Use of Fillers For Optimal Formulation of Self-Com PDF
Use of Fillers For Optimal Formulation of Self-Com PDF
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Abstract
The objective of this study is to achieve an optimal formulation of self-compacting concrete using local materials from
the country of Morocco, the use of this type of concrete remains very limited compared to a concrete vibrated in this
country, due to lack mastery by companies. We will therefore try to study an optimal formulation that respects European
standards and gives comparable results, even improved, to those of vibrated concrete, in order to be able to replace
vibrated concrete with self-compacting concrete in construction sites. Thus, SCC mixtures containing amounts of fillers
were examined, and with different Portland cement dosages: 350; 375 and 400 kg/m 3. The method of formulation is
made in accordance with French regulations. The results obtained were compared to these vibrated concrete counterparts
containing the same cement dosages. Tests include compression, traction and flexion tests at 3, 7 and 28 days of age.
Several studies have been carried out internationally, but at the national level, there is no study to this effect. The results
obtained show that there is an improvement in the strength of concrete, in addition to the liquid appearance of concrete. It
is this last aspect that characterizes the SCC, which allows it a flow in the areas inaccessible by the vibrator, thus saving
time and performance of the structure to achieve.
Keywords: Self-Compacting Concrete; Formuation; Fillers; Resistance.
1. Introduction
Self-consolidating concretes (SCCs), which have been developed over the past three decades by Japanese
researchers [1], are still referred to as "new concretes" because their use remains modest, although they have a high
potential for development. The specificity of SCC compared to traditional concretes lies in the fact that they are
extremely fluid and don’t require vibration to be implemented. Compacting under their own weight, they can be cast
in very scrapped areas or in areas of complex architecture and difficult to access [2].Their origin seems to stem from
the need to use materials that are more and more "efficient" to offset a reduction in the quality of constructions due to
a bad Placement of the material [3]. The use of a traditional concrete requires a vibration phase in order to properly fill
the formwork. This step determines the quality of the final structure, but it is also a laborious task that requires special
know-how. The solution proposed was to use a very fluid material capable of compacting under its own weight
without external vibration. One of the main advantages of the SCC is that it allows the production of high-quality
facings; also, it has an excellent deformability and high resistance to segregation [4-5]. SCCs are formulated
differently from ordinary concretes: they contain less gravel, more fine elements and fluidifiers. This is of course what
gives them an auto-compacting character. However, it is also likely that these results in a different mechanical
behavior compared to ordinary concretes.
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In this research, we will study mixtures of self-compacting concrete, at first we will try to find an optimal and
adequate formulation, and in a second time we will compare the mechanical tests of this formulation with those of an
ordinary concrete, more particularly the compressive strengths at the age of 3, 7 and 28 days. In the first step, the
research concerns the formulation; that is to say, find the dosage of the different components, namely, the gravel, the
sand, the cement, the fillers and the water. The mixtures studied are from MX1 to MX9, which are grouped by dosage
of Portland cement, the first group of MX1 to MX3, are dosed at 350 Kg/m 3, the second group of MX4 to MX6, are
dosed at 375 Kg/m3 and the third group from MX7 to MX9, are dosed at 400 Kg/m3. These mixtures are subject to
preliminary tests, namely the Abrams cone collapse test, the LBOX box flow test and the sieving stability test. These
tests are carried out according to European standards, and according to the results of these tests, we will discard
mixtures that do not meet the specifications of the standards. The mixtures that pass these tests will be subject to a
second measurement campaign, these are the tests of compressive and tensile strengths at different ages of 3, 7 and 28
days. In a second step, these self-compacting concrete mixtures with vibrated concrete counterparts will be compared
in terms of compressive strength. From these results, we can judge the use of self-healing concrete as an alternative of
vibrated concrete in Moroccan construction sites.
2.2.2. Homogeneity
Once the filling has been completed, the material must flow and pass through more or less dense frames. To realize
this property, various tests are available to highlight the capacity of a SCC to flow through reinforcement more or less
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dense. If the aggregates are blocked and arched at the reinforcement bars, the filling of the formwork will not be done
properly. The reference test to characterize this property is: L-box test [8].
It is possible to test the mobility of the concrete in a confined environment. During the test, the vertical part of a L-
shaped box is first filled. After one minute, the trap is lifted allowing the flow through three reinforcements. The final
filling rate H2 / H1 indicates the mobility of the concrete in a confined medium must be greater than 0.8 [2]. A bad
flow of the concrete through the reinforcement informs us of a problem of blocking or segregation.
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blockage. As a result, the quantity of suspending material is increased. But the quantity of sand contained in the
mortar should not be too great since this increases the flow resistance and viscosity. In the case of SCCs, the
maximum diameter of the aggregates is limited (on the order of 16 to 20 mm) [2].
Role of superplasticizers: superplasticizers are used widely to produce flowable, strong, and durable Portland
cement concretes and mortars [12]. The hydration behaviors of Portland cement in the presence of
superplasticizers have been investigated by a number of researchers [13-16]. It is thus possible to manufacture
very fluid concretes, even with less water than is necessary to hydrate the cement, and thus to make concretes
with a low Water / Cement ratio that are easy to install. The time of introduction of the superplasticizer during
kneading plays a role in the saturation dosage. If the introduction is delayed, the saturation dosage is lower; it is
obtained for a smaller quantity of superplasticizer. Thus, delaying its introduction allows the superplasticizer to be
more efficient and to obtain mixtures more fluid than if it had been introduced at the beginning of mixing.
Role of fines: Superplasticizers therefore make it possible to obtain very fluid concretes by reducing the friction
between cement grains and by releasing a certain quantity of water. Their use is not sufficient in the case of SCCs.
Interactions between larger grains must also be reduced. In order to increase the quantity of paste of a SCC, it is
then possible to envisage increasing the quantity of cement [17]. However, this would lead to a significant
increase in the cost of the material but also to problems of shrinkage due to the rise in temperature during the
hydration of the cement. It is therefore necessary to replace part of the cement with mineral additions. Different
additions are cited in the literature [18]: fly ash, blast furnace slag, silica fume and calcareous filler. These
materials can have a chemical influence and / or a physical role depending on their nature.
SCCs are formulated with a higher volume of paste and sand / gravel ratio than in vibrated concrete. Moreover, they
generally contain large quantities of adjuvants.
3. Experimental study
3.1. Materials
The materials used in this study come from the following quarries:
Gravette G1 and Grain de Riz from Oued CHERRAT/Morocco of limestone nature;
Crushed sand from the quarry Ouled ABBOU/Morocco of dolomite nature (SC);
Sand dune from the town of KENITRA/Morocco of siliceous nature (SM);
Mixing water is the drinking water of the network.
The different aggregates were subjected to a laboratory characterization; Table 1. summarizes the results. Figure 4.
schematizes the curves of the particle size analysis performed on the concrete formulation materials. There is clearly
continuity between the three curves, in other words an overlap zone between these curves, and subsequently the matrix
contains the various dimensions from the finest to the largest elements, therefore a texture of the concrete and a
consistent appearance.
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Thus, it is deduced that the best mixture of rheological behavior of a SCC is that obtained from a mixture MX2
comprising approximately 100 kg of calcareous fines. This conclusion was verified for the other cement measurements.
B) Skeletal optimization
The formulation of the SCCs is also based on an optimization of the granular skeleton. Thus, one of the most
important parameters to study was the Gravette / Aggregate Total (G / GT) ratio or the Gravette/Sand (G / S) ratio.
Table 5. presents the different experiments carried out.
Table 6. Optimization of the granular skeleton
Reports studied Phenomenon observed Preliminary Findings Continuation of the study
Spreading : D=650 mm Difficulty of the concrete
G/GT= 0.50 L-BOX : H2 / H1 = 0.3 to pass between the Reduce G / GT Report
Sieve stability : 8% reinforcements
Spreading : D =710 mm
Good appearance of fresh
G/GT =0.48 L-BOX : H2/H1=0.8 Reduce again G / GT
concrete
Sieve stability : 12%
Spreading : D=700 mm
Good appearance of fresh
G/GT=0.45 LBOX : H2/H1=0.8 Reduce again G / GT
concrete
Sieve stability : 12%
Spreading : D =610 mm
The aggregates appear to
G/GT=0.42 Vault formation at armature level Limit G / GT to 0.45
be trapped in the paste
Paste too viscous
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It is then noted that the different results show that the concrete studied exhibits rheological characteristics
conforming for a self-compacting concrete with the exception of concrete MX5.
B) Tests on hardened SCC
Figures 5 and 6. show the evolution of the compressive strength and the tensile strength of the different mixtures
studied. As regards Figure 5, the various mixtures studied, namely MX1 up to MX6, are represented along the x-axis,
and along the y-axis are represented the values of the compressive strengths at the age of 3, 7 and 28 days. According to
this figure, the minimum values of compressive strengths correspond to the MX1 mixture, which are 22, 30 and 43 MPa
for the three ages, while the maximum values are those found for the MX6 mixture, which are 30, 39 and 56 MPa for
the three ages. For Figure 6, the studied mixtures are shown along the x-axis and the results of the tensile strengths at 28
days of age are shown along the y-axis. According to this graph, the maximum resistance is recorded for the mixture
MX6 and which is worth 3.6 MPa, while the minimum resistance is recorded for the mixture MX3 and which is worth
5.0 MPa. The tests are carried out in accordance with the current standards [26-27].
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0
MX1 MX2 MX3 MX4 MX5 MX6
Mixtures
Figure 5. Compressive strength at the age of 3, 7 and 28 days for different SCC mixtures
Figure 6. Tensile strength at the age of 28 days for the various mixtures
It is then noted that the compressive strength of the studied mixtures greatly exceed those required by a class B1
concrete in accordance with standard NM 10.1.008 [28] and in all cases exceed 40 MPa. It is also noted that the
concretes having a ratio G / GT = 0.48 give slightly higher compressive strengths. The compressive and tensile strength
results give values similar to those published by other research carried out on self-placing concrete [29-31].
3.3.2. Test on Vibrated Concrete
In order to compare this type of concrete with traditional concretes, we studied three types of vibrated concrete
(VC), measured at 350, 375 and 400 kg/m3. In the fresh state, the VC has a slump of 4 cm. Table 8. shows the mixtures
adopted for VC.
Table 9. Formulation of vibrated concrete
Type of mixture VC1 VC2 VC3
Figures 7, 8 and 9. show the results of the compression resistances obtained by the two concretes VC and SCC.
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70
60
40
MX3
30
MX4
20 VC
10
0
3 days 7 days 28 days
Figure 7. Comparison of compressive strength between SCC and VC for dosing of 350 Kg/m3
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Compressive Strength (MPa)
60
50
40 MX5
30 MX6
20 VC
10
0
3 days 7 days 28 days
Test Age (days)
Figure 8. Comparison of compressive strength between SCC and VC for dosing of 375 Kg/m3
60
Compressive Strength (MPa)
50
40
MX1
30
MX2
20
VC
10
0
3 days 7 days 28 days
Test Age (days)
Figure 9. Comparison of compressive strength between SCC and VC for dosing of 400 Kg/m3
Figures 7, 8 and 9. attempt to compare the compression tests at the age of 3, 7 and 28 days of SCC mixtures with
those of VC. First, Figure 7. shows the formulations studied with a Portland cement dosage of 350 kg/m3, it is mixtures
MX1 and MX2 for SCC and VC1 for vibrated concrete. According to this figure, there is an improvement of this
resistance, which reaches 10% for MX1 and 18% for MX2. Secondly, Figure 8. shows this comparison for a Portland
cement dosage of 375 kg/m3. The mixtures relate to MX3 and MX4 for SCC and VC2 for vibrated concrete. There is an
improvement of the resistance of SCC compared to VC; this evolution of resistance reaches 20% for MX3 and 16% for
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MX4. Finally, Figure 9. also shows an improvement in the resistance of MX5 and MX6 with respect to VC3. The
dosage adopted is 400 kg/m3 of Portland cement, the increase reaches 8% for MX5 and 10% for MX6. The results
obtained make it possible to conclude that the compressive strengths of the vibrated concretes are lower than the
resistances of the self-compacting concretes.
4. Conclusions
The experimental study led to a first overview of the various parameters having a direct or indirect impact on the
different characteristics of the SCCs. In this context, it is important to note the following findings:
At the material level, the experiment showed that it is quite possible to produce self-compacting concretes from
fired crusher sands.
With these materials, the dosages of fine elements (Cement + fine elements from crushing sand) are between
450 and 500 kg/m3 with a G / GT ratio of between 0.45 and 0.48.
The tested formulations resulted in a self-compacting concrete with the following characteristics:
- A spreading between 610 and 715mm;
- An H2 / H1 coefficient at the L-Box between 0.7 and 0.9;
- A Sieve Stability Coefficient of between 9 and 12.5%;
The compressive and tensile strengths far exceed the characteristic resistances of a Type B1 concrete in the
sense of Moroccan Standard NM 10.1.008. They also exceed the resistances obtained by a control vibrated
concrete.
5. References
[1] Ozawa K., Maekawa K., Kunishima M. and Okamura H. “Performance of Concrete Based on the Durability Design of Concrete
Structures”. Proceedings of the Second East Asia-Pacific Conf Structural Engineering and Construction, Chiang Mai, Thailand
(1989).
[2] EFNARC. “The European Guidelines for Self-Compacting Concrete” (2002).
[3] Agustin, P. Hugas. “Mix Proportion and Properties of Self-Compacting Concrete, Report TVBM-5041, Division of building
Materials, Lund Institute of Technology” (1999).
[4] Aslani Farhad. and Nejadi Shami. “Mechanical Properties of Conventional and Self-Compacting Concrete: An Analytical
Study.” Construction and Building Materials 36 (2012): 330–347. doi: 10.1016/j.conbuildmat.2012.04.034.
[5] Shindoh T., Yokota K. and Yokoi K. “Effect of Mix Constituents on Rheological Properties of Super Workable Concrete.”
Proceedings of the International RILEM conf, Production Methods and Workability of Concrete, Paisely, Scotland (1996).
[6] Yazicioglu S., Caliskan S., & Turk K. “Effect of Curing on the Engineering Properties of Self-Concrete.” Indian Journal of
Engineering & Materials Sciences 13 (2006): 25-29.
[7] EN 12350-8. “Self Compacting Concrete. Part 8 – Slump Flow Test, European Standard” ( 2010).
[8] EN 12350-10. “Self Compacting Concrete. Part 10 – L Box test, European Standard” (2010).
[9] Dreux G., Gorisse F. and Simonnet J. “Composition des Bétons : Méthode Dreux-Gorisse, Annales de l’Institut Technique du
Batiment et des Travaux Publics, France” (1983).
[10] Nagamoto N. and Ozawa K. “Mixture properties of Self-Compacting, High-Performance Concrete.” Proceedings of Third
CANMET/ACI International Conferences on Design and Materials and Recent Advances in Concrete Technology, SP-172, V. M.
Malhotra, American Concrete Institute, Farmington Hills, Mich (1997).
[11] Khayat K.H. and Ghezal A. “Utility of Statistical models in Proportioning Self-Compacting Concrete.” Proceedings, RILEM
International symposium on Self-Compacting Concrete, Stockholm (1999).
[12] Shi Chen, He Ting-shu, Zhang Ge, Wang Xi and Hu Yanyan. “Effects of Superplasticizers on Carbonation Resistance of
Concrete.” Construction and Building Materials 108 (2016): 48–55. doi : 10.1016/j.conbuildmat.2016.01.037.
[13] Yamada Kazuo, Takahashi Tomoo, Hanehara Shunsuke and Matsuhisa Matsuhisa. “Effects of the Chemical Structure on the
Properties of Polycarboxylate-Type Superplasticizer.” Cement & Concrete Researsh, 30 (2000): 197–207. doi: 10.1016/S0008-
8846(99)00230-6.
[14] Kreppelt Fritz, Weibel Martin, Zampini Davide and Romer Micheal. “Influence of solution chemistry on the hydration of
polished clinker surfaces—a Study of Different Types of Polycarboxylic Acid-Based Admixtures.” Cement & Concrete Researsh
32 (2002): 187–198. doi: 10.1016/S0008-8846(01)00654-8.
[15] Carazeanu Ionela, Chirila Elisabita and Georgescu Maria. “Investigation of the Hydration Process in 3CaO–Al2O3–CaSO4–
2H2O–Plasticizer–H2O Systems by X-ray Diffraction.” Talanta 57 (2002): 617–623. doi: 10.1016/S0039-9140(02)00100-5.
[16] Yu Yinhui, Liu Jiaping, Ran Qianping, Qiao Min and Zhou Dongliang. “Current Understanding of Comb-Like Copolymer
76
Civil Engineering Journal Vol. 4, No. 1, January, 2018
Dispersants Impact on the Hydration Characteristics of C3A–Gypsum Suspension.” J. Therm. Anal. Calorim. 111 (2013): 437–444.
doi: 10.1007/s10973-012-2430-3.
[17] Felekoglu Burak. “A comparative Study on the Performance of Sands Rich and Poor in Fines in Self-Compacting Concrete.”
J. Cons.Bui. Mat. 22 (2008): 646–654. doi: 10.1016/j.conbuildmat.2006.10.007.
[18] Aggarwal P., Siddique R., Aggarwal Y. and Gupta S.M. “Self-Compacting Concrete - Procedure for Mix Design.” Leonardo
Electronic Journal of Practices and Technologies 12 (2008): 15-24.
[19] NM 10.1.700. “Essais pour Déterminer les Caractéristiques Géométriques des Granulats - Détermination de la Granularité -
Analyse granulométrique par Tamisage, Morrocan Standards” (2008).
[20] NM 10.1.155. “Granulats - Mesure du coefficient d'aplatissement, Morrocan Standards » (1995).
[21] NM 10.1.146. “Granulats-Mesure des Masses Spécifiques de la Porosité du Poefficient d'Absorption de la Teneur en Eau des
Gravillons et Cailloux, Morrocan Standards (1995).
[22] NM 10.1.149. “Granulats-Mesure des Masses Spécifiques, Coefficient d'Absorption et Teneur en Eau des Sables, Morrocan
Standards” (1995).
[23] NM 10.1.169, “Granulats-Détermination de la Propreté Puperficielle, Morrocan Standards” (1995).
[24] NM 10.1.147. “Granulats - Equivalent de Sable, Morrocan Standards” (1995).
[25] NM 10.1.138. “Granulats - Essai Los Angeles, Morrocan Standards” (1995).
[26] EN 12390-3. “Testing Harderned Concrete. Part 3 – Compressive Strength of Test Specimens, European Standards” (2002).
[27] EN 12390-5. “Testing harderned concrete. Part 5 – Flexural Strength of test Specimens, European Standards” (2002).
[28] NM 10.1.008. “Béton : Spécifications, Performances, Production et Conformité, Morrocan Standards” (2007).
[29] Ravinder Kaur Sandhu and Rafat Siddique. “Influence of rice husk ash (RHA) on the properties of self-compacting concrete:
A review.” J. Cons.Bui. Mat. 153 (2017): 751–764. doi.org/10.1016/j.conbuildmat.2017.07.165.
[30] Stefania Manzi, Claudio Mazzotti and Maria Chiara Bignozzi. “Self-compacting concrete with recycled concrete aggregate:
Study of the long-term properties.” J. Cons.Bui. Mat. 157 (2017): 582–590. doi.org/10.1016/j.conbuildmat.2017.09.129.
[31] Miguel C.S. Nepomuceno, L.A. Pereira-de-Oliveira and S.M.R. Lopes. “Methodology for the mix design of self-compacting
concrete using different mineral additions in binary blends of powders.” J. Cons.Bui. Mat. 64 (2014): 82–94.
doi.org/10.1016/j.conbuildmat.2014.04.021.
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