Sizing Stripping
Sizing Stripping
LAMPIRAN A
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1. Perancangan Stripper
Data yang diketahui,
Komponen yang dipisahkan yaitu H2S, NH3 dan H2O dengan masing-masing konsentrasi
X1 = 0.009 %wt, X2 = 0.486 %wt dan X3 = 0.515 %wt
Laju alir umpan = 170598,22 kg/jam
Suhu umpan = 49 oC = 323.15 K
Recovery = 99.99 %
Equilibrium data
Tekanan parsial pada umpan 0.009 %wt dan suhu umpan 50 oC = 4.3102 mmHg (Tabel
A.1)
4.3102 mmHg
fraksi mol uap = = 0.00567
760 mmHg
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0.009
fraksi mol liquid = 32
0.009 99.991
32 + 18
= 4,765 × 10−5
0.00567
m= = 119.0223
4,765 × 10−5
y1 p1 6.84
= = = 20
y2 p2 0.342
b. Komponen NH3
Tekanan parsial umpan NH3 = 0.486 % x 760 mmHg = 369.36 mmHg
Tekanan parsial pada keluaran recovery 95% = 369.36 mmHg x 0.05 = 18.468 mmHg
Equilibrium data
Tekanan parsial pada umpan 0.486 %wt dan suhu umpan 50 oC = 22.2 mmHg (Tabel A.1)
22.2 mmHg
fraksi mol uap = = 0.029210526
760 mmHg
0.009
fraksi mol liquid = 17
0.009 99.991
17 + 18
= 9.529 × 10−5
0.029210526
m= = 306.5318372
9.529 × 10−5
y1 p1 369.36
= = = 20
y2 p2 18.468
a. Komponen H2O
Tekanan parsial umpan H2O = 0.515 % x 760 mmHg = 391.4 mmHg
Tekanan parsial pada keluaran recovery 95% = 391.4 mmHg x 0.05 = 19.57 mmHg
Equilibrium data
Tekanan parsial pada umpan 0.515 %wt dan suhu umpan 50 oC = 1.6802 mmHg (Tabel
A.1)
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1.6802 mmHg
fraksi mol uap = = 0.002210818
760 mmHg
0.009
fraksi mol liquid = 18
0.009 99.991
18 + 18
= 0.00009
0.002210818
m= = 24.56464209
0.00009
y1 p1 391.4
= = = 20
y2 p2 19.57
Jumlah stage yang digunakan ditentukan berdasarkan laju air “optimum” yang ditunjukkan
pada gambar 17.49 Sinnot, 2013.
Gambar 17.49 Number of Transfer Unit NOG sebagai fungsi y1/y2 dengan mGm/Lm sebagai
Parameter (Sinnot, 2013)
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Jadi, dengan mem-potkan nilai y1/y2 dan mGm/Lm didapat jumlah NOG optimum yaitu
5.9 stage ≈ 6 stage.
Diameter kolom
kg kg
laju alir gas = 2061.918 = 0.5727
jam s
kg kg
laju alir gas = 168874.288 = 46.9095
jam s
Digunakan jenis packed pall ring metal dengan ukuran 50 mm (2 in)
Dari gambar 17.2, Fp = 66 m-1
Densitas gas = 1.0942 kg/m3 (Yaws, 1990)
Densitas liquid = 678,2610 kg/m3 (Yaws, 1990)
Viskositas liquid = 7.55 x 10-4 (Yaws, 1990)
30.095 1.0942
= ×
0.5727 678.261
= 3.3233
Design pressure drop untuk 20 mm vapor/m packing
Dari gambar 17.54 (Sinnot, 2013)
K4 = 0.04
K4 pada flooding = 0.08
0.04
Persentase flooding = √0.08 × 100 = 71%, Terpenuhi
0.04
Diameter = √ x 1.55873 = 1.40912894 m ≈ 1.5 m = 59 in
0.08
π
area kolom = × 1.5 2 = 1.5587 m2
4
1.5
Rasio packing size dengan diameter kolom = = 28.1825
50 × 10−3
Peren flooding pada diameter yang ditentukan:
1.5587
71 × = 71%
1.5587
Menentukan tinggi kolom
Onda’s methode
R = 0.08314 m3/kmol.K
Tegangan permukaan
Tegangan permukaan pada suhu 50oC yaitu:
Sigma = A(1-T/Tc)^n (Yaws, 1990)
T = 323.15 K
sigma
komponen A Tc n sigma %wt campuran
benzene 71.95 562.16 1.2389 24.9372 0.0175 0.43848
toluene 66.85 591.79 1.2456 24.9956 0.0417 1.04329
etilbenzene 66 617.17 1.268 25.7758 0.0046 0.11958
p-xylene 64.85 616.26 1.2743 25.1565 0.0082 0.20649
m-xylene 65.7 617.05 1.278 25.4621 0.0245 0.62474
propana 49.624 369.82 1.192 4.2086 0.0169 0.07142
isobutana 52.165 408.14 1.2723 7.0856 0.0208 0.14781
n-butana 52.66 425.18 1.233 9.0617 0.0559 0.50655
isopentana 50.926 460.43 1.2078 11.8078 0.0737 0.87124
n-pentana 52.09 469.65 1.2054 12.7908 0.0812 1.03948
siklopentana 72.05 511.76 1.373 18.2993 0.0086 0.15818
n-heksana 56.081 507.43 1.2843 15.2705 0.0582 0.88962
metil siklopentane 61.63 532.79 1.2757 18.7512 0.0290 0.54450
sikloheksana 65.097 553.54 1.2553 21.6614 0.0366 0.79480
n-heptana 53.64 540.26 1.2431 17.2709 0.0439 0.75919
dimetil 55.282 547 1.2168 18.6392 0.0267 0.49811
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siklopentana
metil sikloheksana 61.487 590.94 1.2222 23.3697 0.0730 1.70670
n-oktana 52.036 568.83 1.2168 18.7345 0.0284 0.53286
propil siklopentana 56.934 603 1.241 21.9599 0.0128 0.28178
etil sikloheksana 60.1 609.15 1.302 22.4570 0.0441 0.99147
propil sikloheksana 55.81 639.15 1.2117 23.7702 0.0272 0.64746
nonana 55.4 595.65 1.3027 20.0023 0.0437 0.87604
butil sikloheksana 59.04 667 1.3513 24.1157 0.0112 0.27035
dekana 55.777 618.45 1.3198 21.0254 0.0227 0.47732
pentil sikloheksana 55.129 674.01 1.2222 24.8225 0.0063 0.15849
undekana 55.723 638.76 1.3237 21.9146 0.0032 0.07038
C9+ aromatik (C3
alkilbenzene) 63.487 638.38 1.2764 25.7946 0.0263 0.67859
H2 5.336 33.18 1.0622 0 0.0984 0
Total 15.40504
Jadi, tegangan permukaan campuran pada suhu 50oC yaitu = 15.40504 dyne/cm = 1.54 x 10-3
N/m
Percepatan gravitasi,
g = 9.81 m2/s
dari tabel 17.3 (Sinnot, 2013)
jenis packing : Pall Ring metal
Ukuran : 50 mm
Surface, a : 102 m2/ m3
Fp : 66 m-1
σ untuk keramik : 75 x 10-3 N/m
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difusifitas liquid
T = 323.15 K
D=A+B*T+C*T^2 (Yaws, 1990)
propil
-0.03185 0.0002104 4.2597E-07 0.0753 0.02723 0.00205
sikloheksana
nonana -0.0333 0.0002119 4.0210E-07 0.0681 0.04379 0.00298
butil
-0.02969 0.0001940 4.0041E-07 0.0701 0.01121 0.00078
sikloheksana
dekana -0.03116 0.0001839 3.7930E-07 0.0636 0.02270 0.00144
undekana -0.02927 0.0001708 3.5909E-07 0.0597 0.00321 0.00019
C9+ aromatik -0.03454 0.0001661 4.5190E-07 0.0791 0.02630 0.00207
Total 0.07725 cm2/s
Jadi, difusifitas liquid campuran yaitu, DL = 0.07725 cm2/s = 7.725 x 10-6 m2/s
−0.05 0.2
aw σc 0.75 L∗w 0.1 L∗2
wa L∗2
w (Sinnot, 2013)
= 1 − exp [−1.45 ( ) ( ) ( 2 ) ( ) ]
a σL aμL ρL g ρL σL a
0.75 0.1 −0.05 0.2
aw 75 × 10−3 30.4019 30.40192 × 102 30.40192
= 1 − exp [−1.45 ( ) ( ) ( ) ( ) ]
a 1.54 × 10−3 102 × 7.55 × 10−4 678,262 × 9.81 678,26 × 1.54 × 10−3 × 102
aw
= 0.9996
a
aw = 101.9626 m2 /m3
2 1
ρL 1/3 L∗w 3 μL −2
kL ( ) = 0.0051 ( ) ( ) (adp )0.4 (Sinnot, 2013)
μL g a w μL ρL DL
2 1
1/3 −
678,26 30.4019 3 7.55 × 10−4 2
kL ( ) = 0.0051 ( ) ( ) (102 × 66)0.4
7.55 × 10−4 × 9.81 101.9626 × 7.55 × 10−4 678,26 × 7.7 × 10−6
kL = 0.030787 m/s
0.5727
Vw∗ dalam diameter kolom aktual = = 0.36745 kg/m2 s
1.5587
1/3
k G RT Vw∗ 0.7 μV (Sinnot, 2013)
= K5 ( ) ( ) (adp )−2
a Dv μv a ρv Dv
k G = 6.767 × 10−5 kmol/m2 s atm
0.36745
Gm = = 0.01267 kmol/m2 s
29
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30.4019
Lm = = 0.31776 kmol/m2 s
95.6732
Gm (Sinnot, 2013)
HG =
k G aw P
0.01267
HG = = 1.81263 m
6.767 × 10−5 × 101.9626 × 1.013
CT = total konsentrasi,
678,2610
= = 7.08935 m
95.6732
Lm
HL = (Sinnot, 2013)
k L aw CT
0.31776
HL = = 0.01427 m
0.030787 × 101.9626 × 7.08935
HOG = 1.81263 + 0.8 × 0.01427 = 1.82405 m
Z = jumlah stage × HOG = 6 × 1.82405 = 10.95 m ≈ 11 m = 433 in
Pi. Di
ts = + C
2fE − Pi
(Brownell & Young, 1959)
1.1 × 1.5 × 103
ts = + 4
2 × 0,85 × 135 − 1.1
Tebal tutup
Jenis tutup yang digunakan adalah torisperical heads karena jenis head ini digunakan
untuk vessel dengan tekanan atmosferik sampai dengan 15 bar (Coulson & Richardson, 2005,
hal 817).
Pi Rc Cs
th = +C
2fE + Pi(Cs − 0.2)
1 Rc
Cs = (3 + √
4 Rk
Rc = Di = 1.5 m
Knuckle radius, Rk = 6% dari Rc = 0.06 x 1.5 m = 0.09 m
J = 0.85
E = 135
C = 4 mm
1 1.5
Cs = (3 + √ = 1.77
4 0.09
Tinggi head
OA = th + b + sf
Berdasarkan Tabel 5.6 dan 5.8, Brownell and Young [1959] untuk OD = 1.522 m = 60 in
diperoleh:
icr = 3.625 in
rc = 60
Sf = 2 in
𝐼𝐷
𝐴𝐵 = − 𝑖𝑐𝑟 = 25.875
2
𝐵𝐶 = 𝑟𝑐 − 𝑖𝑐𝑟 = 56.375
𝐴𝐶 = √(𝐵𝐶 2 − 𝐴𝐵 2 ) = 50.086
B = rc-AC = 9.914
OA = Sf + B
= 2 + 9.914 = 11.914 in
LEMBAR PERHITUNGAN
Nozzle Stripper
Umpan
Data yang digunakan dalam perhitungan:
Laju alir umpan, F : 114604.8 kg/jam
Densitas Umpan, ρ : 2016.182 kg/m3
Spesifikasi nozzle standar (Brownell & Young, 1959, Appendix F item 1 dan 2, Halaman
349):
Size = 6 in
Flange Nozzle Thickness = 0.5 in
Diameter of hole in reinforcing plate (DR) = 8.75 in
Length of side of reinforcing plate, L = 20.25 in
Width of reinforcing plate, W = 25 in
Distance, shell to flange face, outside, J = 8 in
Distance, shell to flange face, inside, K = 6 in
Distance from Bottom of tank to center of nozzle
Regular, Type H = 11in
Low, Type C = 8 1/8 in
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Produk Atas
Data yang digunakan dalam perhitungan:
Laju alir umpan, F : 112026.3 kg/jam
Densitas Umpan, ρ : 802.4605 kg/m3
Spesifikasi nozzle standar (Brownell & Young, 1959, Appendix F item 1 dan 2, Halaman
349):
Size = 8 in
Flange Nozzle Thickness = 0.5 in
Diameter of hole in reinforcing plate (DR) = 8 3/4 in
Length of side of reinforcing plate, L = 20.25 in
Width of reinforcing plate, W = 25 in
Distance, shell to flange face, outside, J = 8 in
Distance, shell to flange face, inside, K = 6 in
Distance from Bottom of tank to center of nozzle
Regular, Type H = 13 in
Low, Type C = 10 1/8 in
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Produk Bottom
Data yang digunakan dalam perhitungan:
Laju alir umpan, F : 2578.485 kg/jam
Densitas Umpan, ρ : 1213.721 kg/m3
Spesifikasi nozzle standar (Brownell & Young, 1959, Appendix F item 1 dan 2, Halaman
349):
Size = 0.75 in
Flange Nozzle Thickness = coupling
Diameter of hole in reinforcing plate (DR) = 1.43 in
Length of side of reinforcing plate, L = 10 in
Width of reinforcing plate, W = 12 3/8 in
Distance, shell to flange face, outside, J = 6 in
Distance, shell to flange face, inside, K = 6 in
Distance from Bottom of tank to center of nozzle
Regular, Type H = 7 in
Low, Type C = 3.5 in