134

2. MUHAMMAD SYAZWAN BIN SULAIMAN B051710127

3. NORMA SYAKILA BINTI ASOHA B051710156

4. NUR ATIRAH ASNA BINTI MOHAMAD RAUS B051710149

5. SHAHRIN HAKIMI BIN AHMAD B051710205

6. NOOR FATIN NABILAH BINTI ROSLEY B051710143

Score Weightage Marks


INTRODUCTION
Clear and brief explanation on the introduction. 4
Acceptable explanation about the introduction. 3 3
Serious deficiencies in the explanation of introduction. 1
No introduction in the report. 0
RESULTS
Clear explanation of the results. 4
Acceptable explanation of the results. 3 4
Serious deficiencies in the results. 1
No result. 0
DISCUSSION
Clear explanation of the discussion. 4
Acceptable explanation of the discussion. 3 3
Serious deficiencies in the discussion. 1
No discussion. 0
CONCLUSION
Clear directions and wrap up connections to objectives. 5
Acceptable conclusion. 3 1
Serious deficiencies in the conclusion 1
No conclusion 0
REPORT FORMAT AND WRITING SKILLS

Report is well structured and follows standard format. Report is very


clear and sentences are easy to understand. Minor grammatical
5
errors.

Report is well written but occasionally some points are not easy to
understand. Some grammatical errors are present. Standard format is
3 1
used.

Report is not well written with many grammatical errors and/or


1
standard format is not followed.

TOTAL

50

-1-

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