Sallybus 2020-24
Sallybus 2020-24
First Year
1st SEMESTER
Note:
NSS/NCC/Sports proficiency/Community services/Professional society activities/Technical activities
related to the field of Engineering (1st to 3rd year, 2 credits to be earned in 7th semester)
Discipline (1st to 4th year, 1 credit to be earned in 8th semester)
2nd SEMESTER
Note:
NSS/NCC/Sports proficiency/Community services/Professional society activities/Technical activities
related to the field of Engineering (1st to 3rd year, 2 credits to be earned in 7th semester)
Discipline (1st to 4th year, 1 credit to be earned in 8th semester)
2ndYear
3rdSEMESTER
Note:
NSS/NCC/Sports proficiency/Community services/Professional society activities/Technical activities
related to the field of Engineering (1st to 3rd year, 2 credits to be earned in 7th semester)
Discipline (1st to 4th year, 1 credit to be earned in 8th semester)
2ndYear
4thSEMESTER
Note:
NSS/NCC/Sports proficiency/Community services/Professional society activities/Technical activities
related to the field of Engineering (1st to 3rd year, 2 credits to be earned in 7th semester)
Discipline (1st to 4th year, 1 credit to be earned in 8th semester)
3rdYear
5thSEMESTER
Note:
NSS/NCC/Sports proficiency/Community services/Professional society activities/Technical activities
related to the field of Engineering (1st to 3rd year, 2 credits to be earned in 7th semester)
Discipline (1st to 4th year, 1 credit to be earned in 8th semester)
3rdYear
6thSEMESTER
Note:
NSS/NCC/Sports proficiency/Community services/Professional society activities/Technical activities
related to the field of Engineering (1st to 3rd year, 2 credits to be earned in 7th semester)
Discipline (1st to 4th year, 1 credit to be earned in 8th semester)
* There will be 6-8 weeks’ compulsory industrial training after 6th semester theory
examination during summer vacation. Every students will submit the Industrial
Training report within one month from the start of teaching of the 7th semester.
After that it will be evaluated by the team of Training & Placement Officer.
The Credits for the Industrial Training will be awarded in the seventh semester
7
4thYear
7thSEMESTER
Note:
NSS/NCC/Sports proficiency/Community services/Professional society activities/Technical activities
related to the field of Engineering (1st to 3rd year, 2 credits to be earned in 7th semester)
Discipline (1st to 4th year, 1 credit to be earned in 8th semester)
** Marks and Credits for Project work will be awarded in 8th Semester
8
4thYear
8thSEMESTER
Note:
Discipline (1st to 4th year, 1 credit to be earned in 8th semester)
Note:
1. Mid term evaluation shall be as per the format already approved by the competent authority
(as indicated in the scheme already approved for the first year)
2. Departmental electives (I, II and III) shall be offered amongst the list indicated above
depending on the available resources.
3. Open electives (I, II and III) shall be offered amongst the list indicated above depending on the
available resources.
4. List of electives (open and departmental) is subject to change and as approval of the
competent authority from time to time.
10
Fibre Optics: Introduction, optical fibre as a dielectric wave guide: total internal reflection,
numerical aperture and various fibre parameters, losses associated with optical fibres, step
and graded index fibres, application of optical fibres.
Lasers: Introduction to interaction of radiation with matter, principles and working of laser:
population inversion, pumping, various modes, threshold population inversion, types of laser:
solid state, semiconductor, gas; application of lasers.
2. Structural Characterization: (16 hours+5T)
Crystal Lattice, points groups, Bravais lattices, crystal systems, X ray diffraction Symmetry
X-ray generation, Bragg Law, factors influencing intensity, Techniques, Indexing, precise
lattice parameter determination, residual stress measurement
SECTION B
3. Electromagnetism and Magnetic Properties of Materials (17L + 6T)
Dielectric Materials: Review of basic formulas, dielectric constant and polarizability,
sources of polarizability, classical treatment of dipolar, ionic and electronic polarizability,
piezoelectricity, ferroelectrcity. (4)
Magnetic Materials: Review of basic formulas, magnetic susceptibility, classification of
materials, Langevin diamagnetism, paramagnetism (only classical treatment), magnetism in
metals, ferromagnetism in insulators, anti-ferromagnetism and ferrimagnetism,
ferromagnetism in metals, ferromagnetic domains, hysteresis (8)
Superconductivity: Zero resistance, occurrence of superconductivity, Meissner effect,
critical field, thermodynamics of superconducting transitions, electrodynamics of
superconductors, qualitative idea of BCS theory. (3)
Nanotechnology: Nanomaterials and its applications, chemical and physical synthesis
techniques of nano-powder and thin films. (2)
12
Text Books 1. Introduction to Solid State Physics: Charles Kittle 8th Ed.
SECTION B
Chemical Bonding and structure Part II:LigandSubstitution reactions in complexes with
coordination numbers 4 and 6 and their mechanism . Kinetic aspects of substitution in coordination
13
PRACTICAL
Objectives Objectives of the Engineering Drawing course are:
1. To introduce the students to visual science in the form of technical graphics.
2. To give general instructions related to Theory of Orthographic Projection of
points, lines, planes and solids as per the BIS codes prevalent to drawing
practices.
3. To upgrade the basic understanding and visualization of geometric objects
and machine parts by introducing the students to section of solids,
intersection and development of surfaces, isometric projection and
orthographic projection of simple solids/blocks.
15
1. To find the energy band gap of the given semiconductor by four probe method.
2. To study the Hall Effect of a given semiconductor
3. To determine the dielectric constant of the given materials.
4. To study the B-H curve of the ferromagnetic materials.
5. To determine the value of e/m for electron by long solenoid (helical) method.
6. To study the variation of magnetic field with distance along the axis of a circular coil carrying
current by plotting a graph
7. To determine the velocity of ultrasonics waves in a given liquid.
8. To determine the frequency of A.C. mains using a sonometer and an electro-magnet.
9. To find the capacitance of a capacitor using flashing and quenching of a neon lamp.
10. To plot graph between current and frequency in a series LCR circuit and to find the resonant
frequency.
11. To find the wavelength of sodium light using Fresnel’s biprism.(3)
12. (i) To determine the wavelength of He-Ne laser using transmission grating.
(ii) To determine the slit width using the diffraction pattern.
13. To determine the wave length of sodium light by Newton’s rings method.
14. To determine the wave length of sodium light using a diffraction grating.
15. To find the specific rotation of sugar solution using a Bi-quartz Polarimeter.
16. To design a hollow prism and used it find the refractive index of a given liquid
17. To synthesize the nanoparticles by chemical methods and structural characterization through
X-ray diffraction.
18. To investigate the optical band gap of nanomaterial using UV-vis spectroscopy.
19. Fabrication of thin films by spray pyrolysis technique.
20. Fabrication of thin films using spin coater technique.
Text Books 1. Practical Physics by CL Arora, S Chand & Co.
2. Engineering physics by S.K. Srivastva
Reference Books A text book of practical physics by William & Watson
Course Assessment One *project out of 6 carries 40% marks, 20% for respective viva and 20% for
Methods external exams and 10% for attendance.
Text Book: Vogel’s Qualitative Inorganic Analysis, 7th Ed. By G. Svehla, Pearson Education.
Course Outcomes
The student will be able to
1. apply the concept of normality, molarity and oxidation and reduction and apply redox
titrations involving potassium dichromate and Iodine
2. use Complexometric Titrations to determine metal ions by EDTA method.
3. use gravimetric procedures for estimation (Estimate Ba+2/SO4 -2, and Fe+3)
2nd SEMESTER
differential equations.
5. evaluate complex integrals and apply these to various problems.
Synthetic utility of diazonium salts, synthetic utility of Grignard reagents and alkyllithiumsk, basicity
of amines, multistep synthesis. 05hrs
Books Recommended:
1. Bahl, B. S. &Bahl, Arun : Text-book of Organic Chemistry, 16th Edition, S. Chand and
Company Ltd., New Delhi.
2. Solomons, T. W. G. : Fundamentals of Organic Chemistry, John Wiley and Sons, Inc., New
York, 1994.
3. Morrison &Boyd : Organic Chemistry, Pearson education, 6th edition, 2007.
4. F.A.Carey: Organic Chemistry, Tata McGraw Hill, 7th edition, 2008.
5. Mukherji& Singh: Reaction mechanism in organic chemistry, Macmillan India Ltd.,
electrical machines.
To make them aware of the difference between analog and digital system
and study diodes, rectifiers, digital circuits.
Note for The semester question paper of the subject will be of 50 marks having 8 questions of
examiner equal marks. The paper will be divided into two parts having four questions each
from Section A and Section B. The candidate is required to attempt total 5 questions
selecting atleast two questions from each Section. The duration of End Term exam
will be 3 hrs.
SECTION A
DC Circuits and Single Phase A.C. Fundamentals
General introduction to Electrical Engineering, Kirchoff’sLaws ,Mesh and Node analysis,
Superposition theorem , Thevenin Theorem, Norton Theorem, Maximum power transfer theorem.
Generation of alternating voltages and currents, Equations for AC quantities, cycle, time period,
frequency, amplitude, calculation of R.M.S values, Average values for different waveforms, solution
and phasor diagram of single phase AC circuit with sinusoidal source of excitation, series and
parallel combination of R-L-C circuits.
Three Phase AC Fundamentals
Disadvantages of single phase system, star and delta connection in three phase circuits, relation
between line and phasor quantities, power in three phase system, solution of three phase balanced
circuits, power and power factor measurement by two wattmeter method.
Electrical Machines
Basic principle and construction of transformers, E.M.F equation, approximate equivalent circuit,
phasor diagram, losses, efficiency and condition for maximum efficiency, open circuit and short
circuit test on single phase transformers. Operating principle and construction of three phase
induction motors, Operating principle and construction of DC Machines, types of DC Machine &
E.M.F equations
SECTION B
Semiconductor Diodes and Transistors
General introduction to Electronics.Concept of stiff Voltage and Current Source. PN Junction,
Depletion layer, Barrier Potential, Forward and Reverse Bias, Breakdown voltage, V-I
characteristics, Half wave and full wave rectifiers, Zener diode. Introduction to junction transistors,
Transistor amplifying action, CB, CE, CC-configuration characteristics.
Digital Electronics
Binary and Hexadecimal number system, conversion of numbers from one system to other, OR,
Relations: Commutative, Associative and Distributive Laws. Concept of flip-flops, RS,JK flip flops,
shift register.
Text Books 1. Edward Hughes: Electrical and Electronic Technology, Pearson Education
Publication, Asia, 2003.
2. Nagsarkar, T.K. and Sukhija M.S.: Basic Electrical Engg., Oxford University
Press, 2004.
3. Bhargava: Basic electronics and Linear circuits, Tata McGraw Hill.
Reference 1. Nagrath, I.J. and Kothari, D.P.: Basic Electrical Engg., TMH, New Delhi.
Books 2. Malvino: Digital Principles and Applications, Tata McGraw Hill
Course 1. The student will understand how various loads are connected in circuits
Outcomes and difference between single and three phase system.
2. The students will know the principles and working of different types of
electrical machines used in industry
3. The students will have the basic knowledge of digitalization and
conversion of physical quantity to digital quantity.
21
Material Balances for Reacting systems including balances involving recycle and purge streams.
Combustion Calculations.
Energy balances on nonreactive and reactive systems.
Books Recommended:
1. Bhatt, V. I. & Vora, S. M. : Stiochiometry, 3rd Edition, Tata McGraw Hill, 1984.
2. Himmelbleau, D. M. : Basic Principles and Calculations in Chemical
Engineering, 6th Edition, Prentice Hall, 1977.
3. Felder, R. M. & Rousseau R.W. : Elementary Principles of Chemical Processes, 3rd
Edition, John Wiley and Sons, 1986.
4. Reklaithis, G. V. : Introduction of Material and Energy balances, John
Wiley, 1983.
5. Lubyben, L.W. & Winzel, L. A. : Chemical Process Analysis, 2nd Edition, Prentice
Hall, 1988.
experiments.
1. Overview of the equipments, instruments and procedure to be used, safety precautions and
report writing.
2. To study resonance in R-L-C series and parallel circuit.
3. Measurement of power and power factor by three voltmeter method.
4. Measurement of power and power factor by three ammeter method.
5. To measure power and power factor using a single wattmeter in a single phase circuit.
6. Measurement of power and power factor of three phase balanced load by two wattmeter
method.
7. To perform open circuit test and short circuit test on a single phase transformer and
draw equivalent circuit.
8. To obtain magnetization characteristics of DC Machine
9. Study the forward and reverse biased diode characteristics.
10. Study the CB, CE, CC transistor characteristics.
11. To obtain the waveforms of half wave rectifier circuit on CRO.
12. To obtain the waveforms of full wave rectifier circuit on CRO.
13. Verification of basic and universal gates.
14. To verify the thevenin theorem, nortan theorem, Maximum power transfer theorem
Course Outcomes Students will
have hands on knowledge about the design, purpose and working of R-
L-C and parallel circuits
become confident in taking accurate readings of voltmeter, ammeter
and wattmeter
have in depth knowledge about transformers, transistors , diodes and
rectifiers and will be able to understand their applications in industry.
have knowledge about networking theorems and their utility in
industry.
Course outcomes :
List steps for identifying simple organic compounds
Use different analytical procedures
SECTION B
Atkins, P.W & Paula, J.D. Physical Chemistry, 10th Ed., Oxford University Press(2014).
Barrow, G. M., Physical Chemistry 5th Ed., Tata McGraw Hill: New Delhi (2006).
Silbey, R. J.; Alberty, R. A. &Bawendi, M. G. Physical Chemistry 4th Ed., JohnWiley & Sons, Inc.
(2005).
1. Mc Cabe, W.L. and Smith, J.C. : Unit Operation of Chemical Engineering, McGraw Hill.
2. Fox, R.W. and McDonald, A.T. : Introduction of Fluid Mechanics (SI Version) 4th ed. John
Wiley and Sons, 1996.
3. Coulson, J.M. and Richardson, J.F. : Chemical Engineering, Vol. I, Pergamon
4. Foust, A.S., Wensel, L.A., Clump, : Principles of Unit Operations, John Wiley.
C.W., Maus, L. and Anderson, L.
5. Badger, W.L. and Banchero, J.T. : Introduction to Chemical Engineering, Tata McGraw Hill
Pub. Co. Ltd., 1997.
6. Chattopadhya, P. : Unit Operations of Chemical Engineering, Vol. I, Khanna
Publishers, Delhi, 1997.
27
THEORY
Note for the The question paper should be divided into Section A and Section B Total of 8
Examiner questions. 4 questions from section A and 4 questions from section B are to be set.
The students will be required to attempt 5 questions selecting at least 2 from each
section.
SECTION- A
Fuels: Types of conventional fuels, their merits and demerits. Non-conventional/renewable energy
sources, their importance for sustainable development and environmental protection.
Solid Fuels: Origin of coal, proximate and ultimate analysis of coal, coal preparation and washing
methods, safe storage of coal. Low and High temperature carbonization, products of carbonization, By
product coke ovens. Synthetics fuels from coal –Bergius process and Fischer Tropsch process.
Liquid fuels: Origin of petroleum, refining and distillation of crude oil, uses of petroleum products.
Gaseous fuels: Natural gas, manufacture of water gas and producer gas, gas cleaning methods.
SECTION- B
Principles of combustion: Combustion calculations, waste heat utilization.
Furnaces: Classification of furnaces, draught, furnace atmosphere, Portland cement continuous rotary
kiln, blast furnace, glass melting furnace
Alternate sources of energy:
Introduction to solar radiation and evaluation of radiation incident on a solar collector.
Applications of solar thermal energy such as solar water heater, solar cooker, solar concentrators
and solar thermal power generation.
Types of solar photovoltaic systems and applications.
Photosynthesis and biomass conversion systems.
Wind Energy: Nature of wind and wind turbine performance.
Other renewable energy sources such as geothermal, tidal, ocean and wave.
Recommended Books
1. Gupta, O.P. : Elements of Fuels, Furnaces & Refractions, 5th Edition, Khanna Publishers,
2007.
2. Rao, S. and : Energy Technology – Non-conventional, Renewable & Conventional, 3
Parulekar, B.B. Edition, Khanna Publishers, 2007.
3. Dayal, M. : Renewable Energy – Environment and Development, Konark Publishers
Pvt. Ltd., 1989.
4. Sukhatme, S.P. : Solar Energy – Principles of Thermal Collection and Storage, 2nd Edition, Tata
McGraw – Hill Publishing Company Ltd., 2006.
5. Sharma, S.P. and : Fuels and Combustion, Tata Mc-Graw Hill Publishing Company Ltd.,
Mohan, C. 1984.
Hours
SECTION- A
Stresses and Strains: Concept of simple stress and simple strain, mechanical properties of solids, types
of load, Tensile stress , compressive stress, shear stress, complementary shear stress, thermal stresses,
tensile test , stress strain curve , Hooke’s law, modulus of elasticity, modulus of rigidity, Principle of St.
Venant strain, factor of safety, compound bars, , Compound Stresses and Compound Strains in two-
dimensional stress system , Stresses on oblique plane due to pure shear, principle planes and principle
stresses, maximum shear stress, Mohr’s circle of stress, Poisson’s ratio, volumetric strain, elastic
constants and relations between them.
Shearing Force and Bending Moments in Beams: Shearing force, bending moment, types of beams,
types of load on beams, types of supports, sign- conventions for shearing force and bending moment,
point of inflection , relations between bending moment and shearing force shearing force and bending
moment diagrams for beam under different loads. Concentrated loads, uniformly distributed loads,
numerical problems.
Bending Stresses and Shearing Stresses in Beams: Pure bending, graphical determination of moments
of inertia, bending stress, composite beams, reinforced concrete beams, General eccentric loading,
combined direct and bending stresses, eccentric longitudinal loads , Shear stress distribution in
rectangular section and circular section, numerical problems.
Deflection of Beam:Introduction, Macauly’s integration method, simply supported beam with load at
mid span and beam with eccentric load, moment area method, deflection due to shear, numerical
problems.
SECTION-B
Torsion of Shafts: Torsion of thin circular shaft, composite shaft, combined bending and torsion.
equivalent torque, equivalent bending moment, numerical problems.
Struts and Columns:Definition of strut and column, Euler’s Column theory and assumptions made,
Strut with both ends pinned, strut with one end fixed and one end free, strut with both ends free,
Slenderness ratio, limitations of Euler theory, Rankine’s Empirical formula, strut with eccentric loading,
numerical problems.
Stresses and Strains in Thin Shells:Thin cylinder under internal pressure, thin spherical shell under
internal pressure, volumetric strain, modifications for built-up shells, numerical problems.
Stresses and Strains in Springs: Types of Springs, stresses in Close coiled helical springs, open coiled
helical springs, leaf springs, springs in parallel and in series, numerical problems.
Strain Energy and Theories of Elastic Failure: Strain energy and resilience, Strain energy in tension and
compression due to suddenly applied load and impact loads, strain energy due to shear, strain energy
due to bending, strain energy due to torsion, theories of elastic failure and their graphical
representation, numerical problems.
Books Recommended:
1. Ryder, G. H. : Strength of Materials, 3rd Edition S.I. Units Macmillan,
1969.
2. Bedi, D. S. : Strength of Materials, 6th Edition Khana Book
Publishing Co. (P)Ltd.
29
Books Recommended:
1. Lavitt, B.P. : Findlay’s Practical Physical Chemistry, Longman Group
Ltd.
1. General study of pipe fittings, valves and other equipments in the unit operations laboratory.
2. Pressure drop for flow through pipelines, valves & fittings.
3. Characteristics of pumps.
4. Flow measurement by the use of orifice meter, venturimeter, rotameter & pitot tube.
5. Flow over weirs and notches.
6. Flow measurement of compressible fluids.
31
Convection:Free and forced convection, concept of heat transfer co-efficient, dimensionless numbers
in free and forced convection, Dimensional analysis, Determination of Heat transfer coefficient using
heat and momentum transfer analogies, experimental determination of heat transfer coefficient and
common working correlations.
Radiation Heat Transfer: Black Body radiation, and grey body radiation, physical mechanism,
radiation properties and shape factor, heat exchange between non-black bodies, radiation shields
pyrometry and effect of radiation on temperature measurement
SECTION- B
Condensation and Boiling: Condensation heat transfer phenomenon, film condensation on vertical
plates and cylinders as well as on horizontal cylinders. Effects of non-condensable gases and vapor
velocity on condensation, pool boiling, forced convection boiling, working correlations for pool
boiling.
Evaporation: Types of Evaporators, single and multiple effects, single and multiple effects
calculations, evaporator capacity, economy, effect of liquid head and boiling point elevation, methods
of feeding.
Heat Exchangers: Various types of heat exchangers, overall heat transfer coefficients, heat
exchanger mean temperature differences, heat exchanger effectiveness and the number of transfer
units.
Books Recommended:
1. Mc Cabe, W.L., Smith, J.C. : Unit Operations of Chemical Engineering McGraw Hill.
2. Holman, J.P. : Heat Transfer, McGraw Hill Book Co.
3. Mc Adams, W.H. : Heat Transmission, McGraw Hill Book Co.
4. Chapmann, A.J. : Heat Transfer, Mc Millan Publishing Co.
5. Kern, D.Q. : Process heat Transfer, McGraw Hill Book Co.
6. Kreith, F. : Principles of Heat Transfer, Harper & Row Pub., London.
7. Geankoplis, C.J. : Transport Processes and Unit Operations, Prentice Hall of
India Pvt. Ltd., 3rd Edition, 1999.
32
Brief review of the terms: state functions, types of systems, internal energy, heat and work and
reversible and irreversible processes. First Law of Thermodynamics and its Engineering Applications
i.e. constant volume processes, constant pressure processes, isothermal and adiabatic processes,
pumps, turbines, compressors, nozzles, heat exchangers, pitot tube, venturimeter and orifice meter.
Throttling Processes, Joule-Thomson Coefficient, liquefication of gases, thermochemistry includes a
brief review of heat capacities and their measurement, standard heat of reaction, standard heat of
formation, standard heat of combustion, flame temperature, H-x diagrams, heat of solution, partial,
molar enthalpies, enthalpy for phase change etc. Equation of state for real gases and their mixtures.
Principle of corresponding states and generalized compressibility factor.
Review of Second law of thermodynamics, entropy concept, Entropy and lost work calculations.
Microscopic interpretation of entropy. Third Law of thermodynamics and its applications. Free
energy functions and their significance in phase and chemical equilibria, Clapeyron’s equation and
some important correlations for estimating vapor pressures. Estimation of thermodynamic
properties by using graphs and tables.
SECTION- B
Phase Equilibria:
Partial molar properties, partial molar Gibbs free energy, Chemical potential and its dependence on
temperature and pressure Ideal solutions (Lewis-Randel Rule).
Fugacity and its calculations. Dependence of fugacity of temperatures and pressure
Solution behaviour of real liquids and solids. Activity and activity coefficients. Variation of activity
co-efficient with temperature and composition. Activity coefficients of electrolytes standard states.
Properties of mixing. Excess Properties, Gibbs-Duhem equation and its application to vapour-liquid
equilibria.
Chemical Equilibria:
Equilibrium constant in terms of measurable properties variations of equilibrium constant with
temperature and pressure.
Adiabatic reactions, Gibbs phase rule, equilibria in heterogeneous reactions.
Books Recommended:
1. Smith, J.M., Van Ness, H.C. and : Introduction to Chemical Engineering Thermodynamics, 7th
Abbott, M.M. Edition, McGraw Hill Professional, 2005
2. Elliott, J.R and Lira, C.T. : Introductory Chemical Engineering Thermodynamic,
Prentice Hall PTR., 1999.
3. Rao, Y.V.C. : Chemical Engg. Thermodynamics, Orient Blackswan, 1997.
4. Dodge, B.F. : Chemical Engg. Thermodynamics, McGraw Hill, 1944,
Original from the University of Michigan, 2007.
5. Narayanan, K.V. : A Textbook of Chemical Engineering Thermodynamics, PHI
Learning Pvt. Ltd., 2004.
33
Books Recommended:
1. Mc Cabe, Warren L., Smith, Juluain : Unit Operations of Chemical Engineering, 5th Edition, Mc
C. and Harroit, Peter Graw Hill Int. ed (Chemical Engineering Series) Mc Graw
Hill Book Company, New York, 1993.
2. Foust, Alan S., Wenseli, Leonard A., : Principles of Unit Operations, Wiley International Edition,
Clump, Curtis W., mans, Louis and John Wiley & Sons Inc., New York.
Anersen, L. Bryce
3. Coulson, J.M. and Richardson, J.F. : Unit Operations (Volume 2 of Chemical Engineering) New
York: Mc Graw – Hill Book Co;, Inc.
THEORY
Note for the The question paper should be divided into Section A and Section B Total of 8
Examiner questions. 4 questions from section A and 4 questions from section B are to be set.
The students will be required to attempt 5 questions selecting at least 2 from each
section.
SECTION- A
Errors in Numerical Calculations, Solution of Algebratic and Transcendental Equations: The Bisection
Method, The method of False Position, The Iteration Method, Newton-Raphson Method.
Interpolation: Finite Differences, Differences of a Polynomial, Newton’s Formulae for Interpolation,
Central Difference Interpolation Formulae, Interpolation with Unevenly Spaced Points, Divided
Differences and their Properties, Inverse Interpolation, Curve Fitting, Least-Squares Curve Fitting
Procedures, Weighted Least Squares Approximation.
Numerical Differentiation and Integration: Trapezoidal Rule, Simpson’s 1/3 –Rule, Simpson’s 3/8-
Rule, Weddle’s Rules and Romberg Integration.
SECTION- B
Solution of Linear Systems, Gaussian Elimination Method, Gauss-Jordan Method, Jacobi Iteration
Method, Gauss-Seidel Iteration Method.
Numerical Solution of Ordinary Differential Equation: Taylor’s Series Expansion Method, Picard’s
Method, Euler’s Method, Runga-Kutta Methods, Predictor-Corrector Methods, Simultaneous and
Higher Order Equations.
Numerical Solution of Partial Differential Equations: Finite-Difference Approximation to Laplace’s
Equation, Parabolic Equations and Hyperbolic Equations
Recommended Books
1. Hildebrand, F.B. : Introduction to Numerical Analysis.
2. Scarborough, J.B. : Numerical Mathematical Analysis, Oxford and ISH Pub. Co.
3. Chopra, S.C., & Canale, : Numerical Methods for Engineers.
R.P.
SECTION-A
Atomic Structure: Review of bonding in solids, Bonding forces and energies, Primary and Secondary
bonds, structure – property – processing relationships
Crystal Structure : Space lattice, crystal systems, close packed morphology (Hexagonal and cubic
close packing), interstitial spaces, Miller indices, linear and planar densities in crystals, single and
polycrystalline structures, structure of ceramics (NaCl, Zinc blende, CsCl, silica and silicates, diamond
crystal), effect of radius ratio on co-ordination
SECTION-B
Phase diagrams and phase transformation: binary phase diagrams – Fe-Fe3C, Cu-Ni, Pb-Sn.
microstructure development, TTT diagrams, heat treatment processes-hot and cold working,
hardening and softening processes.
Materials: Standards and specifications, unified alloy numbering system, ferrous metals and alloys,
nonferrous metals and alloys; overview of ceramic, polymeric and composite materials;
Corrosion: Types and mechanism of corrosion, factors influencing corrosion, combating corrosion,
selection of materials of construction for handling different chemicals.
Books Recommended:
1. Askelland, Donald R. : The Science & Engineering of Materials, PWSKENT.
2. Shackleford, J.F. : Introduction to Material Science for Engineers, Mc Millan.
3. Van-Vlack, L.H. : Elements of Material Science & Engineering, Addison Wesley
4. Raghavan, V. : Material Science & Engineering, Prentice Hall of India
5. Callister Jr. William D. : Materials Science and Engineering- An Introduction, Wiley
THEORY
Note for the Examiner The question paper should be divided into Section A and Section B Total of 8
questions. 4 questions from section A and 4 questions from section B are to be set.
The students will be required to attempt 5 questions selecting at least 2 from each
section.
SECTION- A
Mass transfer operations, classification of mass transfer operations, choice of separation methods,
methods of conducting mass transfer operations, design principles.
Introduction to mass transfer and diffusion, molecular diffusion in gases and liquids, diffusion coefficients
for gases and liquids, diffusion in solids, types of solid diffusion.
Mass transfer coefficients, types of mass transfer coefficients, mass transfer coefficients in laminar
flow, theories of mass transfer.
38
SECTION- B
Working principle, construction and industrial applications of various gas liquid contacting equipments
like sparged vessels, mechanically agitated vessels, tray towers, packed towers, spray chambers,
venturi scrubbers.
Humidification operations, psychometric chart, adiabatic saturation temperatures, wet bulb
temperature, adiabatic operations, types of cooling towers.
Principle of drying, batch drying, drying curve, constructional details and working of different dryers
Recommended Books
1. Treybal, Robert E. : Mass Transfer Operations, 3rd Edition. McGraw-Hill, 1981.
2. Sherwood, T.K., Pifford, : Mass Transfer, McGraw-Hill.
Robert L. and Wilke,
Charles R.
3. Sharma, K.R. : Principles of Mass Transfer, Prentice Hall of India Pvt. Ltd.,
2007.
4. McCabe, Warren L., Smith : Unit Operations of Chemical Engg., 7th Edition, McGraw-Hill,
Juliam C. and Harriott, 2005.
Peter
5. Coulson & Richardson : Chemical Engineering, Vol.I (6th Edition, 2009) and Vol. II. (5th
Edition, 2006).
Chloralkali industry: Electrochemistry of brine electrolysis, current efficiency, energy efficiency, diaphragm,
mercurcy and dow Cells, caustic soda, chlorine.
Soda Ash: Manufacture of soda ash by Solvay and Modified Solvay process,, handling and safety.
Sulphuric Acid: Introduction, Manufacture of sulphuric acid by Chamber and Contact process, Material
of construction, Storage and handling.
Industrial gases: Manufacture and uses of carbon dioxide, oxygen and nitrogen,
39
acetylene.
Paints: Introduction, Classification of paints, Manufacture of paints, Requirement of a good Paint.
Fertilizers: Nitrogeneous fertilizers- Manufacture of Ammonia, Nitric acid, Urea, CAN, Ammonium
Sulphate. Phosphatic fertilizers- superphosphate and triple superphosphate. Potassic fertilizers-
Potassium Chloride and Potassium Sulphate, Safety aspects.
Books Recommended:
1. Shreev, R.N. & Brink, J.A. : Chemical Process Industries, 5th Edition, McGraw Hill, 1987.
2. Austine, G.T. : Shreeves Chemicals Process Industries, 5th Edition, Mc Graw
Hill, 1984.
3. Dryden, C.E., Rao M.G. & : Outlines of Chemical Technology, 3rd Edition, Affiliated East
Silting, M. West Press Pvt. Ltd., N. Delhi, 2008.
4. Pandey, G.N. : Chemical Technology, Volume-I, Lion Press, Kanpur.
Practical
1. Kinetic studies in a batch reactor.
2. Kinetic studies in a plug flow reactor.
3. Kinetic studies in a CSTR.
4. Kinetic studies in a semi batch reactor.
5. RTD studies in CSTR.
6. Dispersion number for packed bed reactor.
7. Adiabatic batch reactor.
Practical
1. Design of piping & piping networks.
2. Selection, specification & power requirements of process pumps, fans and blowers.
3. Design of settling equipments like Dor thickeners, dust chambers, cyclone separators and
centrifuges.
4. Design of agitated vessels using various types of impellers.
5. Design of Conveyor system for solids.
40
Recommended Books
1. Luding, E.E. : Applied Process Design in Chemical in Petrochemical
Plants, Gulf Publishing Company.
2. Perry, J.H. : Chemical Engineers Handbook, McGraw Hill.
3. Joshi, M.V. : Process Equipment Design, Macmillan Indian.
4. Peters, M.S. and Timmerhaus, K.D. Plant Design and Economics for Chemical Engineers
McGraw Hill.
SECTION- B
Fluid - fluid reactions rate equations and their application to the design of reactors.
Fluid Solid non-catalytic reactors rate equations and their application to the design of reactors.
Analysis of rate data design outline and selection of fixed bed, fluidised bed and slurry reactors for
fluid solid catalytic reactions.
Recommended Books
1. Levenspiel, O : Chemical Reaction Engg., John Wiley
2. Fogler, H.S. : The elements of Chemical Kinetics, McGraw Hill.
3. Smith, J.M. : Chemical Engineering Kinetics, McGraw Hill.
4. Walas, S.M. : Reaction Kinetics for Chemical Engg., McGraw Hill.
5. Hills, C.J. : An Introduction to Chem. Engg., Kinetics and Reactor Design.
SECTION- B
Liquid-Liquid Extraction: Ternary Equilibria and its representation on various plots. Selection criteria
for solvent, Multistage extraction using partially miscible & immiscible solvents. Stagewise contact for
countercurrent and crosscurrent extraction. Constructional details of equipment like mixer-settler,
packed columns, pulsed extractor, sieve-tray extractor and centrifugal extractor.
Leaching: Preparation of solid, countercurrent and crosscurrent multistage contact Shank’s system.
Constructional details of equipment like Rotocel extractor, Hildebrandt extractor, Bollman extractor,
Kennedy Extractor & Beet-Sugar Diffusion battery extractor.
Adsorption: Types of adsorption, nature of adsorbents, equilibria for adsorption systems. Brief manufacture
and commercial applications and characteristics for common adsorbents. Stagewise & continuous
contacting of fluid and solid phase. Description of contact filtration adsorption system. Hypersorber Ion-
exchange system.
Crystallization: Growth and properties of crystals saturation, nucleation, growth of crystals, effect of
impurities on crystal formation, effect of temperature on solubility, fractional crystallization, yield of
crystals, crystal purity, yield calculation using phase diagram, energy requirements using enthalpy-
concentration diagram. Methods of creating super saturation-Meirs supersolubility curve. Mechanism
and methods for nucleation. Derivation for ideal growth of crystals and discussion of actual growth.
Swanson-Walker and various vacuum crystallizers.
Recommended Books
1. Treybal, Robert E. : Mass Transfer Operations, 3rd Edition, McGraw-Hill, 1981.
2. Sherwood,T.K., Pigford, R.L : Mass Transfer, McGraw-Hill, Chemical Engineering Series,
& Wilke,C.R. 1975.
3. Skelland, A.H.P. : Diffusion Mass Transfer, John Wiley &Sons., New York, 1974.
4. McCabe, Warren L., Smith : Unit-Operations of Chemical Engg., 7th Edition, McGraw-Hill,
Julian C. and Harriot, H.P. 2005.
5. King, C.J. Separation Processes, Tata McGraw Hill Publishing Co. Ltd.,
: New Delhi , 1982.
6. Geankoplis, C.J. : Transport Process and Separation Processes, 4th Edition,
Prentice Hall Inc., New Delhi, 2003.
THEORY
Note for the The question paper should be divided into Section A and Section B Total of 8 questions.
Examiner 4 questions from section A and 4 questions from section B are to be set. The students
will be required to attempt 5 questions selecting at least 2 from each section.
SECTION- A
Incentives for chemical process control, design aspects of a process control system. Difference
between feedback and feed forward control configuration. Hardware elements of a control
system, Block Diagrams.
Laplace transform and transfer functions. Difference between lumped and distributed
parameter systems, Dynamic behaviour of first and higher order systems, interacting and non-
43
THEORY
Note for the Examiner The question paper should be divided into Section A and Section B Total of 8
questions. 4 questions from section A and 4 questions from section B are to be
set. The students will be required to attempt 5 questions selecting at least 2 from
each section.
SECTION-A
Oils & Fats: Introduction, Extraction of oils from vegetable oils, refining of oils and fats,
hydrogenation of oils.
Soaps and Detergents: Introduction, Raw materials, Manufacture of soap, Classification of detergents,
finishing of detergents.
Water: Sources and Constraints, Impurities: dissolved, suspended, colloidal; Hardness of water;
Water softening; Lime soda, Ion exchange.
Desalination: Classification of processes; Evaporative processes, Multieffect evaporation, multistage
flash, vapour compression; Membrane processes, Reverse osmosis, electrodialysis.
SECTION-B
Pulp & paper: Introduction, Raw Materials, types of pulp, Manufacture of paper.
Sugar: Introduction; Sugar extraction, defacation, sulphitation, carbonation, concentration,
crystallization, drying, refining; Uses of molasses and bagasse.
Polymers :Introduction,Degree of polymerisation,Classification of polymers,Polyethylene,Polyesters
Books Recommended
1. : Chemical Process Industries, 5th Edition, McGraw Hill, 1987.
Shreev, R.N. & Brink, J.A.
2. Austine, G.T. : Shreeves Chemicals Process Industries, 5th Edition, Mc Graw
Hill, 1984.
3. Dryden, C.E., Rao M.G. & : Outlines of Chemical Technology, 3rd Edition, Affiliated East
Silting, M. West Press Pvt. Ltd., N. Delhi, 2008.
4. Pandey, G.N. : Chemical Technology, Volume-II, Lion Press, Kanpur.
Practicals
1. Oils & Fats: Determination of Acid value, Iodine value, Saponification value.
2. Carbohydrates: Reducing and non reducing sugars by (i) Fehlings method (ii) Pavy’s method.
3. Soaps: Determination of free and combined alkali, total fatty matter, moisture and insoluble.
46
THEORY
Note for the Examiner The question paper should be divided into Section A and Section B Total of 8
questions. 4 questions from section A and 4 questions from section B are to be set.
The students will be required to attempt 5 questions selecting at least 2 from each
section.
Section-A
Unit-1
Unit-2
Interphase momentum transport- definition of friction factor for flow in tubes, around spheres.
Section-B
Unit-3
Unit-4
Unit-5
Emphasis on tha analogy between momentum, heat and mass traner with respect to transport
mechanims and governing equations.
Books Recommended:
1. Bird, R.B., Stewart, W.E. and Lightfoot, E.N.: Transport Phenomena, 2nd Edition,
47
THEORY
Note for the Examiner The question paper should be divided into Section A and Section B Total of 8
questions. 4 questions from section A and 4 questions from section B are to be set.
The students will be required to attempt 5 questions selecting at least 2 from each
section.
SECTION-A
General Concept: Need and classification of measurements and instruments, Basic and
auxiliary functional elements of a measurement system. Static and Dynamic Characteristics of
Instruments: Static Characteristics: Range and span, accuracy and static error, reproducibility
and drift, sensitivity and dead zone. Dynamic Characteristics: Speed of response and lag,
fidelity and dynamic error, dead time.
Temperature measurement: Bimetallic thermometers, filled-in system thermometers.
Thermocouples, metal resistance thermometers and thermistors, optical and radiation
pyrometers, radiation receiving elements.
Pressure measurement: Bourdon gauge, Bellows type gauge.
Vacuum measurement– Mcleod gauge, thermoionic type ionization gauge, pirani vacuum
gauge. Measurement of pressure in corrosive fluids: Diaphragm seal, liquid seal and purge
system.
SECTION-B
Liquid level measurement: Direct measurement of liquid level– Float & tape liquid level
gauge, float and shaft liquid level unit, hydraulic remote transmission of liquid level. Level
measurement in open vessels: Bubbler system, diaphragm box system, air trap system. Level
measurement in pressure vessels– Differential pressure manometer, use of liquid seals with a
manometer, displacement float liquid level gauge.
Measurement of viscosity, conductivity, humidity and pH.
Density measurement: Liquid level method, displacement meter and hydrometer.
Weight measurement: Spring scale, pneumatic force meter and hydrostatic force meter.
Process Instrumentation: Recording instruments, indicating and signaling instruments,
48
Books Recommended:
1. Patranabis, D. : Principles of Industrial Instrumentation, Tata McGrawHill Publishing
Co. Ltd.
2. Eckman, Donald P. : Industrial Instrumentation, CBS Publisher and Distributors
3. Considine, D.N. : Process Instruments and Controls Handbook, McGraw Hill
4. Fribance, A.E. : Industrial Instrumentation Fundamentals, Tata McGraw
Publishing Co.
5. Singh, S.K. : Industrial Instrumentation and Control, Tata McGraw-Hill
:
Practical
1. Process design and specifications of double pipe heat exchanger, shell and tube heat exchanger,
plate type heat exchanger, condenser and reboiler.
2. Design of distillation column, calculation of number of plates, height and design of fractionator
internals- sievetray.
3. Absorber/Stripper design of stage-wise and continuous contact equipment (packed column),
height of column and diameter calculations. HTU and NTU.
4. Design aspects of fixed bed reactors and fluidized bed reactors.
Books Recommended:
1. Coulson, Richardson & Sinnott, : Chemical Engineering, Volume 6 – An Introduction to Chemical
R.K. Engineering Design, 4th Edition, Pergamon Press, 2007.
2. Ludwig, E.E. : Applied Process Design in Chemical and Petrochemical Plants,
2nd Edition, 1977.
3. Perry, J.H. : Chemical Engineers Handbook, 8th Edition, McGraw Hill, 2007.
4. Kern, D.Q. : Process Heat Transfer, McGraw Hill, 1965.
5. Shell and Tube Type Heat : Instt., IS: 43-197.
Exchangers, Indian Standards.
6. Treybal, Robert E. : Mass Transfer Operations, 3rd Edition, McGraw-
1981.
7. Levenspiel, O. : Chemical Reaction Engineering, 3rd Edition, John Wiley
and Sons,
2004.
8. Walas, S.M. : Reaction Kinetics for Chemical Engg., McGraw Hill.
Practical
Forms of technical reports: aims and forms according to type of readership and extent of circulation.
Abstracts, extended abstracts, tables, graphs. Visual representation of data: slides, microfilms, others
techniques including those of audio-visual representation. Correct use of audio equipment.
Research papers and their presentation and publication. Information retrieve direct and through
abstracts.
Practical training in writing and presentation of technical reports through audio-visual means.
Technique of effective public speaking organized and imprompt discussions.
Preparation of technical report on an assigned topic after survey of scientific, technical and
commercial literature, using card indexes, microfilms and other information retrieval methods.
Use of Computer softwares for report writing.
Books Recommended:
1. Mikdran, A.M. : Use of Engineering Literature, Butter Worths.
2. Sottle, R.T. : The Use of Chemical Literature, Butter Worths.
3. Hoover, H. : Essentials For TheTechnical Writer, John Wiley.
4. Robertson, W.S. & : Technical Writing and Presentation, Pergamon.
Siddle, W.D.
50
THEORY
Note for the Examiner The question paper should be divided into Section A and Section B Total of 8
questions. 4 questions from section A and 4 questions from section B are to be set.
The students will be required to attempt 5 questions selecting at least 2 from each
section.
SECTION-A
Ambient air and water standards. Principal sources of pollution.
Inter-relationship between energy and environment pollution. Prevention of environmental pollution
through conservation, raw material substitutions, process and equipment modifications. A case study
on the concept of zero discharge.
Air Pollution:
- Principal air pollutants and their usual sources.
- Effect of air pollutants on human health, animals, vegetation and materials.
- Atmospheric dispersion of air pollutants, temperature inversions, Estimation of pollutants by
Gaussian plume model.
- Process and equipments used for the control of particulate pollutants.
SECTION-B
Water Pollution:
- Types of water pollutants, their sources and effects.
- BOD and COD
- Waste water treatment techniques and equipments, flocculation, skimming, floatation, etc.
- Primary Treatment-through settling.
- Secondary Treatment-Aerobic and anaerobic digestion, activated sludge process, trickle filter and
oxidation ponds.
Solid wastes: Control and disposal, sanitary landfill, incineration, pyrolysis gasification and
recycling.
Books Recommended:
1. Perkins, H.C. : Air Pollution, McGraw Hill, N.Y.
2. Rao, C.S. : Environmental Pollution Control Engineering, 2nd Edition, New Age
International Pvt. Ltd., 2006.
3. Williamson, S.J. : Fundamental of Air Pollution, Addison Wesley Co. N.Y.
4. Numerow, N.L. : Liquid Wastes of Industry, Addison Wesley Co., N.Y.
5. Sincero, A.P. and Environmental Engineering, Prentice-Hall of India, 1999.
Sincero, G.A. :
6. Hammer, M.J. and Jr. : Water and Wastewater Technology, 6th Edition, Prentice-Hall of
Hammer, M.J. India, 2008.
7. Mahajan, S.P. : Pollution Control of Process Industries, Tata McGraw Hill.
8. Metcalf and Eddy : Waste-Water Engineering, 4th Edition, Tata McGraw Hill, 2007.
51
THEORY
Note for the The question paper should be divided into Section A and Section B Total of 8
Examiner questions. 4 questions from section A and 4 questions from section B are to be set.
The students will be required to attempt 5 questions selecting at least 2 from each
section.
SECTION-A
Cost estimation: Factors affecting investment and production costs. Capital investments, fixed
investments and working capital. Cost indices. Estimating equipment costs by scaling 6/10 factor rule.
Methods for estimating capital investment. Estimation of total product cost. Different costs involved in
the total product costs. Different cost involved in the total product for a typical chemical process
plant.
Interest and Investment Costs: Simple and compound interest. Nominal and effective rates of interest.
Continuous interest ordinary annuity. Perpetuities and capitalized costs.
Taxes and Insurance: Types of taxes and tax returns, types of insurance and legal responsibility.
Depreciation: Types of depreciation. service life salvage value, present value and methods of
determining depreciation, single unit and group depreciation.
SECTION-B
Profitability, Alternative Investments and Replacements: Mathematical methods of profitability
evaluation. Cash flow diagrams. Determination of acceptable investments. Alternatives when 'an
investment must be made and analysis with small increment investment, replacement. Breakeven
analysis. Balance sheet and income statement.
Optimum Design: Procedure with one variable, optimum reflux ratio in distillation and other examples.
Preliminary Steps in Plant Design: Plant design factors. project organization, plant location, preliminary
data collection, process engineering
Books Recommended:
1. Peters, M.S. & : Plant Design and Economics of Chemical Engineers, Mc Graw Hill,
Timmerhaus, K.D. New York, 4th Edition, 1991.
2. Ulrich, G.D. : A Guide to Chemical Engineering Process Design & Economics, John
Wiley, 1984.
3. Guthrie, K.M. : Process Plant Estimating, Evaluation & Control, Craftsman Solano
Beach, Calif, 1947.
4. Jelen, F.C. : Cost and Optimisation Engineering, McGraw Hill, New York, 1970.
5. Holland, F.A. & : Introduction to Process Economics, 2nd Edition, Wiley, 1983.
Wastson, F.A.
6. Bassel, W.D. Preliminary Chemical Engineering Plant Design, Elsevier, New York,
1976.
PROJECT WORK
Proj. Marks: 50 Credit: 2
Each student is required to submit a project report on the design of a chemical plant, selecting the
best process with optimum equipment size and operating conditions. The object is to test the ability of
52
the student to apply his entire knowledge of Chemical Engineering principles to conceptualize, analyze
and solve the problems. To judge his knowledge and originality and capacity for application of
laboratory data in designing chemical plants and to determine the level of his proficiency at the end of
the course.
Practical
Functional design, property estimate as inputs for design. System concepts for computer aided design,
computer aided flow sheet design. Process analysis. Process variables selection, equipment design
through the selection of free parameters subject to constraints and other parameters, modular design.
Simulation optimality. Dynamic design including control stability.
Typical equipments to be considered: heat exchangers, distillations columns, reactor and process
equipments.
Books Recommended:
1. Luyben, W.L. : Process Modeling, Simulation & Control, Mc Graw-Hill Book Co.
2. Franks, R.G. E. : Modeling and Simulation in Chemical Engineering, Wiley
Interscience.
3. Mischke, C. : Computer Aided Design, Prentice Hall.
53
Section-A
Overview of fuel cells: Low and high temperature fuel cells;
Fuel cell thermodynamics - heat, work potentials, prediction of reversible voltage, fuel cell efficiency.
Fuel cell reaction kinetics - electrode kinetics, overvoltages, Tafel equation, charge transfer reaction,
exchange currents,
Electrocatalyses - design, activation kinetics,
Fuel cell charge and mass transport - flow field, transport in electrode and electrolyte.
Section-B
Fuel cell characterization: - in-situ and ex-situ characterization techniques, i-V curve, frequency
response analyses; Fuel cell modeling and system integration: - 1D model - analytical solution and CFD
models. Balance of plant; Hydrogen production from renewable sources and storage; safety issues,
cost expectation and life cycle analysis of fuel cells.
Books Recommended
Text books: 1. O'Hayre, R.P.,S. Cha, W. Colella, F.B.Prinz, Fuel Cell Fundamentals, Wiley, NY
(2006).
2. Basu,S.(Ed) Fuel Cell Science and Technology,Springer, N.Y.(2007).
3. Liu, H.,Principles of fuel cells, Taylor & Francis, N.Y. (2006)
Reference 4. Bard,A. J. , L. R., Faulkner,Electrochemical Methods, Wiley, N.Y.(2004)
Books:
NANO TECHNOLOGY(Theory)
THEORY Time 3 Hours
Note for the The question paper should be divided into Section A and Section B Total of 8
Examiner questions. 4 questions from section A and 4 questions from section B are to be set.
The students will be required to attempt 5 questions selecting at least 2 from each
section.
Section-A
Introduction: Plenty of room at the bottom-Feynman’s concept, evolution of ultra-fine materials, the
missing link between conventional laws in physics and chemistry and new theories.
Building Blocks of Nanotechnology: covalent architecture, coordinated architecture and weakly
bound aggregates, Interactions and topology
54
Chemical Properties: The effect of nanoscale metals on chemical reactivity, effect of nanostructure on
mass transport, metal nanocrystallites support on oxides, supported nanoscale catalysts.
General principles for synthesis of monodispersed nanoparticles, metals and intermetallics, Ceramics,
composites, nanoparticles, colloids/Micelles/vesicles/Polymers/glasses, Crystalline, and zeolite hosts.
Review of fundamental behaviour of 0-D(nanoclusters), 1-D(nanowires), 2-D(thin film multilayers),
and 3-D(bulk nanostructures) materials. Introduction to size dependent phenomenon in nanostructure
for various applications, specific production techniques like chemical vapor deposition, arc ignition etc.
Formation of clusters and nanoparticles from supersaturated vapor and selected properties,
sputtering and thermal evaporation and laser methods. Synthesis of nanoparticles by chemical routes.
Section-B
Approches to production: Top down and bottom up,Mechanical attrition, high energy ball milling, and
mechanical attrition, nanocomposites by mechano-chemistry, mechanism of grain size reduction,
property of microstructure relationships.
Characterization techniques : Tools in nanotechnology: Scanning electron microscopy(SEM),
Transmission electron microscopy and high resolution(TEM), energy dispersive spectroscopy (EDX),
Atomic force microscopy(AFM), Magnetic force microscopy(MFM), Chemical Force Microscopy(CFM),
Focused ion beam, nanolithography, powder x-ray diffractometry, UV visible.
Books Recommended
1. Nanoscale Materials in Chemistry by Kenneth J. Khabhunde (ed.) Wiley Interscience.
2. Nanotechnology – An introduction to nanostructure of technique by Michel Kohler and
Wolfgang Frittsche 2004- Wiley VCH
3. Springer Handbook of Nanotechnology by Bharat Bhushan
4. Encyclopedia of Nanotechnology- Hari Singh Nalwa.
5. Nanostructures and Nanomaterials by G. Cao, Imperial College Press, 2004
6. Introduction to Nanotechnology by Owen and Poole, Wiley
7. Nano-materials by A. K. Bandopadhyay, New Age International
Section-A
Chemistry of polymers:
Monomers, functionality, degree of polymerizations, classification of polymers, glass transition,
melting transition, criteria for rubberiness,
Polymerization methods: addition and condensation; their kinetics, copolymerization, monomer
reactivity ratios and its significance, kinetics, different copolymers, random, alternating, azeotropic
55
Polymer Characterization:
Solubility and swelling, concept of average molecular weight, determination of number average,
weight average, viscosity average and Z-average molecular weights, polymer crystallinity, analysis of
polymers using IR, XRD, thermal (DSC, DMTA, TGA), microscopic (optical and electronic) techniques.
Section-B
Polymer Technology:
Polymer compounding-need and significance, different compounding ingredients for rubber and
plastics, crosslinking and vulcanization
Polymer processing:
Compression molding, transfer molding, injection molding, blow molding, reaction injection molding,
extrusion, pultrusion, calendaring, rotational molding, thermoforming, rubber processing in two-roll
mill, internal mixer.
Books Recommended:
SECTION A Hrs
Difference equations:Solution of difference equations with constant coefficients,
Complementary function and Particular solution. 5
SECTION B Hrs
Text Books 2. G. B. Thomas, R. L. Finney: Calculus and Analytic Geometry, Ninth Edition, Pearson
Education.
3. E. Kreyszig: Advanced Engineering Mathematics, Eighth Edition, John Wiley.
Reference 4. B. V. Ramana: Higher Engineering Mathematics, Tata McGraw Hill.
Books 5. B. S. Grewal: Higher Engineering Mathematics, 41st Edition, Khanna Publishers,
Delhi.
Course Assessment will consist of the following components
1.Mid-Term
Assessment a. One best of two minor tests (50% of Mid -term marks)
Methods b. Assignments (20% of Mid-term marks)
c. Class Surprise Tests/ Quizzes/Presentations/Term paper (20% of Mid-term marks)
d. Attendance. (10% of Mid-term marks)
2.End –Term
Course The students are able to:
Outcomes solve difference equations with constant coefficients.
find Z-transforms and inverse Z-transforms and apply these to solve difference
equations.
find correlation, coefficient of correlation, rank correlation, regression and standard
error of estimate.
apply various probability distributions, test of significance and goodness of fit.
57
Section-A
Introduction to Supply Chain Management:Definition; Scope & Importance of Supply Chain
Management; Key drivers Of the SCM; Features of Supply Chain Management; Supply Chain Network –
1st Tier , 2nd Tier; Network decisions in SCM; Suppliers and Customers; Customer Service Dimension
(Seven “R” Principles, Service after sale, Customer delight)
Role of Logistics in Supply Chains: Definition of Logistics Management; Scope and role of
Transportation, Traffic & transportation; Relationship between transportation and other business
functions, Transport Economics: Distance – volume-density, Freight Cost, Handling, Liability, market
factors; Third party logistics (3 PL) & fourth party logistics service provider (4 PL), Logistics equipment;
Reverse Logistics, Government rule & regulations related to Logistics; Purchase Cycle, Make or Buy,
Price analysis, Negotiations.
Section-B
Inventory Management: Inventory Control, Planning & Managing Inventories; Warehouse
Management (Receipt, issue, storage and preservation, stock verification, In bound and out bound
distribution operations); Order Management; Competitive advantage through logistics and supply
chain management; Responsive Supply Chain; Supply chain process integration, performance
measurement; Value Chain, Value System and Supply Chain.
Planning demand and supply: Planning & Sourcing in Supply Chain, Demand forecasting, Type and
Time horizon of forecast and category of forecasting, aggregate planning; Financial issues in Supply
Chain - Macro and micro view, Asset management, Du Pont Model, Supply Chain Costing; Decision
environment in SCM; Global supply chain perspectives - New business models, role of IT in SCM.
Books Recommended:
1. Harald Dyckhoff et al, Ed.: Supply Chain Management and Reverse Logistics, Springer (India).
2. Jayashree Dubey and M.L. Saikumar Ed.: Supply Chain Management, IIPE Hyderabad and New
Century Publication.
3. Sarika Kulkarni, Ashok Sharma: Supply Chain Management-Creating Linkages for Faster Business
Turnaround, McGraw Hill.
4. RP Mohanty: Supply Chain Management-Theories and Practice, Biztantra.
5. Robert B. Handfield, Ernest L. Nicholas, Jr.: Introduction to Supply Chain Management,Pearson
Education.
6. Ronald H. Ballou, Samir K. Srivastava: Business Logistics/Supply Chain Management, Pearson
Education.
7. John Mentzer: Supply Chain Management, Response Books.
8. Janat Shah: Supply Chain Management, Pearson Publications.
9. N. Chandrasekaran: Supply Chain Management - Process, System and Practice, Oxford Press.
58
Books Recommended:
Section-A
Introduction to petroleum industry, world petroleum resources, petroleum industry in India. Origin,
exploration & drilling of petroleum crude. Transportation of crude and products.
Crude pretreatment: Refining and distillation of petroleum crude, composition and classification of
petroleum crude, methods of evaluation: ASTM, TBP and EFV distillation. Properties and specifications
of petroleum products such as LPG, gasoline,naphtha, kerosene, diesel, lubricating oils and waxes.
Section-B
Separation Processes: Design and operation of topping and vacuum distillation units and tube still
furnaces. Solvent extraction processes for lube oil base stock and for aromatics from naphtha and
kerosene steams, solvent dewaxing.
Conversion Processes: Thermal cracking: visbreaking and coking processes, catalytic cracking, thermal
reforming and catalytic reforming, alkylation, polymerization, isomerisation and hydroprocessing.
Safety and pollution considerations in refineries.
Books Recommended:
1. Nelson, W.L. : Petroleum Refinery Engineering, 5th Edition, McGraw Hill, 1985.
2. Rao, B.K. : Modern Petroleum Refining Processes, 5th Edition, Oxford & IBH
Publishing Co., 2009.
3. Guthrie, V.B. : Petroleum Products Handbook, McGraw Hill, 1960.
4. Hobson, G.D., Pohl. : Modern Petroleum Technology, 5th Edition, John Wiley, 1984.
W.
Section-A
Definition, Hazards identification, Hazards and operability studies (HAZOP), Failure mode and effect
analysis (FMEA), classification and assessment of various types of hazards in work-place environment
and Industrial Hygiene, protective and preventive measures in hazard control.
Toxic Chemicals: maximum allowable concentrations and other standards. Biological threshold limit
values.
Mechanical and electrical hazards. Personal protective equipments. Explosives and inflammable
substances. Radioactive hazards. Good housekeeping in industrial environment.
Section-B
60
Fire prevention, design to prevent fire and explosion (inverting static electricity, sprinkler system),
boiling liquid expending vapour explosion (BLEVE). Fire triangle, Dow’s Fire and explosion index,
dilution and ventilation.
Standard safety procedures and disaster control; OSHAS, OHSMS and OSHA. Current amendments in
Indian Legislation on safety and prevention of hazards and safety code: ISO 14000, ISO 9000.
Environmental impact assessment. Control strategies for hazardous wastes.
Case Studies of typical hazardous industries.
Books Recommended:
1. Wills, G.L. : Safety in Process Plant Design.
2. Less, F.P. : Loss Prevention in Process Industries.
3. Chanleft, E.T. : Environmental Protection.
4. Berhowex, P.M. & Rudd, : Strategy of Pollution Control.
D.F
5. Safety for Chemical : A.I.Ch.E. Publications, 1976-77.
Engineers
PLANT UTILITIES(Theory)
THEORY Time 3 Hours
Note for the The question paper should be divided into Section A and Section B Total of 8
Examiner questions. 4 questions from section A and 4 questions from section B are to be set.
The students will be required to attempt 5 questions selecting at least 2 from each
section.
Section-A
Importance of Process utilities in Chemical Plant.
Compressed air and Vacuum: Reciprocating air compressors, vacuum pumps, air receivers, piping
systems.
Steam: Boiler, steam handling and distribution steam nozzles.
Section-B
Refrigeration: Air refrigeration cycle, vapour compression cycle, liquification processes.
Power Generation: Internal Combustion engines. Gas turbines, steam power plants.
Water: Water Resources, storage & distribution of water reuse & conservation of water.
Books Recommended:
1. Jouganson, R. : Fan Engineering, Buffalo Rorge Co., 1970.
2. Wangham, D.A. : Theory and Practice of Heat Engines, ELBSCambridgeUniversity Press,
1960.
3. Lyle, O. : Efficient Use of Steam, HMSO, 1963.
4. Stoccker, W.F. : Refrigeration and Air Conditioning, Mc-Graw Hill, 1950.
5. Kurl, W.F. J.H.M. : Reuse of Water in Industry, Butterworth, London.
Section-A
General Introduction: Definition, history and economic perspective of petrochemical
industry, raw materials for petrochemical industry-petroleum, natural gas, coal, bio-mass,
agro-residues, etc.
First Generation Petrochemicals: Petrochemicals based on aliphatic, olefinic, acetylene,aromatics, etc.
Hydrocarbons-processing and applications.
Second Generation Petrochemicals: Products based on Synthesis Gas, Method, Ethanol,Ethylene
Oxide, Vinyl Chloride, Propylene Oxide, Isopropyl Alcohol, Acetone, AllylAlcohol, Glycerol, Phenol,
Aniline.
Section-B
Nylon Monomers, Polyester Monomers, Styrene, Other Monomers - Bisphenol A, Epichlorophydrin,
diisocyanates, Pentaerythritol, etc. - properties,process technologies and applications. .
Third Generation Petrochemicals: Important Polymers such as Polyethylene, Polypropylene and their
Copolymers and other Derivatives Rubbers, Diene Polymers, Styrene Polymers,Vinyl Polymers and
Condensation Polymers - properties, process technologies and applications.
Books Recommended:
1. Steiner, H.: Introduction to Petroleum Chemicals, Pergamon Press.
2. Waddane, A.L. : Chemicals from Petroleum, John Murry.
3. Topchiev, A.V. : Synthetic Materials from Petroleum, Pergamon Press.
4. Astle, M.J. : The Chemistry of Petrochemicals, Reinhold.
5. Maiti, S.: Introduction to Petrochemicals, Oxford and IBH Pub. Co. Ltd., New
Delhi, 1992.
6. Frank, H.G. &Stadelhofer, J.W.: Industrial Aromatic Chemistry, Springer Verlag Berlin, 1987.
Section-A
Isolation and Utilization of Enzymes: Purification, immobilization, application of enzyme technology.
Kinetics of Enzyme-Catalyzed Reactions: The substrate, enzyme kinetics, factors affecting enzymatic
activity and enzymatic reactions in heterogeneous reactions.
Metabolic Pathways and Energetics of the Cell: The concept of energy coupling, aerobic and anaerobic
metabolism, photosynthesis and biosynthesis, transport across cell membranes.
Cellular Genetics and Control: Growth and reproduction of a single cell, alteration of cellular DNA,
commercial applications.
Section-B
Kinetics of Substrate Utilization. Product Yield and Biomass Production: Growth cycle for batch
cultivation and its mathematical modeling, products synthesis kinetics, thermal death kinetics of cells
and spores.
Transport Phenomena in Microbial Systems: Gas-liquid mass transfer, determination of oxygen
transfer rates, mass transfer, surface-area correlations for mechanically agitated vessels, scaling of
mass transfer equipment, particulate mass transfer, heat transfer.
Design and Analysis of Biological Reactors: The ideal continuous-flow stirred-tank reactor (CSTR),
residence time distribution, different types of reactors, relationship between batch and continuous
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1. Balley & Ollis : Biochemical Engineering Fundamentals, McGraw Hill Book Co.,
1986.
2. Aiba Humphrey & Millis : Biochemical Engineering, Academic Press, 1973.
3. Whitaker Stanbury & : Principles of Fermentation Technology, Adita Books, New Delhi,
Whitaker, Hall 1997.
SECTION B
Reference Books
McCabe WL, Smith JC and Harriott P. 1993. Unit operations of Chemical Engineering.
McGraw Hills.
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