Water Quality Analysis Introduction
Water Quality Analysis Introduction
2. Page 2 of 6Procedures of Water Quality AnalysisThe general flow of procedures for water quality
analysis is as follows: SELECTION OF PARAMETERS SELECTION OF METHODS PRECISION AND ACCURACY
OF METHOD SELECTED AS PER REQUIREMENT PROPER SAMPLING PROPER LABELING PRESERVATION
CHAIN-OF-CUSTODY PROCEDURES ANALYSIS REPORTINGSELECTION OF PARAMETERSThe parameters of
water quality are selected entirely according to the need for a specific use of that water.Some examples
are: Drinking Industries As per WHO/CPCB Standards As per specific requirement Irrigation Domestic
Consumption pH As per BIS Standards Conductivity Sodium & Potassium Water Bodies Nutrients As per
CPCB guidelines Specific compounds M.Tech. / Water Quality Laboratory / Handout – 01 / Prepared by:
Ritabrata Roy (ritroy@gmail.com)
3. Page 3 of 6 However, some of the most common parameters followed for checking potability and
industrial use in India are as follows: PARAMETERS Physical Inorganic / Toxic Metals Organic,
Bacteriological Biology Radioactive Chemical Nutrient & Elements Demand Temperature Copper Total
Coliform Phytoplankton Colour Hardness Chromium Zooplankton Alpha Emitter Faecal Coliform Odour
Calcium Cadmium BOD Beta Emitter Taste Magnesium Zinc COD Chloride Lead Phenols Turbidity
Sulphate Mercury Oil & Grease pH Fluoride Iron Pesticides Conductivity Alkalinity Manganese
NitrateTotal Dissolved Solids Nitrate Phosphate SELECTION OF METHODS The methods of water quality
analysis are selected according to the requirement. The factors playing key role for the selection of
methods are: (i) Volume and number of sample to be analyzed (ii) Cost of analysis (iii) Precision required
(iv) Promptness of the analysis as required PRECISION AND ACCURACY OF METHOD SELECTED AS PER
REQUIREMENT What precision and accuracy to be maintained against a particular method is selected
according to the need. The factors influencing this decision includes: (i) Cost (ii) Parameter (iii) Use
CHAIN–OF–CUSTODY PROCEDURES Properly designed and executed chain-of-custody forms will ensure
sample integrity from collection to data reporting. This includes the ability to trace possession and
handling of the sample from the time of collection through analysis and final disposition. This process is
referred to as “chain-of-custody” and is required to demonstrate sample control when the control when
the data are to be used for regulation or litigation. Where litigation is not involved, chain-of-custody
procedures are useful for routine control of samples. M.Tech. / Water Quality Laboratory / Handout – 01
/ Prepared by: Ritabrata Roy (ritroy@gmail.com)
5. Page 5 of 6PROPER SAMPLINGProper sampling is a vital condition for correct measurement of water
quality parameters. Even if advancedtechniques and sophisticated tools are used, the parameters can
give an incorrect image of the actualscenario due to improper sampling. The proper sampling should
fulfill the following criteria:1. Representative: The data must represent the wastewater or environment
being sampled. So, the following factors must be well planned for proper sampling: (i) Process of
Sampling (ii) Sampling size/volume (iii) Number of Sampling Locations (iv) Number of Samples (v) Type
of Samples (vi) Time Intervals During sampling, these factors must also be taken care of: (a) Choosing of
proper sampling container (b) Avoiding contamination (c) Ensure the personal safety of the collector2.
Reproducible: The data obtained must be reproducible by others following the same sampling and
analytical protocols.3. Defensible: Documentation must be available to validate the sampling
procedures. The data must have a known degree of accuracy and precision.4. Useful: The data can be
used to meet the objectives of the monitoring plan.PROPER LABELINGProper labeling prevents sample
misidentification and ensures the responsibility and accountability of thecollector. The sample container
should be labeled properly, preferably by attaching an appropriately inscribed tagor label. Alternatively,
the bottle can be labeled directly with a water-proof marker. Barcode labels are also
availablenowadays.Information on the sample container or the tag should include at least: (i) Sample
code number (identifying location) (ii) Date and time of sampling (iii) Source and type of sample (iv) Pre-
treatment or preservation carried out on the sample (v) Any special notes for the analyst (vi) Sampler’s
namePRESERVATIONThere is usually a delay between the collection and analysis of a sample. The nature
of the sample can be changedduring this period. Therefore proper preservation is required in the way to
laboratory after collection, and in thelaboratory upto when analysis starts. M.Tech. / Water Quality
Laboratory / Handout – 01 / Prepared by: Ritabrata Roy (ritroy@gmail.com)