CHPL332 Size Reduction of Solids - Semester 1-2024
CHPL332 Size Reduction of Solids - Semester 1-2024
• rr
Mr PC Jiyane
1st Semester 2024
Why Carry Out Size Reduction?
Size reduction also known as Comminution –
increases the surface area of solid material
and is carried out to achieve the following:
• To break material into very small particles in
order to separate two constituents.
• To considerably influence the properties of
material, e.g., chemical reactivity.
• To improve the colour and the covering power
(tinting strength) of a pigment.
• To improve or promote intimate mixing of solids.
2
Some Pros and Cons to NOTE
• In reactions – the rate of reactions is directly
proportional to the area of contact, e.g. in
combustion, the rate of combustion of solid particles
is proportional to the area presented to the gas.
1.6
Mass per μm (%)
1.2
1150
950
800
650
0.4 500
400
200
0
4 0 200 400 600 800 1000 1200 1400 1600
Particle diameter (μm)
Mechanism of Size Reduction
Size reduction process consists of two parts:
• Opening of any small fissures present, and the
• Formation of new surfaces.
5
Mechanism of Size Reduction
Basic Force Application Patterns:
Impact Compression Shear Attrition
6
Energy Requirements
For fracture to occur, the particle must first go through
the condition of plastic deformation. And a much larger
portion of energy is expended to achieve this. This
energy is regarded as waste as it does not result in
fracture.
Although it is impossible to estimate accurately the
energy required to effect size reduction, 3 empirical laws
may be used.
8
Energy Requirements
L1
If p = −1, then integration gives: E = Cn
L2
L1
Substituting q = and C = 5 Ei , this becomes the Bond’s Law:
L2
100 1
E = Ei
1 −
q
L2
13 kW mm
𝐾𝑅 𝑓𝐶 = = 162.5
0.08 kgΤs
Expression for
Measured Characteristic
Mean Diameter
σ 𝑛1 𝑑14
Mass mean diameter: 𝑑𝑚 𝑑𝑚 =
σ 𝑛1 𝑑13
σ 𝑛1 𝑑13
Surface mean diameter: 𝑑𝑠 𝑑𝑠 =
σ 𝑛1 𝑑12
σ 𝑛1 𝑑12
Length mean diameter: 𝑑𝑙 𝑑𝑙 =
15 σ 𝑛1 𝑑1
Particle Characterization
Screen Analysis
Test sieves are scientific screening equipment, that utilize woven
wire screens mounted on rigid frames to help generate
reliable particle size distribution curves.
Sieves with varying mesh openings
are typically stacked on top of each
other, working to separate the
particles of a material sample based
on their size.
37.987 177.918
𝑳𝟐 = 𝟒. 𝟔𝟖𝟒 𝐦𝐦
𝟑𝟕. 𝟗𝟖𝟕 𝟏𝟕𝟕. 𝟗𝟏𝟖
18
Class Exercise SR2: Solution Refer to
Slide 24
𝐿1 kJ/kg MN 42.5
𝐸 = 𝐾𝐾 𝑓𝐶 ln = 0.255 45 ln
𝐿2 MN/m2 m2 0.5
𝑘𝐽
𝑃 = 50.98 × 1 kg/s
𝑘𝑔
19
𝑷 = 𝟓𝟎. 𝟗𝟖 𝐤𝐖
Energy Utilization
It can be concluded (from investigations) that the distribution
of energy fed into a crusher is utilized as follows:
Jaw Crusher
the type of equipment
chosen to handle
specific properties of
21 the material.
Crusher Feeding Methods
Free Crushing: feeding material at comparatively low
rates.
• Product can escape readily
• Residence time of material in machine is
short
• Production of large quantities of undersize
material is avoided.
Undersize
Separator
Undersize
Flow Diagram for
Oversize
Closed Circuit Grinding System
Fine
23 Product Crusher
Equipment Classification
Generally, it is not economical to effect large reduction ratio in
a single unit.
When a number of units are used, the equipment is usually
divided into the following classes according to the size of feed
and the product.
29
Coarse Crushers
u Cross-section of Stag Jaw Crusher
30
Intermediate Crushers
u Swing Claw Hammer Mill
31
Fine Crushers
u View of an NEI
Sectional
Pendulum 5-Roller Mill
32
Typical SR Plant Layout
u
Product
34
Crushing Rolls
• Two rolls, one in adjustable bearings, rotate in opposite
directions. Feed
requirements.
• Capacity is between 10 and 30% of that
calculated on the assumption that a
continuous ribbon of material forms
between the rolls. Product
(r1 + b )
Thus the angle of nip is given by: cos =
(r2 + r1 )
36 and the coefficient of friction, μ = tan α
Class Exercise SR3
If crushing rolls 1 m in diameter are set so that
the crushing surfaces are 12.5 mm apart and the
angle of nip is 310, what is the maximum size of
particle which should be fed to the rolls?
37
Class Exercise SR3: Solution
?
Given: 𝑟1 = 𝑑Τ2 = 1.0Τ2 = 0.5 m ; 2𝛼 = 310 ; 𝑟2 = ? Particle
0
𝛼 = 31 ൗ2 = 15.50 → 𝑐𝑜𝑠𝛼 = 0.9636
α α
2𝑏 = 12.5 mm → 𝑏 = 12.5Τ = 6.25 mm α α
2 Crushing Roll b b Crushing Roll
𝑏 = 0.00625 m
cos =
(r1 + b ) 0.5+0.00625 0.50625
↔ 0.9636 = =
(r2 + r1 ) 𝑟2 +0.5 𝑟2 +0.5
𝒓𝟐 = 𝟎. 𝟎𝟐𝟓𝟒 𝐦 𝒐𝒓 𝟐𝟓. 𝟒 𝐦𝐦
kg
Now: 𝑙 = 0.4 m ; 𝜌 = 2500 ൗm3 ; 𝑣 = 2 m/𝑠
ሶ
Mass flowrate m = 15% × 𝑄 × 𝜌 = 0.15 × 0.010 × 2500
38
𝐦 = 𝟑. 𝟕𝟓 𝐤𝐠/𝐬
Types of Crushing Equipment
Ball Mill Abrasive Balls
Product
Rotation
39
The Ball Mill
• Used for grinding a wide range of materials, including
coal, pigments and felspar for pottery.
• Can take on feed with particle size up to 50 mm.
• In compound mills, the cylinder is divided into a number
of compartments by vertical perforated plates.
• Compartments have different size balls – large balls at the
entry end and small balls grind material before discharge.
• Material flows axially along the mill and passes from one
compartment to the next through perforations in the plate.
• Efficiency increases with the hold-up in the mill, until the
voids between the balls are filled. Any further increase in
the quantity, lowers the efficiency.
40
The Ball Mill
Grinding Material (Balls):
42
The Ball Mill
u
The property of the feed material The level of material in the mill
The larger the feed, the larger is the product Power consumption is reduced by
under given operating conditions. A smaller maintaining a low level of material in the mill.
size reduction is obtained with hard material.
The speed of rotation
Weight of balls
• Low speeds – Balls simply roll over one
Heavy charge of balls produces a fine
another and little crushing occurs.
product.
• Slightly higher speeds – Balls are
Diameter of balls projected short distances across the mill.
Small balls facilitate the production of fine
• High speeds – Balls are thrown greater
material, although they do not deal effectively
distances and wear on the lining of the
with larger particles in the feed.
mill takes place.
The slope of the mill • Very high speeds – Balls are carried right
An increase in the slope of the mill increases round in contact with the sides of the mill
the and little relative movement or grinding
44 capacity of the plant – retention time is
reduced but coarser product is produced. takes place.
The Ball Mill
Factors influencing the size of the product
• The rate of feed • The slope of the mill
• The properties of the feed material • Discharge freedom
• Weight of balls • The level of material in the mill
• The diameter of the balls • The speed of rotation of the mill
Thus when the mill is rotating at the critical angular velocity, 𝝎𝒄 then:
𝑔
𝜔𝑐 =
𝑅−𝑟
The critical rotational speed, 𝑵𝒄 in revolutions/unit time, is given by:
𝜔𝑐 1 𝑔
𝑁𝑐 = =
2𝜋 2𝜋 𝑅 − 𝑟
• where 𝑹 is the radius of the mill, 𝒓 is the radius of the particle, and
𝒈 is the acceleration due to gravity = 9.81 m/s 2
45 Optimum speed is bt ½ and ¾ of the critical speed.
Class Exercise SR4
A ball mill, 1.20 m in diameter, is run at 0.80 Hz
and it is found the mill is not working properly.
Should any modification in the condition of
operation be suggested?
Rotating Direction of Mill
f = 0.80 Hz
Feed Material
d = 1.20 m
Steel Balls
46
Class Exercise SR4: Solution
Given: 𝑅 = 𝑑Τ2 = 1.20Τ2 = 0.60 m ; 𝑓 = 0.80 𝐻𝑧
For small particles: 𝑅 − 𝑟 ≈ 0.60 ;
𝑔 9.81
𝜔𝑐 = ↔ 𝜔𝑐 = = 4.04 rad/s
𝑅−𝑟 0.60
1 𝑔 1 9.81
𝑁𝑐 = = = 0.463 rps
2𝜋 𝑅 − 𝑟1 2𝜋 1.2 − 0.04
0.463 rev 60 s
𝑁𝑐 = ×
s 1 min
𝑁𝑐 = 27.78 rpm
1 𝑔 1 9.81
𝑁𝑐 = = = 0.458 rps
2𝜋 𝑅 − 𝑟2 2𝜋 1.2 − 0.0175
0.458 rev 60 s
𝑁𝑐 = ×
s 1 min
𝑁𝑐 = 27.48 rpm