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salt analysis
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14 views4 pagesSalt Analysis
salt analysis
Uploaded by
Akto StatecommitteeCopyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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a
QUALITATIVE ANALYSIS
SALT ANALYSIS:
PHYSICAL EXAMINATION
EXPERIMENT
OBSERVATION
INFERENCE
COLOR OF SALT IS NOTED
obtained
White or cofourloss salt is
‘Absence of Cu”,Fo”,Fo" Ni" Win"
Solubility
Soluble
‘Absence of sulphates and carbonates of
calcium and barium
Odour if salt is noted
4] Ammoniacal smell is note
2]Vinegar smell is noted
1] NE" is prosent
2ICH,COO is present
ELAME TEST
‘Take a pinch of salt and add 2 or 3
‘drops of con HCl, make s paste of It
and show it tawards the flame using
2 glass rod.
1] Grassy graen flama
2] Crimson red fame
3] Brick red flame
4] Green flashes
§] Bright bluish green
1] Ba®* is present |
2] 5 is present
3] Calis present
4] MPs present
5] Gu" Is preser
Ash test
‘Take 2 mi of salt solution in a test
fube and then add 4 or 2 drops of
con. HINOs and a litte cobalt nitrate
Solution Boi it, ip a fier paperin it
and then bum t into aches
1] Blue ash is noted
2] Gteen ash is noted
IP ink ash is noted
AAP is present
2]zi" Is present
31Mg"" is present
Carbonate[Co] Brisk effervescence with the | Carbenate ion is present
To a test tube of salt solution add | evolution of colourless
a few drops of dil. HCI odourless gas is formed that
can tum lime water milk
Acetate[CH,COO4 Small of vinegar is ebtained | Acetate ion is present
pinch of salt is taken Is rubbed
with diLHS04
Chloride[CLy
pinch of salt is taken in 8 test
tube and is heated along with
con,H2S04
‘Acolourless gas is obtained
which give a dense white,
furnes when a glass rod
dipped in NH,OH is:
Introduced to the mouth of
the test tube
Chloride ion is present
Nitrate[NO,]
‘A pinch of salt is taken in a dry
test tube and is heated along with
con.H,50, After boiling a paper
ball is added.
Sulphate[$O.*]
To a test tube a salt solution add
4 or 2 drops of BaCl,
Acredidish-brovrn vapour is
obtained INO; ges]
Nitrate ion is present
A thick white precipitate is
formed
Sulphate jan js present ‘CONFIRMATORY TEST FOR ANIONS
EXPERIMENT ‘OBSERVATION INFERENCE
Carbonate Ambite precipitate is obtained | Presence of carbonate is confirmed
4. To a test lube of salt solution ade 1 or 2 | whieh is soluble in di HCl
‘drops of BaCl,
2, Alitie of salt solution is teated with | Awhile precipitate is obtained’ | Presence of carbonate is confirmed
Mgso4
Acatate Acdeep red coloration is formed | Presence of acetate is confirmed
1. To a test tube of salt solution acid 2
sdtops of FeGia solution
2, Prepare a solution of solid salt Vinegar smell is obtained Presence of acetate is confirmed
H2C204 and 2 drops of water,
Chloride A white curdy precipitate Is Presence of Chloride ian is confirmed,
1. A test tube of salt solution is acidified | obtained which is soluble in
‘with di HNO3 and then itis boded,caoled | NH4OH.
and AgNOS is added to it.
Greenish yellow gas is formed. | Presence of Chioride ion is confirmed
2. Propare a solution of MnO2 and
con. H2S04_
Nitrate
Brown ring test A brown ring is formed at the Nitrate is confirmed
1. To atest tube of salt solution add equal | junctian of tw layers .
lume of freshly prepared FeSO
solution. Te this con.H2804 is carefully
added along tha side of the tast tube.
Deep blue coloration is formed | Nitrate is canfimed
2. To.a test tube of salt eolution add a few
drops of diohenylamine
Sulphate White precipitate which is Suiphato is confirmed
1. To test tube of sit solution add a few | insoluble in diLHCl is formed
drops of lead avetate S0/*+ PbICHSCOO!2 + PDSO4 +
2CH3000-
2. A litle of sat solution is acicfied with | White pracipitata which is