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Iso 9096

ISO 9096 provides guidance on manually determining the mass concentration of particulate matter in stationary source emissions. It describes key principles such as isokinetic sampling to ensure representative samples. The document specifies minimum numbers of sampling points and times based on duct size to obtain accurate measurements. Sampling is done by extracting a gas sample through an isokinetic nozzle into a filter to separate and weigh collected particulate matter.

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Hairul Saprudin
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346 views13 pages

Iso 9096

ISO 9096 provides guidance on manually determining the mass concentration of particulate matter in stationary source emissions. It describes key principles such as isokinetic sampling to ensure representative samples. The document specifies minimum numbers of sampling points and times based on duct size to obtain accurate measurements. Sampling is done by extracting a gas sample through an isokinetic nozzle into a filter to separate and weigh collected particulate matter.

Uploaded by

Hairul Saprudin
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as PPTX, PDF, TXT or read online on Scribd
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ISO 9096

Stationary source emissions — Manual determination of mass


concentration of particulate matter
ISOKINETIC
• %isokinetic = Vn/Vs
ISOKINETIC

ISO = EQUAL + KINETIC = MOTION

Nozzle
UNDER ISOKINETIC
When the nozzle velocity is less than the stack velocity the results
will be biased high due to the inertia of the large particles.

Nozzle
OVER ISOKINETIC
When the nozzle velocity is greater than the stack velocity the results will biased low
since the larger particles break through the air stream and bypass the nozzle.

Nozzle
PRINCIPLE

A sample stream of the gas is extracted from the main gas stream at specified sampling points for a measured
period of time, with an isokinetic controlled flowrate. The volume of gas collected is measured, and a pre
weighed filter, which is then dried and reweighed, separates the particulate matter (dust) entrained in the gas
sample. Deposits upstream of the filter in the sampling equipment are also recovered and weighed. The
increase in mass of the filter and the mass deposited upstream of the filter is attributed to particulate matter
collected from the sampled gas. The ratio of the mass of the particulate matter collected to the volume of gas
collected allows the flue gas particulate concentration to be calculated.
Sampling plane and sampling points

1. sampling line
Line in the sampling plane along which sampling points are located, bounded by the
inner duct wall
2. sampling plane
The sampling plane shall be as far downstream and upstream as possible from any
obstruction that may cause a disturbance and produce a change in the direction of flow
(disturbances caused by e.g. bends, fans or pollution abatement equipment).
3. access port
A minimum diameter of 125 mm or a surface area of 100 mm × 250 mm are
recommended, except for small ducts (less than 0,7 m diameter) for which the port size
needs to be smaller
4. Flow
5. top of duct
Sampling plane and sampling points Cont.

Table 1 — Minimum number of sampling points for circular ducts

Minimum number of Minimum number of


sampling sampling
Minimum
Range of points per line points per plane
number
duct
of sampling
diameters
lines
m
(diameters)
incl. centre excl. centre incl. centre excl. centre
point point point point

< 0,35 — 1a — 1a —
0,35 to 0,70 2 3 2 5 4
0,70 to 1,00 2 5 4 9 8
1,00 to 2,00 2 7 6 13 12
> 2,00 2 9 8 17 16
a Using only one sampling point can give rise to errors greater than those specified in this International
Standard.
Sampling plane and sampling points Cont.

Table 2 — Minimum number of sampling points for rectangular ducts characteristic dimension of a duct cross-section

Range of sampling plane Minimum number of


Minimum number of side
areas sampling
division
m2 points per plane

< 0,09 — 1b

0,09 to 0,38 2 4

0,38 to 1,50 3 9

> 1,50 4 16

a Other side divisions may be necessary, for example if the longest duct side length is more than twice the
length of the shortest
side.
b Using only one sampling point can give rise to errors greater than those specified in this International
Standard.
Sampling time

the volume of the sample, Vn


expected dust concentration (cexp)
assumed and the mass of particulate matter (m)
the total sampling time, t (min)
volumetric flowrate under actual conditions, Qa (l/min), i.e.
Vn = tQa
Sampling Apparatus
In stack filter method
Sampling Apparatus
out stack filter method
Sampling

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